| Search |
| [Next Page] |
Glycine Perchlorate
Regarding the perchloric acid, I have advocated the NaClO4 + concentrated HCl several times in the p ... |
26-6-2023 at 23:53
by: Microtek |
Glycine Perchlorate
[quote]
The next interest in this exploration is a pure HClO4 sample. Which probably should have ... |
24-6-2023 at 08:49
by: Microtek |
DDNP & related compounds: The über thread!
Easy, but the product is of unknown purity. The test that he does at the end of that video is indeed ... |
21-6-2023 at 22:34
by: Microtek |
DDNP & related compounds: The über thread!
I used a method to produce (organic) nitrite by reducing dilute (ca. 50%) nitric acid with potato st ... |
20-6-2023 at 09:05
by: Microtek |
DDNP & related compounds: The über thread!
Yes, you can use nitric acid or sulfuric acid with a nitrate salt for the nitration of a phenol in t ... |
20-6-2023 at 03:16
by: Microtek |
Preparation of nitrostarch
I tried your method LL, but my NC does not dissolve so cleanly in acetone. I'm sure the reason is th ... |
13-6-2023 at 09:15
by: Microtek |
Preparation of nitrostarch
You can do some other things to remove traces of acid. For instance, place the NS in a coloumn and l ... |
12-6-2023 at 21:49
by: Microtek |
Preparation of nitrostarch
A mixed acid with 38% nitric and 62% sulfuric does not contain any water. If your nitric was 80% con ... |
11-6-2023 at 23:06
by: Microtek |
Nipolyt
I have experimented with the RDX-variant. It works well even in small charges, and is quite sensitiv ... |
8-6-2023 at 12:35
by: Microtek |
Erythritol Tetranitrate
I don't think melt cast ETN is more sensitive than powdered ETN. It is more sensitive WHILE you have ... |
4-6-2023 at 23:57
by: Microtek |
Make plastic explosive out of ETN/PETN & EDGN
The setup looks fine, but add insulation as described above and preferably some vacuum if possible. ... |
1-6-2023 at 08:27
by: Microtek |
Det Cap Strategies
Have you tried setting a detonator off inside it on purpose (and with proper safety measures)? A num ... |
1-6-2023 at 08:18
by: Microtek |
Exotic Primaries - Complex Salts
I think you are supposed to react the product of the acetylization (from heating the guanidine deriv ... |
1-6-2023 at 08:15
by: Microtek |
Make plastic explosive out of ETN/PETN & EDGN
The longer the distillation path, the more you will need to heat it to collect anything. This can be ... |
31-5-2023 at 08:17
by: Microtek |
Exotic Primaries - Complex Salts
I would request that you examine solubilities of the salt as well as the free acid (I know that does ... |
30-5-2023 at 22:29
by: Microtek |
Make plastic explosive out of ETN/PETN & EDGN
I have had some batches of HDN decompose from heating on a steam bath (which of course can't exceed ... |
29-5-2023 at 08:58
by: Microtek |
Make plastic explosive out of ETN/PETN & EDGN
Yes, a vacuum distillation is what I'm talking about. You don't need a very strong vacuum, just enou ... |
27-5-2023 at 13:11
by: Microtek |
Make plastic explosive out of ETN/PETN & EDGN
If you want to concentrate your nitric further, redistil it from more sulfuric acid (distilling from ... |
26-5-2023 at 00:19
by: Microtek |
Make plastic explosive out of ETN/PETN & EDGN
TNT can easily be made with 96% sulfuric acid, and I've done so myself many years ago. The main reas ... |
24-5-2023 at 23:20
by: Microtek |
Make plastic explosive out of ETN/PETN & EDGN
Yes, I would think so. Not as well as NC I'm sure, but you could doubtlessly do it. |
23-5-2023 at 23:45
by: Microtek |
3-amino-1-nitroguanidine Salts
Yes, I've found a couple of patents. CN104370776A:
-------------------------------------------- ... |
23-5-2023 at 07:39
by: Microtek |
3-amino-1-nitroguanidine Salts
Do you have a reference for a good synthesis of a diaminoguanidine salt (or the free base I suppose) ... |
22-5-2023 at 22:28
by: Microtek |
Glycine Perchlorate
I would suggest the aluminum block crater if you can make the GlyP fire in "small" charges (otherwis ... |
21-5-2023 at 01:51
by: Microtek |
Glycine Perchlorate
[quote]
1) Reflux NH4ClO4 + Glycine in a beaker, several hours, evaporate, dry. 2) Reflux NH4ClO4 ... |
20-5-2023 at 13:41
by: Microtek |
3-amino-1-nitroguanidine Salts
Hey Buddy:
Regarding the cyclization of aminonitroguanidine, I found by reading the attached pape ... |
18-5-2023 at 23:03
by: Microtek |
| [Next Page] |
