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Quinone to make Energetic Compound
Alternatively, one could begin with nitro-quinone. The oxidation with nitric acid is tricky. You mus ... |
19-6-2010 at 21:40
by: Anders Hoveland |
Preparation of Iodomethane
Iodomethane is known to react with anhydrous AgClO4 dissolved in benzene to make AgI precipitate and ... |
19-6-2010 at 21:15
by: Anders Hoveland |
Assorted Extreme Reactions
Thanks for doing the reaction. I do not happen to have any SO2Cl2 on hand.
A possible explanation f ... |
19-6-2010 at 21:00
by: Anders Hoveland |
Horribly Dangerous, but useful, Reaction
But there are not too many ways for the basement chemist to obtain anhydrous HClO4. The Ag2C2 is a n ... |
19-6-2010 at 20:41
by: Anders Hoveland |
Idea for Energetic Ring
#1 nitrosyl bisulfate, made by bubbling NO and NO2 into concentrated H2SO4, adds the NO group, simil ... |
19-6-2010 at 20:35
by: Anders Hoveland |
di[nitromethylene] diazo, N-oxide
Alternatively NH2CHNOH might react with a limited amount of very dilute H2O2 to make NO2CH2NNCH2NO2. ... |
19-6-2010 at 20:03
by: Anders Hoveland |
Exotic thermites & analogs
I have tried magnesium powder with sulfur, and Mg powder with MnO2.
Adding sulfur to thermite seems ... |
19-6-2010 at 19:36
by: Anders Hoveland |
Horribly Dangerous, but useful, Reaction
I bubbled acetylene into a solution of AgClO4.
Ag2C2 precipitated out at the bottom, and presumably ... |
19-6-2010 at 19:30
by: Anders Hoveland |
Ethyl Perchlorate
I once prepared nitromethylene perchlorate, by using AgClO4 dissolved in toluene and adding iodine a ... |
19-6-2010 at 19:19
by: Anders Hoveland |
Square Ring Explosive, Rough Synthesis
I have designed several routes for new energetic compounds. However, most of them, including this on ... |
19-6-2010 at 18:58
by: Anders Hoveland |
Ethylene diamine perchlorate
And how to methylate NH2OH? Maybe start with the methyl group to begin with. I think HSO3- might red ... |
19-6-2010 at 18:21
by: Anders Hoveland |
High Yield Hydrazine Synthesis?
I have not actually tried this one.
Trichloroisocyanuric acid is available at pool supply stores in ... |
19-6-2010 at 18:06
by: Anders Hoveland |
sulfuric acid from gypsum CaSO4
3Ca(BO3)2 + 6NH4Cl heated--> 3CaCl2 + 2H3BO3 + 6NH3gas
I have a beginning chemistry book that sa ... |
19-6-2010 at 17:41
by: Anders Hoveland |
Reactions to Easily make new Precursors
I am sure someone will find something interesting in here and try a few of the reactions. I just had ... |
18-6-2010 at 14:23
by: Anders Hoveland |
1,2,2 trinitro propane
Also, this has many resonance states, so could be expected to be stable. Plus you could stick on 2 e ... |
18-6-2010 at 14:08
by: Anders Hoveland |
1,2,2 trinitro propane
Analine and Cl2O6 (which has a ClO2+ in it) might make the intermediate phenylNHClO2 (and an analine ... |
18-6-2010 at 13:49
by: Anders Hoveland |
1,2,2 trinitro propane
I have designed molecular structures, for instance. In addition, 1,2,4-tri(nitromethylene) pentazole ... |
18-6-2010 at 13:38
by: Anders Hoveland |
New Energetic Materials - Current Research
I saw one researcher prepare compounds with the ---CCSF5 group, a triple bond between the carbons. T ... |
18-6-2010 at 13:21
by: Anders Hoveland |
Advanced Super Acid Chemistry
When you acidify thiosulfate, it turns yellow, but opaque. I would have thought that HI reacts with ... |
18-6-2010 at 13:11
by: Anders Hoveland |
sulfuric acid from gypsum CaSO4
The main advantage of the technique is that it could operate at a lower temperature than the oxidati ... |
18-6-2010 at 13:01
by: Anders Hoveland |
Reactions to Easily make new Precursors
If you are willing to sort through a bunch a "trash", you will likely find several interesting react ... |
18-6-2010 at 12:53
by: Anders Hoveland |
Reactions to Easily make new Precursors
IF7 + ClF3 + 2PtF6 --> IF6PtF6 + ClF4PtF6
4(IF6+) + 2(MnF6)-2 --> 2MnF3 + IF7 + F2
4(ClF4+) ... |
18-6-2010 at 12:31
by: Anders Hoveland |
Reactions to Easily make new Precursors
6SbF5 + 3I2 --> 5SbF4I + IF4SbF6
15SbF3 + 6IF5 --> 5SbF4I + IF4SbF6 + 9SbF5
Cl2O7 + ClO3- ... |
18-6-2010 at 12:19
by: Anders Hoveland |
Reactions to Easily make new Precursors
Making N2H4:
A buret slowly drips NaOCl bleach into a beaker. The beaker has two layers, a top NH4O ... |
18-6-2010 at 12:04
by: Anders Hoveland |
Reactions to Easily make new Precursors
4IF5 + 10Ca(ClO3)2 --> 2I2O5 + 10CaF2 10ClO2 + 5Cl2O6
5AgF + 3I2 in benzene is known to make 5Ag ... |
18-6-2010 at 11:56
by: Anders Hoveland |
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