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The short questions thread (2)
[rquote=152073&tid=12054&author=Jor]
Maybe my supplier confused and gave me the sulfate.[/r ...
2-5-2009 at 20:39
by: S.C. Wack
Sodium peroxymonosulfate
That may depend on concentration.
http://v3.espacenet.com/publicationDetails/originalDocument?CC=GB ...
19-4-2009 at 06:28
by: S.C. Wack
Zinc in brass does not react with acids?
You would want the older type of battery, for zinc, if they are still sold there. These are the ones ...
14-4-2009 at 14:11
by: S.C. Wack
strange (?) results from nitrating toluene
I have not found the reaction to require more than a very slight excess of toluene. Or end up black. ...
14-4-2009 at 13:43
by: S.C. Wack
Reduction of arsenic pentoxide? What is the best method?
Other people seem to be happy with reduction with As+3. Here they use warm very conc. HCl with their ...
9-4-2009 at 14:36
by: S.C. Wack
Reduction of arsenic pentoxide? What is the best method?
There do seem to be some wet methods in the old literature, at least as sensitive tests, don't know ...
9-4-2009 at 03:02
by: S.C. Wack
Lab Prep of Diethyl Sulfate
Both article and patent mention [url=http://v3.espacenet.com/publicationDetails/originalDocument?CC= ...
7-4-2009 at 14:18
by: S.C. Wack
Lab Prep of Diethyl Sulfate
This patent is similar and utilizes the well-known reaction of bisulfate with alcohol.
http://v3.es ...
7-4-2009 at 03:03
by: S.C. Wack
tin salts thread
Relevant: http://books.google.com/books?id=kuZ8fvczfZoC&pg=PA216

The amount of cyanide used t ...
4-4-2009 at 22:28
by: S.C. Wack
Preparation of anthranilic acid
I was wrong on the number of references; I forgot about the patent, and the Russian article.

The ...
31-3-2009 at 14:49
by: S.C. Wack
Preparation of anthranilic acid
It has been made from o-nitrotoluene 3 times in the literature, but with NaOH or KOH, and the yield ...
31-3-2009 at 03:05
by: S.C. Wack
Parrafin
http://books.google.com/books?id=inIGAQAAIAAJ&pg=PA209
26-3-2009 at 21:23
by: S.C. Wack
Preparation of cyanides
[quote][i]Originally posted by len1[/i]
Thanks for the info SC Wack. But none of the links work. ...
24-2-2009 at 03:59
by: S.C. Wack
Preparation of cyanides
I'm sure people will be giving that a try now.

----

There are many places where one can find a ...
23-2-2009 at 18:35
by: S.C. Wack
Something Else to Do with Your Red P
BTW Gmelin's (up to 1960) quite unsurprisingly says nothing more about the reaction of PX3 with Cl, ...
23-2-2009 at 18:00
by: S.C. Wack
Phosphorus Chlorides
I scanned Gmelin's on the preparation of PCl3, PCl5, and the inorganic reactions of PCl5, because so ...
21-2-2009 at 17:39
by: S.C. Wack
PBr3 -> PCl3 "New" Old Method
[quote][i]Originally posted by Sauron[/i]
I do not know where (or if) I can lay hands on Philosophi ...
18-2-2009 at 19:56
by: S.C. Wack
Something Else to Do with Your Red P
It was suggested to me that I read this thread again, and I guess I have just a little more that I c ...
16-2-2009 at 20:29
by: S.C. Wack
CRC Handbook Editions
No one downloads anything from gigapedia ever - they host nothing but URL's. Anyone afraid of gmail ...
15-2-2009 at 16:37
by: S.C. Wack
CRC Handbook Editions
You'll find the electronic CRC's at ebook sites like gigapedia (which I despise since people bury an ...
15-2-2009 at 09:17
by: S.C. Wack
Something Else to Do with Your Red P
[quote][i]Originally posted by Sauron[/i]
I am trying to find p 489.[/quote]

My link doesn't go ...
12-2-2009 at 15:29
by: S.C. Wack
Something Else to Do with Your Red P
I did not post a link because I already downloaded it some time ago and figured that anyone could fi ...
12-2-2009 at 04:10
by: S.C. Wack
Something Else to Do with Your Red P
[quote][i]Originally posted by Sauron[/i]
I have unearthed a lot of ways to make POCl3 but unfortun ...
11-2-2009 at 19:00
by: S.C. Wack
CRC Handbook Editions
Well if you love the 35th ed, you'd really love the one I use, 1939's 23rd, which sold for $3.50 at ...
11-2-2009 at 18:32
by: S.C. Wack
Highly concentrated H2O2 by extraction with CCl2H2
Well, continuing with the ether thing, it may also be possible with lower concentrations of peroxide ...
8-2-2009 at 16:46
by: S.C. Wack
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