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tryptophan to alpha methyl tryptamine
Correct me if I am wrong, but would it be possible to do a Kochi on tryptophan using Pb(OAc)4 and Li ...
26-5-2012 at 19:22
by: Rich_Insane
Hotplates!
I think anything with low flammability, low specific heat and low volatility will do... I'm just wor ...
9-5-2012 at 20:52
by: Rich_Insane
Hotplates!

[quote]
If you use vegetable oil in a heating bath, especially canola oil, it will go rancid befo ...
8-5-2012 at 12:25
by: Rich_Insane
Hotplates!
Hey guys, so I have a quick and slightly related question. I'm at maximum budget, and have to cut ou ...
7-5-2012 at 13:22
by: Rich_Insane
Hotplates!
Hey guys. So I've decided to get a new hotplate. I'm a bit confused on what I should get. I can't af ...
6-5-2012 at 13:19
by: Rich_Insane
A Bit of Market Research
I need various adapters for my lonely reflux condenser. A three necked flask would be so awesome, bu ...
1-5-2012 at 10:04
by: Rich_Insane
how can i dissolved amino acid
Which amino acid? They're all a bit different from each other. I suspect that the COOH and amine gro ...
30-4-2012 at 21:29
by: Rich_Insane
Boric Acid Catalyzed Amidation of Carboxylic Acids

[quote]
Unless I am mistaken, the aldehyde you are trying to oxidize is the aldehyde protecting g ...
30-4-2012 at 21:26
by: Rich_Insane
Opening a lactone - Easy?

[quote]
"Heating a lactone with a base (sodium hydroxide) will hydrolyse the lactone to its paren ...
5-4-2012 at 21:14
by: Rich_Insane
Opening a lactone - Easy?
Hey guys. So there is this reagent I need. The actual carboxylic acid is very, very expensive, but s ...
5-4-2012 at 12:46
by: Rich_Insane
Vanillin Demethylation
I'm no expert, but I think pyridine will accept the methyl group to form methyl pyridinium.
27-3-2012 at 11:28
by: Rich_Insane
Vanillin Demethylation
Not long ago, there was a patent speaking of O-demethylation using thiourea and AlCl3. There was als ...
24-3-2012 at 10:10
by: Rich_Insane
Cold extraction of piperine from black pepper
I've attached the paper for extraction from pepper using DCM, since Megaupload seems to be going thr ...
20-3-2012 at 14:01
by: Rich_Insane
Solvent free oxime formation
Have you seen: [url]http://www.orgmedchemlett.com/content/pdf/2191-2858-1-12.pdf[/url]

They use B ...
20-3-2012 at 13:39
by: Rich_Insane
Hofmann rearrangement
[url=http://www.sciencedirect.com/science/article/pii/S0013468600003807]Electrochemical Hoffman[/url ...
16-3-2012 at 13:58
by: Rich_Insane
Hofmann rearrangement
Semi-on topic: [url=http://www.scribd.com/doc/62402536/The-Preparation-of-Methylamine-Hydrochloride- ...
15-3-2012 at 13:37
by: Rich_Insane
Boric Acid Catalyzed Amidation of Carboxylic Acids

[quote]
Beyond that, using more catalyst will probably only hurt you. Since Aromatic amines like ...
12-3-2012 at 21:24
by: Rich_Insane
Boric Acid Catalyzed Amidation of Carboxylic Acids

[quote]
Also, I assume you'd be planning on using the amide in a hofmann rearrangement (or perhap ...
12-3-2012 at 07:37
by: Rich_Insane
Boric Acid Catalyzed Amidation of Carboxylic Acids
Hello folks!

So I just wanted to post a little proposition or curiosity I have. I've been looking ...
11-3-2012 at 20:32
by: Rich_Insane
caffeine hcl salt
I wonder if bubbling HCL through a solution of caffeine in CCl4 or CHCl3 would work. This would only ...
24-2-2012 at 16:28
by: Rich_Insane
Ideas for new hallucinogens?

[quote]
I can't agree Nicodem ─ by itself, THC is quite mild by comparison to, say, LSD ...
15-2-2012 at 12:59
by: Rich_Insane
Ideas for new hallucinogens?
On the chemistry side of things, Dr. Nichols from Purdue has published a lot of interesting work. He ...
15-2-2012 at 12:28
by: Rich_Insane
Preparation of amides via esters or carboxylic acids?

[quote]
That's odd, because in other posts you have said you were taking college organic chemistr ...
12-2-2012 at 21:27
by: Rich_Insane
NMR Analysis?
Hello. I have a friend who is new to doing organic synthesis at home. He wants to see how he can get ...
10-2-2012 at 12:30
by: Rich_Insane
Preparation of amides via esters or carboxylic acids?
Hey everyone! So I've been thinking about how one can prepare a primary amide (is that the right ter ...
6-2-2012 at 14:16
by: Rich_Insane
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