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Chloropicrin synthesis
I am fairly certain the chlorination here requires alkaline conditions, to convert the nitromethane ...
12-7-2013 at 16:09
by: AndersHoveland
Oh yeah, no reason to be paranoid...
[rquote=241751&tid=19386&author=johansen] the NSA can't factor your private key.[/rquote]
T ...
12-7-2013 at 15:36
by: AndersHoveland
Best way to get rid of hypochlorite?
H2O2 would probably work. It reacts with hypochlorite to form O2 and NaCl.

H2O2 typically does no ...
11-7-2013 at 21:09
by: AndersHoveland
Acetic anhydride preparation
I think sulfur dichloride could be used to dehydrate acetic acid.

4 AcOH + 2 SCl[sub]2[/sub] --&g ...
11-7-2013 at 01:18
by: AndersHoveland
Trichloride failure
Just keep the amounts small, do not have more than tiny amounts in one place. I would not suggest ma ...
10-7-2013 at 21:56
by: AndersHoveland
Isopropyl Alcohol (2-propanol) Peroxides
[rquote=291734&tid=21495&author=kristofvagyok]Today afternoon I will start an experiment wit ...
10-7-2013 at 21:40
by: AndersHoveland
Synthesising Copper Hypophosphite
[quote]
"...it is known that phosphorous acid, reduced with nascent hydrogen, yields phosphine and ...
10-7-2013 at 18:41
by: AndersHoveland
Ethanol chlorination..
Under some conditions, chlorine reacts with ethanol to form ethyl hypochlorite. For this reason, it ...
10-7-2013 at 16:58
by: AndersHoveland
Manuf. of chlorocompounds
Some compounds can be easily chlorinated at room temperature. Acetone easily reacts with chlorine, e ...
10-7-2013 at 16:40
by: AndersHoveland
Who here is capable of Non-Peroxide initiators?
I still think that adding KClO3 would greatly help the explosive properties of Cu2C2. Let's not forg ...
10-7-2013 at 16:30
by: AndersHoveland
Isopropyl Alcohol (2-propanol) Peroxides
That isopropanol could be peroxidated in storage is not too surprising. That alpha hydrogen atom is ...
10-7-2013 at 15:26
by: AndersHoveland
Who here is capable of Non-Peroxide initiators?
Is this just complete ignorance of chemistry? What is the problem if you can't find AgNO3 ? Just [i] ...
10-7-2013 at 15:04
by: AndersHoveland
Home made spectrometer
[rquote=55019&tid=4831&author=Quibbler]I've had a look at the spectrum of some LEDs.[/rquote ...
10-7-2013 at 14:54
by: AndersHoveland
Who here is capable of Non-Peroxide initiators?

There is also copper acetylide, though I am not sure whether it would be an effective primary.
[ ...
10-7-2013 at 14:16
by: AndersHoveland
Who here is capable of Non-Peroxide initiators?
[rquote=291653&tid=25018&author=The_Davster]If you have aminogunanidine and nitrite, do not ...
10-7-2013 at 14:03
by: AndersHoveland
Who here is capable of Non-Peroxide initiators?
Another old primary is "Tetrazene"
[quote]
[file]24180[/file]

Tetrazene was first prepared by ...
10-7-2013 at 12:57
by: AndersHoveland
Who here is capable of Non-Peroxide initiators?
What about lead or mercury fulminate?

[rquote=291633&tid=25018&author=golfpro]to even get ...
10-7-2013 at 12:06
by: AndersHoveland
Trichloride failure
[rquote=291636&tid=25005&author=chemcam]I was thinking of doing it with the chloroform layer ...
10-7-2013 at 12:01
by: AndersHoveland
Trichloride failure
Nitrogen trichloride is [i]much[/i] more sensitive than nitroglycerin!

Nitrogen trichloride [i]f ...
10-7-2013 at 11:51
by: AndersHoveland
Copper acetate problem. Muddy brown solution
Both copper and manganese(III) can form unusual structured complexes with acetate. These might not b ...
10-7-2013 at 00:51
by: AndersHoveland
Trichloride failure
Yes indeed. One time the door was left open to a little room under the big pool at my university. I ...
10-7-2013 at 00:29
by: AndersHoveland
Trichloride failure
This is a little topic, but we all know that hydrazine can be made from hypochlorite and ammonia. So ...
9-7-2013 at 23:27
by: AndersHoveland
Trichloride failure
The pH has to be within a certain range, if it is too low or too high, nitrogen trichloride will not ...
9-7-2013 at 21:56
by: AndersHoveland
Hottest & Most Heat-Producing Chemical Reaction
The reaction between Beryllium and Oxygen releases more energy per unit weight (24.36 kJ/g) than any ...
9-7-2013 at 00:27
by: AndersHoveland
Ozone solubilities - Chlorocarbons
From what I have read, ozone is soluble in carbon tetrachloride.

I am not really sure how compati ...
8-7-2013 at 23:53
by: AndersHoveland
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