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Capillary tube for vacuum distillations
[quote]If all else fails you can use CO2 for most things or scrub O2 from air[/quote]
CO2 would pro ...
4-12-2006 at 03:39
by: Hilski
Capillary tube for vacuum distillations
[quote][i]Originally posted by neutrino[/i]
Sorry, but the He gas sold for balloons and such is not ...
2-12-2006 at 14:02
by: Hilski
No more Providone Iodine over the counter?
Its still available everywhere here. Even the dinky little "every thing's a dollar" chains carry it ...
2-12-2006 at 09:10
by: Hilski
Capillary tube for vacuum distillations
Wow. I would have thought that it would need a lot more than what a balloon could hold, so I'm glad ...
2-12-2006 at 08:58
by: Hilski
Capillary tube for vacuum distillations
Thanks for the replies.

Benzaldehyde is near the top of the short list of things I would like to ...
2-12-2006 at 07:18
by: Hilski
Capillary tube for vacuum distillations
I was just wondering if anyone has ever successfully used a capillary tube to stir/agitate the conte ...
1-12-2006 at 21:31
by: Hilski
Anodizing dye
I always used Rit brand concentrated dye, and never had any problems at all. I mostly anodized thin ...
23-11-2006 at 15:37
by: Hilski
Aldehyde distillation/purification
[quote][i]Originally posted by Nicodem[/i]
You read wrong. It just needs to be neutral (devoid of a ...
19-11-2006 at 06:31
by: Hilski
Aldehyde distillation/purification
I have several hundred ml of an orange mixture of benzaldehyde, toluene and a bit of whatever else m ...
19-11-2006 at 02:05
by: Hilski
Just a few pictures
Here is how the mixture looks after the reaction is complete:

[img]http://www.sciencemadness.org/ ...
6-11-2006 at 07:18
by: Hilski
Anyone ever built an overhead stirrer?
Just an update:

I ended up using (temporarily) a small shaded pole AC motor I had. I think it ca ...
5-11-2006 at 08:41
by: Hilski
"Carbon carbide"
I have heard the head metallurgist in the Q.A. lab at the company I work for, refer to a compound he ...
2-11-2006 at 19:12
by: Hilski
Anyone ever built an overhead stirrer?
Sorry. Let me clarify that. I mean all the ones [u]I[/u] have are stepper motors. I had 2 Epson p ...
1-11-2006 at 14:26
by: Hilski
Anyone ever built an overhead stirrer?
Now I know why I never considered using printer motors. They're ALL bipolar stepper motors, and I d ...
1-11-2006 at 09:23
by: Hilski
Anyone ever built an overhead stirrer?
[quote][i]Originally posted by Magpie[/i]
What about a "chuck" of some kind, like on a drill. Perh ...
31-10-2006 at 10:03
by: Hilski
Anyone ever built an overhead stirrer?
I just took apart an old printer I had. These are the motors that were in it. Are they suitable fo ...
31-10-2006 at 09:35
by: Hilski
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
Just an update: This stuff does indeed work for oxidizing toluene. Sorry, but I don't have any pic ...
31-10-2006 at 09:32
by: Hilski
Anyone ever built an overhead stirrer?
[quote][i]Originally posted by bio2[/i]
A motor from an old printer in a standard clamp on a ring ...
31-10-2006 at 07:35
by: Hilski
Anyone ever built an overhead stirrer?
Yes. Basically I need to make a bearing for the stirrer shaft, to keep it from moving around too mu ...
30-10-2006 at 11:38
by: Hilski
Anyone ever built an overhead stirrer?
I'm going to try and build an overhead stirrer similar to the one shown here:

http://designer-dru ...
29-10-2006 at 10:42
by: Hilski
toluene --> benzaldehyde
[quote][i]Originally posted by herbalextractions[/i]
whats happened to all the pictures? :( [/quote ...
26-10-2006 at 08:37
by: Hilski
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]Keeping some vapor pressure of a volatile
solvent residue or deliberately added impurity li ...
21-10-2006 at 15:04
by: Hilski
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
I almost forgot. Here are a couple of pictures of the cell after about running at 4 amps for 22+ ho ...
20-10-2006 at 20:08
by: Hilski
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]I take it you mean the " ous " reduced salt as opposed to the " ic " oxidized salt ?[/quote]
...
20-10-2006 at 13:25
by: Hilski
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]This electrolytically regenerated reagent scheme should
also be applicable to other polyvale ...
20-10-2006 at 10:20
by: Hilski
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