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Dehydration of nitric acid with acetic anhydride
There are even nitrations in acetic anhydride - to trap the reaction water so the nitration proceeds ... |
20-7-2023 at 01:58
by: Fery |
1,4-Dioxane from Ethylene Glycol and H2SO4
After that 350 g of the product stayed in 0,5 l bottle for almost 1 year in a fridge at +4C, in the ... |
16-7-2023 at 01:42
by: Fery |
Phthalate Metal Complexes
Well done! The Ni phthalate looks pale green on photos or is it pale blue as you wrote (camera senso ... |
15-7-2023 at 09:49
by: Fery |
Selenium polycations
Bedlasky well done! Beautiful colors! |
11-7-2023 at 12:28
by: Fery |
benzyl methyl ether
I confirm. I opened the bottle and no lachrymation. I will process the methanolic solution further. ... |
4-7-2023 at 02:06
by: Fery |
Dichloromethane ban
I've bought 25 L drum from chemland.pl while it costed 50 EUR about 2 years ago. Now the price is tr ... |
4-7-2023 at 01:49
by: Fery |
Usage of potassium chlorate in organic chemistry
http://www.orgsyn.org/demo.aspx?prep=CV2P0553
http://www.orgsyn.org/demo.aspx?prep=CV3P0042
http:/ ... |
1-7-2023 at 07:16
by: Fery |
Ketamine synthesis work
Well done, great practical skills, a lot of step synthesis with very nice yield !!! Well documented ... |
24-6-2023 at 09:20
by: Fery |
benzyl methyl ether
Anisole did not scent to me pleasant either natural, for me it had some "chemical" scent. Even pheno ... |
24-6-2023 at 03:40
by: Fery |
1,2 dichlorobenzene EU supplier or synthesis
If you have a trip through my country I can share o-dichlorobenzene with you for free. I do not sell ... |
20-6-2023 at 20:49
by: Fery |
Making glacial acetic acid
I let glass bottles with commercial 98% acetic acid in a fridge for few months. The temperature osci ... |
13-6-2023 at 06:30
by: Fery |
Making (propylthio)benzene
I found only this one info with its melting point:
http://www.chemspider.com/Chemical-Structure.128 ... |
12-6-2023 at 19:59
by: Fery |
Making glacial acetic acid
You can also try to approximate its purity by its freezing / melting point. It tends to produce supe ... |
12-6-2023 at 19:49
by: Fery |
Making (propylthio)benzene
Thanks for sharing the synthesis. It is interesting route suitable for home labs as it avoids malodo ... |
11-6-2023 at 21:29
by: Fery |
Synthesis of t-nitrosobutane (w/ pictures)
Bedlasky well done! Nice color!
I found that another compound nitrosobenzene should be green liquid ... |
11-6-2023 at 21:13
by: Fery |
NH4[BF4] synthesis question
Is it necessary to consume almost all the H3BO3 to prevent your product contamination due to H3BO3 l ... |
5-6-2023 at 02:53
by: Fery |
Is pyrrolidine hydrochloride deliquescent, or easy to dry?
Interesting findings! I synthesized freebase and it was easily to dehydrate by solid NaOH, b.p. of p ... |
4-6-2023 at 03:11
by: Fery |
benzyl methyl ether
Yes I have almost 2 L of this nasty stuff. Luckily I found first good usage for me in the ether synt ... |
4-6-2023 at 02:50
by: Fery |
benzyl methyl ether
Figure I in the article posted by kmno4
25 C 0,001 mol KHCO3 / 1 L methanol
45 C 0,006 mol KHCO3 ... |
1-6-2023 at 11:07
by: Fery |
benzyl methyl ether
So I setup this experiment and I let it to stay in summer oscillating temperatures sealed and inside ... |
1-6-2023 at 03:17
by: Fery |
benzyl methyl ether
as you wrote, adding a little of KI should increase the speed of the reaction
BnCl + KI -> BnI w ... |
31-5-2023 at 21:08
by: Fery |
benzyl methyl ether
kmno4 - great idea !!! thx !!!
the researchers synthesized all the ethers at scale of above 10 kg, ... |
31-5-2023 at 12:17
by: Fery |
benzyl methyl ether
Yes Williamson is the way I will have to go. Methanol + NaOH <-> Na methoxide + H2O. Benzyl ch ... |
30-5-2023 at 20:38
by: Fery |
Potassium permanganate from manganese dioxide, potassium hydroxide and potassium chlorate (as oxidising agent).
Hi Keras, well done and perfectly detailed description! Observing that pyro-lava effect must be amaz ... |
30-5-2023 at 10:59
by: Fery |
benzyl methyl ether
Hi Keras, thx for the idea, it is worth to try. This database reports its scent:
http://www.thegood ... |
30-5-2023 at 10:20
by: Fery |
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