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Iodination of organic compounds
I still have 10g elemental iodine.
Does anybody know how i could use that for halogenations?
I k ... |
25-6-2003 at 10:53
by: BASF |
Thionyl Chloride Preparation
Hmm. sounds very interesting!
Is this a precipitation-reaction?
Is SOCl2 insoluble in polar solven ... |
20-6-2003 at 06:46
by: BASF |
Where do you experiment ?
It is often difficult to find a good place to release poisonous fumes, spill cooking acid and distin ... |
18-6-2003 at 11:39
by: BASF |
HMX by way of nitration of dpt
The solubility of HMX in acetone is not very good.
But the one of RDX is.  
Acetone has been ... |
10-6-2003 at 09:12
by: BASF |
perpetual motion
Arrgh...tapped into the trap
I didn´t want to express that too complicated, although you´re ... |
10-6-2003 at 09:08
by: BASF |
perpetual motion
Yep. And what adds to the problems vulture mentioned, this would then only be a p.m. of the kind fro ... |
10-6-2003 at 05:13
by: BASF |
HMX by way of nitration of dpt
? however, i was just fascinated by the fact this method works without Ac2O or P2O5...
BTW, i would ... |
10-6-2003 at 05:06
by: BASF |
perpetual motion
Ok, let´s out myself ... there was a time when i was completely amazed by the thought of building a ... |
9-6-2003 at 11:08
by: BASF |
HMX by way of nitration of dpt
Thanks a lot !
5% yield for DPT is not impressive, but it´s science, isn´t it ?
 |
6-6-2003 at 10:01
by: BASF |
new ernergetic materials
[quote]
Good idea BASF!
[/quote]
wow, from the big master. Let´s mark the day red in the c ... |
6-6-2003 at 09:58
by: BASF |
formula for approximation of Trauzl-test
I wondered wether there is a good formula......
Older patents often refer only to Trauzl-test-val ... |
6-6-2003 at 09:24
by: BASF |
HMX by way of nitration of dpt
Surprisingly, i found this ref. on totse...
They have it from "the preparatory manual of exp ... |
4-6-2003 at 10:48
by: BASF |
heat capacity of Sorguyl
Thanks a lot !
- Thats it. I know rough means really rough in this case......thanks for the hint ... |
13-5-2003 at 07:33
by: BASF |
heat capacity of Sorguyl
I´m looking for the value for Cv or Cp for Tetranitroglycoluril, which i need for the calculation o ... |
13-5-2003 at 00:39
by: BASF |
Concentrating H2O2 by electrolysis
yeah, do that.
Be sure to use clean containers and use a water bath, if you like.
For higher conce ... |
8-5-2003 at 07:59
by: BASF |
Concentrating H2O2 by electrolysis
Somewhere in the general chemistry-section is a thread on how to concentrate H2O2.
It is not that d ... |
8-5-2003 at 05:14
by: BASF |
new ernergetic materials
I still prefer realizable ideas. |
8-5-2003 at 04:59
by: BASF |
bromo-RDX?
I wonder wether it would be possible to brominate RDX...
Mild conditions.
The problem is, i know ... |
7-5-2003 at 06:14
by: BASF |
P2O5 by pyrolysis
Hmm, from my point of view it seems possible what you proposed.....
Why copper? i always wondered ... |
7-5-2003 at 05:30
by: BASF |
Zinc + phenol
another possibility:
When the vapours of Phenol are passed over red-hot zinc dust, then reduction ... |
6-5-2003 at 11:08
by: BASF |
P2O5 by pyrolysis
according to the following patent, aluminum metaphosphate can be decomposed at 950-1100°C:
Al3(P ... |
6-5-2003 at 10:23
by: BASF |
resorcinol from salicilic acid?
Another proposal:
1.) protecting the OH-group of phenol by making an ether
1a).a voluminous t ... |
8-4-2003 at 04:50
by: BASF |
Mg + h2o
By the way......want to make a hydrogen-balloon?
The russians solved the task of filling a ... |
8-4-2003 at 03:42
by: BASF |
new ernergetic materials
[quote]
Tetrazole exists, I have 2kg of 5-aminotetrazole. Even on it's own it is quite energet ... |
7-4-2003 at 13:35
by: BASF |
Acetaldehyde, the holy grail-method
BTW, i am at least sure i found formic acid in a product called "WC-Ente" from Henkel for ... |
5-4-2003 at 14:29
by: BASF |
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