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Propositioned by U2U
Aww why didn't I get one of those shady U2Us? I wanted to feel like a cool kid too....  |
11-12-2016 at 02:50
by: Cryolite. |
What could one do with ICl?
Can you get sulfur powder? If so, try burning it and bubbling the produced SO2 through a sodium hydr ... |
28-11-2016 at 12:49
by: Cryolite. |
Solvent drying - molecular sieves
@Bert: As far as I know, those reactions are pretty fast: keto-enol tautomerism is relatively fast a ... |
28-11-2016 at 09:44
by: Cryolite. |
What the hell did I just make?
Na-DCCA is the mono sodium salt of dichlorocyanuric acid. This dichlorocyanuric acid is simply the d ... |
28-11-2016 at 09:27
by: Cryolite. |
Preparation of methyl tosylate, safe methylating agent
I would just like to point out that, while toluenesulfonyl chloride has been difficult for the amate ... |
25-11-2016 at 19:19
by: Cryolite. |
What could one do with ICl?
Iodine monochloride is a very useful electrophillic iodination. It functions as a source of I+, and ... |
24-11-2016 at 11:31
by: Cryolite. |
Anyone interested in purchasing rhodium or ruthenium sponge? Your budget is the limit!
Ruthenium tetroxide is capable of oxidizing ethers to the corresponding diacids. In the case of THF, ... |
23-11-2016 at 13:02
by: Cryolite. |
Copper glycerol jelly ?
I have no idea about the complex, but the acrid whiff you caught was most likely acrolein formed by ... |
17-11-2016 at 13:38
by: Cryolite. |
The Short Questions Thread (4)
I have some guanidine carbonate, but I would like to convert it to (dry) guanidine hydrochloride, fo ... |
31-10-2016 at 18:40
by: Cryolite. |
Secondary amine mannich condensation + ring formation.
[rquote=465015&tid=70391&author=AvBaeyer]There are many well documented ring forming reactio ... |
25-10-2016 at 13:28
by: Cryolite. |
Ethyl Acetate Purification
So, Dean-Stark conditions? |
25-10-2016 at 13:19
by: Cryolite. |
Synthesis of Allylbenzene
I was aware of the tosylhydrazone based reductions, but sodium cyanoborohydride is unobtanium for me ... |
25-10-2016 at 09:30
by: Cryolite. |
Reagent Bottles! (OCD)
I use old instant coffee bottles for solids which can handle a bit of air exposure. (sodium thiosulf ... |
24-10-2016 at 17:13
by: Cryolite. |
Synthesis of Allylbenzene
I wonder why no one has brought up a route from cinnamaldehyde, since the OP mentioned it a a potent ... |
24-10-2016 at 16:14
by: Cryolite. |
Benzaldehyde on Amazon Prime?
I'm guessing they are using Amazon as a way to clear up stock: things that they want sold quickly ge ... |
24-10-2016 at 09:03
by: Cryolite. |
Benzaldehyde on Amazon Prime?
Yep, HiMedia is an actual lab supplier, and they do sell a lot of things through Amazon. If you're w ... |
23-10-2016 at 21:09
by: Cryolite. |
Preparation of Succinic Acid
Could you try ammonium formate or sodium formate as a hydrogen source? I don't think you could have ... |
21-10-2016 at 20:08
by: Cryolite. |
Maths assistance please
3 years is a very long time, but half a milliamp is a minuscule amount of current. If you can guaran ... |
18-10-2016 at 14:46
by: Cryolite. |
Maths assistance please
I believe you are confusing units here. An ampere is a unit of current, but to measure the capacity ... |
18-10-2016 at 13:15
by: Cryolite. |
Pretty Pictures (2)
Iron salicylate is purple too-- maybe add that one in? |
13-10-2016 at 21:59
by: Cryolite. |
Polyphosphoric Acid
From what I remember, copper does technically work, but it turns the acid a dark black color due to ... |
13-10-2016 at 09:38
by: Cryolite. |
Polyphosphoric Acid
A quick warning about dehydrating phosphoric acid: although the process is conceptually simple (just ... |
13-10-2016 at 00:51
by: Cryolite. |
Short question / quick answer - Thread
I recently purchased some dicyandiamide for conversion to tetrazole derivatives. However, I would li ... |
11-10-2016 at 18:38
by: Cryolite. |
Bad days in the lab or with glassware?
I was distilling some benzyl chloride with plastic Keck clips. I shifted the glassware slightly, the ... |
11-10-2016 at 18:15
by: Cryolite. |
thiamine uses
Thiamine can be used as a catalyst in the benzoin condensation. This is lower yielding than the trad ... |
3-10-2016 at 22:32
by: Cryolite. |
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