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Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]I am wondering if the oxidation product of ethanol
is acetaldehyde or acetic acid , or if e ...
20-10-2006 at 04:52
by: Hilski
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote][i]Originally posted by chemoleo[/i]
Oh how annoying I can't access the patent. It requires ...
19-10-2006 at 21:15
by: Hilski
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]a good rule of thumb is that a
10 gauge wire will have a resistance of one miliohm per foot ...
19-10-2006 at 00:42
by: Hilski
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]Nice little setup! Just a wire shunt will give an accurate current
as voltage reading on a c ...
18-10-2006 at 18:44
by: Hilski
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
Inspired by Cycloknight's posts in the Toluene--->Benzaldehyde thread, I decided to have a go at ...
18-10-2006 at 09:18
by: Hilski
Distillation set questions
I think it would be safe to say that the largest thing I would ever try to distill would fit in a 10 ...
11-10-2006 at 16:22
by: Hilski
Distillation set questions
I plan on buying the equipment needed for doing distillations and I had a couple of questions.

I ...
11-10-2006 at 13:19
by: Hilski
MnO2 -> MnSO4; What is the best route?
Thank you guys for all the tips. All this info will definately come in handy for future projects.
9-10-2006 at 18:02
by: Hilski
MnO2 -> MnSO4; What is the best route?
That was a rather interesting read.

I decided to just dissolve the MnO2 in HCl and precipitate wi ...
8-10-2006 at 20:33
by: Hilski
MnO2 -> MnSO4; What is the best route?
[quote]MnO2 + H2O2 + H2SO4 => O2 + 2H2O + MnSO4[/quote]

Thank you. I was hoping that was the ...
5-10-2006 at 04:31
by: Hilski
MnO2 -> MnSO4; What is the best route?
[quote][i]Originally posted by guy[/i]
I used 3%. But looking at the scale of your experiment, it ...
4-10-2006 at 23:05
by: Hilski
MnO2 -> MnSO4; What is the best route?
[quote][i]Originally posted by guy[/i]
Is the H2O2 method too expensive for you guys or something? ...
4-10-2006 at 07:23
by: Hilski
MnO2 -> MnSO4; What is the best route?
[quote]Incidentially, why is this thread under organic...still?[/quote]

Yeah, sorry about that. ...
3-10-2006 at 19:01
by: Hilski
Thanks
This is very informative. Thanks for all the replys.

My intentions are to combine any MnSO4 that ...
3-10-2006 at 15:07
by: Hilski
MnO2 -> MnSO4; What is the best route?
[quote]
6) Indirect method : React MnO2 with HCl ( careful ! Cl2 gas is evolved as a by-product) to ...
2-10-2006 at 19:56
by: Hilski
MnO2 -> MnSO4; What is the best route?
I have about 1kg of MnO2 that I would like to try and convert to MnSO4, and I was wondering what the ...
2-10-2006 at 08:49
by: Hilski
Amino alcohol via Akabori, trial run
[quote]I have tried twice this reaction increasing time even 2x without stirring and yields were at ...
28-9-2006 at 12:39
by: Hilski
Stirrer/Hotplate Question
This may be a dumb question, but how important is it that the alanine/benzaldehyde be continuously s ...
27-9-2006 at 07:55
by: Hilski
Cyanate substitutes for CBrN
My apologies.
It will not allow me to edit or delete the original post. I assume it's because it ...
22-9-2006 at 08:17
by: Hilski
Cyanate substitutes for CBrN
[quote][i]Originally posted by Nicodem[/i]
Show some damn minimum level of respect for this forum!
...
21-9-2006 at 17:18
by: Hilski
Cyanate substitutes for CBrN
You are correct in your assumption. Thank you very much for the reply.
20-9-2006 at 16:25
by: Hilski
Benzyl Alcohol -> Benzaldehyde via Silica Gel Supported Jones Reagent
Seems the answer was right here all along. Or at least something close. I suppose that as long as ...
20-9-2006 at 12:50
by: Hilski
Cyanate substitutes for CBrN
uh...yeah, I know that.

I was referring to this little snippett that I have seen in more than one ...
20-9-2006 at 10:40
by: Hilski
Cyanate substitutes for CBrN
I was just curious which (if any) cyanate compounds can be substituted for CBrN in production of a ...
19-9-2006 at 19:29
by: Hilski
Benzyl Alcohol -> Benzaldehyde via Silica Gel Supported Jones Reagent
Anyone ever try this? Seems way too easy to be true.


[b]Representative Procedure[/b]

Dry si ...
18-9-2006 at 14:35
by: Hilski
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