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Ammonium Perchlorate manufacture
6 Fe(2+) + ClO3- + 6H+ ---> Fe(3+) + Cl- + 3H2O

Notice the equilibrium is heavily dependent on ...
29-1-2008 at 07:23
by: 12AX7
Chlorate as an all-purpose oxidizer?
It's usually given the formula NiOOH, I think.

Segue-ing into nickel, can it be oxidized in neutr ...
28-1-2008 at 09:53
by: 12AX7
Perchlorate manufacture (not) with Graphite
Yes, all three of them. At least, what area of the anode *is* plated...

Tim
27-1-2008 at 11:33
by: 12AX7
My Cells (plural)
Seems proper to put in here, as all three are running perchlorate at the moment.

Put together two ...
26-1-2008 at 21:20
by: 12AX7
remove H2SO4 from H20?
H - two - O, not H-twenty.

Sure are ways, but you're kind of fighting thermodynamics here. Notic ...
26-1-2008 at 20:17
by: 12AX7
Advice needed for HF synthesis
Go for ammonium bisulfate, it's an acidic mixture after all.

Don't know what kind of heat you'd n ...
26-1-2008 at 19:46
by: 12AX7
Ester hydrolysis
Dur, UTFSE!!!! :rolleyes:

http://www.google.com/search?q=utfse

A tip: www.acronymfinder.com an ...
26-1-2008 at 00:19
by: 12AX7
What about high-silicon iron as a substrate?
I have both transformer iron and lump ferrosilicon (75%, IIRC).

Transformers rust every day, I do ...
25-1-2008 at 19:48
by: 12AX7
The lead salts preparation thread!
I often get clear, colorless, well-formed crystals from colored solutions -- yeah, after forgetting ...
25-1-2008 at 19:47
by: 12AX7
The lead salts preparation thread!
Ooh, octahedral! I love octahedra! :)

Sweet! (And probably literally, like lead acetate!)

Tim
25-1-2008 at 13:41
by: 12AX7
Chlorate as an all-purpose oxidizer?
As many of you know, I have a lot of chlorate on hand. As such, I look for ways to use it.

One I ...
25-1-2008 at 10:43
by: 12AX7
Plating Titanium
I've tried running the titanium as cathode in an alkaline solution. All I get is a cruddy deposit t ...
24-1-2008 at 06:47
by: 12AX7
Copper in grams per liter
Damnit Jim, I'm a doctor, not a spectrophotometer! :P

I would guess somewhere under 0.2M. Why do ...
23-1-2008 at 22:28
by: 12AX7
Updated my website
Put some pertinent information up, and two other things bumping around:
http://webpages.charter.net ...
23-1-2008 at 19:10
by: 12AX7
More on PbO2 electrodes
I'm reminded of something wholly useless I did.

I had a moist sample of PbO2 powder in a jar. On ...
21-1-2008 at 18:50
by: 12AX7
AP dimer-Trimer Seperation
On a similar subject, what is the configuration of MEKP? Is it a cycle like TATP? Is it 1,2,3-cis ...
21-1-2008 at 05:41
by: 12AX7
One last one. May be hopeless, though...
ARGH! SHRINK IMAGES BEFORE POSTING!
21-1-2008 at 05:38
by: 12AX7
More on PbO2 electrodes
My stock is just as springy in current condition as it is annealed to orange heat.

It sands just ...
20-1-2008 at 20:32
by: 12AX7
PC PSU to laboratory PSU
[quote][i]Originally posted by bio2[/i]
How's that?
[/quote]

Still no excuse! ;)

I haven't b ...
20-1-2008 at 15:32
by: 12AX7
Perchlorate chemistry
Fairly he says! Come to think of it, the perchlorates of Na and K may have the largest difference i ...
20-1-2008 at 15:27
by: 12AX7
More on PbO2 electrodes
I use an extra length of titanium strip and bolt a copper strap onto the end.

The wirebrush I hav ...
20-1-2008 at 11:29
by: 12AX7
PC PSU to laboratory PSU
An MOT is good for up to, say, 10A primary current (with fan), which is 1200VA, but not 1200VAR. To ...
20-1-2008 at 11:26
by: 12AX7
PC PSU to laboratory PSU
Don't use capacitors -- use inductors. Much more economical for large supplies, and capacitors make ...
20-1-2008 at 08:53
by: 12AX7
Perchlorate chemistry
From Technochemistry;

[quote][i]Originally posted by chloric1[/i]
[quote][i]Originally posted by ...
20-1-2008 at 08:45
by: 12AX7
PC PSU to laboratory PSU
Switchmode circuits can be very simple: all the complexity gets tied up in a chip. Take the UC3842 ...
20-1-2008 at 06:03
by: 12AX7
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