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(HPO3)n Dehydrating agent (polyphosphoric or metaphosphoric acid) Alright, well I really doubt anyone here can answer from experience. In all likelihood the answer is ... |
1-5-2021 at 14:28 by: njl |
Synthesis of Ethyl Methylphenylglycidate [rquote=659221&tid=157363&author=Amos] The actual phenylacetone precursor found in clandesti ... |
1-5-2021 at 14:23 by: njl |
Acetic anhydride preparation Yes I believe in earlier pages of this thread. Sometimes a pain to read through, but I remember it b ... |
1-5-2021 at 14:15 by: njl |
(HPO3)n Dehydrating agent (polyphosphoric or metaphosphoric acid) You're gonna have to elaborate on "sulfuric monochloride". Do you mean chlorosulfuric acid? Or disul ... |
1-5-2021 at 12:37 by: njl |
Synthesis of Ethyl Methylphenylglycidate Yes, my mistake. The precursor compound is sold as a phenylacetone precursor under the name "BMK gly ... |
30-4-2021 at 19:01 by: njl |
Ketalization of Phenol Cyclohexanone is just a regular ketone, it will form a ketal under the conditions commonly used for ... |
30-4-2021 at 15:00 by: njl |
Synthesis of Ethyl Methylphenylglycidate Cool your jets SC. I also thought this thread was about [b]benzyl[/b] glycidate (the compound you're ... |
30-4-2021 at 14:57 by: njl |
Methyl iodide (iodomethane) woes (Red P method) A funnel clogged with red p sounds like a pain... the phosphorus might slowly react to various oxide ... |
30-4-2021 at 06:19 by: njl |
Most toxic compound OTC? We need a stickied thread on OTC antimatter ASAP |
30-4-2021 at 04:35 by: njl |
preparation/acquisition of acetone (weird problem ik) Ketonic decarboxylation is a known reaction that has been thoroughly documented. While it may be a s ... |
29-4-2021 at 10:23 by: njl |
Recovery of styrene monomer from polystyrene Off topic to this thread, but what did you end up doing with it?
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29-4-2021 at 04:50 by: njl |
Acetic anhydride preparation Atara is referring to a thread on the vespiary by user Scarecrow called "Reliable OTC Acyl chloride ... |
29-4-2021 at 02:57 by: njl |
preparation/acquisition of acetone (weird problem ik) This is just the beginning of an idea (can't give you any conditions at the moment), but perhaps the ... |
29-4-2021 at 02:46 by: njl |
distilling Metheglin I am speaking from my experience with [url=https://www.walmart.com/ip/Great-Value-Distilled-White-Vi ... |
28-4-2021 at 14:12 by: njl |
Recovery of styrene monomer from polystyrene [rquote=659009&tid=157360&author=unionised]
Also works with PMMA
[/rquote]
Yielding met ... |
28-4-2021 at 14:01 by: njl |
Recovery of styrene monomer from polystyrene The gist of polystyrene to styrene monomer is mostly thermal cracking as far as I know. There are so ... |
28-4-2021 at 05:08 by: njl |
Making n-butyl bromide (1-bromobutane) for TBAB (Tetrabutylammonium bromide) synthesis There are good reviews for chemcraft in one of the reagents acquisition threads. |
27-4-2021 at 17:00 by: njl |
Isolation of 1,1-diphenyl ethanol If what I suggested works I don't see why you shouldn't go for it, however I think Drac is right in ... |
27-4-2021 at 16:58 by: njl |
Isolation of 1,1-diphenyl ethanol You can try removing more of the hexane then cool as low as possible and wait. To improve yield and ... |
27-4-2021 at 13:09 by: njl |
distilling Metheglin
[quote]
The problem here is vocabulary and definitions. The sour end liquid is called badly "vine ... |
27-4-2021 at 10:54 by: njl |
Preparation of elemental phosphorus Yes, I think it would be necessary to remove the phosphorus as it forms by distilling it off. But th ... |
27-4-2021 at 10:37 by: njl |
distilling Metheglin
[quote]
Metheglin / meed?
me·theg·lin
[Welsh meddyglyn : meddyg, medicinal (from Latin medi ... |
27-4-2021 at 08:18 by: njl |
Path to 4-Anisaldehyde Mass harder to visualize for me than volume, so for reference (with a density of 1.6 g/cc) .2 grams ... |
27-4-2021 at 07:48 by: njl |
Preparation of elemental phosphorus Atara, if you do the math: 2 percent solution of Ca3(PO4)2 in 1 Kg molten salt = 20 grams Ca3(PO4)2 ... |
27-4-2021 at 06:18 by: njl |
Effecting a separation of two, nearly identical compounds PubChem claims that AN is somewhat soluble in acetone, while urea is not. |
27-4-2021 at 04:59 by: njl |
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