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benzyl chloride
Ok I see. I could easily produce ZnCl2*hydrate but can I dry it will the H2SO4?

Edit: STupid que ...
28-6-2007 at 10:43
by: guy
benzyl chloride
Can you make the HCl more "concentrated" by adding concentrated H2SO4? For example, if I wanted to m ...
28-6-2007 at 10:16
by: guy
Catalytic oxidation of alcohols/aldehydes with Copper VIDEO
[quote][i]Originally posted by froot[/i]
Maybe the copper took on that typical pink colour after it ...
25-6-2007 at 21:45
by: guy
Catalytic oxidation of alcohols/aldehydes with Copper VIDEO
But doesn't the methanol oxidation over copper to form methanal go through a similar procedure at hi ...
25-6-2007 at 01:40
by: guy
Catalytic oxidation of alcohols/aldehydes with Copper VIDEO
http://www.netexperimente.de/netexperimente/index.php?c=chemie&section=121

The reaction susta ...
24-6-2007 at 22:13
by: guy
Copper (I) oxide/Carbon reductions
Check out this site. It's like youtube but for chemistry. There is a video of the Cu2O/C reduction ...
24-6-2007 at 22:06
by: guy
Need Help - Ammonia Question
I would say run it through a flask submerged under dry ice and acetone. This will be cold enough to ...
23-6-2007 at 02:05
by: guy
Best method of producing Cu(I)Cl?
[quote][i]Originally posted by garage chemist[/i]
Though dont use sodium dithionite or products con ...
22-6-2007 at 17:15
by: guy
gallium spoon in tea
Can you use Gallium be used to activate Al as Hg does?
22-6-2007 at 16:22
by: guy
Best method of producing Cu(I)Cl?
Sufite is the fastest. You can find solid sodium sulfite in Iron Out which is cheaply available in ...
22-6-2007 at 16:01
by: guy
Can iodine tincture be used for Al(Oi-Pr)3 synthesis?
[quote][i]Originally posted by Eclectic[/i]
Also that 1% water in your 99% IPA is a real show stopp ...
22-6-2007 at 12:29
by: guy
Can iodine tincture be used for Al(Oi-Pr)3 synthesis?
I tried adding some CuCl2*2H2O to some 99% isopropanol and a bit of I2. Not much happened. I heate ...
21-6-2007 at 23:42
by: guy
Can iodine tincture be used for Al(Oi-Pr)3 synthesis?
I used solid iodine and 99% Isopropanol and Al foil. I used 10g of Al foil, 150mL i-PrOH, and a tin ...
21-6-2007 at 15:37
by: guy
Can iodine tincture be used for Al(Oi-Pr)3 synthesis?
[quote][i]Originally posted by not_important[/i]
Do you mean Al(i-Pr)3 or Al(O i-Pr)3 ?

In the ...
20-6-2007 at 23:19
by: guy
Can iodine tincture be used for Al(Oi-Pr)3 synthesis?
I'm just wondering because I don't know if the synthesis requires water free conditions.

[Edited on ...
20-6-2007 at 22:01
by: guy
Stability of Chromium Salts in Aqueous Soln.
So any update on the separation?
20-6-2007 at 14:13
by: guy
Ethanol + H2O2
It is probably ethanal (acetaldyhyde) and ethyl acetate. Both smell fruity.
18-6-2007 at 13:56
by: guy
Extracting Glycine and Proline from gelatin
Ah the copper picrate route seems pretty good. A solution of picrate salt is safe right?
16-6-2007 at 18:42
by: guy
Extracting Glycine and Proline from gelatin
Gelatin contains a fair amount of glycine and proline. Is there a way to separate them?

From w ...
16-6-2007 at 14:59
by: guy
Methanol Dehydration
[quote][i]Originally posted by garage chemist[/i]
The standard method for ethylene preparation from ...
15-6-2007 at 23:26
by: guy
Formylation of Salicylic acid?
Thanks, according to that I should use at least a 10:1 NaOH to phenol molar ratio :o
I could do tha ...
12-6-2007 at 13:15
by: guy
Formylation of Salicylic acid?
How do you guys get access to ftp's?
12-6-2007 at 12:46
by: guy
Formylation of Salicylic acid?
I know salicylic acid can be formylated with CHCl3 with 20% yield in the ortho form. I need help wi ...
10-6-2007 at 14:35
by: guy
Really colorful oxidation states of ruthenium
Woelen, try and make some awesome catalysts with that. Can you get triphenylphosphine?
7-6-2007 at 12:33
by: guy
Oxidation of ethanol
Ok. so I tested it by adding some of the NaDCC with NaOH and hypochlorite is definietly formed. Ok ...
27-5-2007 at 20:38
by: guy
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