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Making fire (youtube collaborative video)
Manganese heptoxide is simply to made and can ignite any organic compaund.
It can be preparated sim ...
22-4-2011 at 09:47
by: ItalianChemist
Total synthesis for beginner
[rquote=207469&tid=16044&author=NurdRage]I did,
its the video.[/rquote]
Final yeld?
I'll ...
21-4-2011 at 06:26
by: ItalianChemist
ibuprofen and it's derivatives
[rquote=207459&tid=16085&author=Jor]How did you extract it? With hexane/pentane/heptane/pet ...
21-4-2011 at 04:09
by: ItalianChemist
ibuprofen and it's derivatives
Very interesting :)
I've just extracted about 18g of ibuprofen, this evening I will do 2-(3-nitro-4 ...
21-4-2011 at 01:48
by: ItalianChemist
Total synthesis for beginner
You can made some ethyl esters, but you need a reflux condenser and some acid (such as acetic acid, ...
21-4-2011 at 00:58
by: ItalianChemist
Acyl chloride/ MeOH = esterification?
Acyl chlorides are very reactive and react immediately with the alcool to form ester and HCl.
I thi ...
15-4-2011 at 05:21
by: ItalianChemist
alizarine synthesis
Does anyone have a synthesis of alizarine from anthraquinone?
In my book is reported that alizarin ...
13-4-2011 at 05:26
by: ItalianChemist
purifying toluene properly
toluene can be easily purified, first being shacked with some water, to remove impurities solible in ...
13-4-2011 at 05:06
by: ItalianChemist
Pthtalic acid OTC
[rquote=206619&tid=16009&author=kuro96inlaila]I never expect it to be so simple!:)
Thanks I ...
12-4-2011 at 08:33
by: ItalianChemist
Pthtalic acid OTC
[rquote=206486&tid=16009&author=kuro96inlaila]Is there a way to get phthalic acid from potas ...
12-4-2011 at 02:48
by: ItalianChemist
oxalyl chloride and water
Thanks Ozono!
The other products are phosgene and tricloroacetyl chloride isn't it?
Wow! You have ...
12-4-2011 at 02:41
by: ItalianChemist
Pthtalic acid OTC
I obtained pthalic acid from hydrolisys of pthalic anhydride!
I put some phtalic anhydride in a few ...
10-4-2011 at 05:12
by: ItalianChemist
oxalyl chloride and water
Thanks Ozono, let me know the results!
Isn't used anhydrous dichloromethane in the Shotten-Baumann?
10-4-2011 at 03:01
by: ItalianChemist
oxalyl chloride and water
A few time ago I put oxalyl chloride in not anhydrous solvent.
A lot of withe smoke appeared, i thi ...
8-4-2011 at 12:51
by: ItalianChemist
Looking for Oxalyl Chloride (Swern ox) and 3-bromoanisole
I bought (COCl)2 from Sigma withouth any problem!
19-2-2011 at 12:53
by: ItalianChemist
chemiluminescence!!
The TCPO obtained still smells like 2,4,6-TCP?
I also tried it and when I added oxalyl chloride a l ...
19-2-2011 at 12:49
by: ItalianChemist
Triethylamine complexes
Ops...:(
I will try again with a better procedure!
I would use it also for TCPO synthesis but I do ...
29-1-2011 at 07:17
by: ItalianChemist
Triethylamine complexes
Thanks to all!
I've just tried to neutralize a triethylamine solution in acetone with diluited hydr ...
28-1-2011 at 13:49
by: ItalianChemist
Triethylamine complexes
Thanks a lot! :)
I Will try this as soon as possible!
If i made triethylammonium hydrochloride it ...
26-1-2011 at 07:14
by: ItalianChemist
Concentration of "Dilute" Chemicals
You can concentrate sulfuric acid only boiling it, until withe smokes of SO3 appears.
The other aci ...
26-1-2011 at 06:11
by: ItalianChemist
Triethylamine complexes
Hi! I'm new and i excuse me for my english, but I'm Italian and I kwow it only a little...
I ask fo ...
26-1-2011 at 05:40
by: ItalianChemist

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