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Preparation of anthranilic acid
[rquote=156690&tid=10272&author=crazyboy]what about o-xylene to phthalic acid[/rquote]

If ...
12-7-2009 at 14:28
by: S.C. Wack
Poll: Is there too much illegal drug discussion?
The problem is of course people with no actual interest or understanding of chemistry who post anywa ...
12-7-2009 at 09:08
by: S.C. Wack
Mandatory Home Inspections Under Climate Bill
Yeah well the House passes stuff all the time that never becomes law.

Funny how this widely quote ...
6-7-2009 at 17:34
by: S.C. Wack
Acetic acid/ sodium hydroxide
Vacuum crystallization:
[url=http://v3.espacenet.com/publicationDetails/originalDocument?CC=US& ...
5-7-2009 at 15:03
by: S.C. Wack
Synthesis of polychromates
A very old HNO3-less route that I noticed while going through my papers...probably have this in Engl ...
5-7-2009 at 13:55
by: S.C. Wack
Preparation of anthranilic acid
Well I see that espacenet only supports full (very long) urls now. Nice of them to change that. Do t ...
5-7-2009 at 11:15
by: S.C. Wack
Making Lithium Metal
Repost of the above by request.

http://ifile.it/skohwq0
4-7-2009 at 11:57
by: S.C. Wack
Adios
[rquote=156593&tid=12469&author=Sauron]I am weary of the arbitrary and petty tyranny of some ...
4-7-2009 at 11:38
by: S.C. Wack
Benzene synthesis
Benzene rich oil by the decarboxylation of PET
http://staff.aist.go.jp/tohru-kamo/FSRJ/output/7_nen ...
29-6-2009 at 11:40
by: S.C. Wack
fractional distillation
elements_of_fractional_distillation_by_robinson_1950.djvu
http://ifile.it/93jyo6p

handbook_of_l ...
24-6-2009 at 12:05
by: S.C. Wack
fractional distillation
I have to wonder how many CAREFUL fractionations that the people arguing against lagging have done. ...
23-6-2009 at 18:46
by: S.C. Wack
Acetamide from sodium acetate and ammonium sulfate
It works in France, with chlorides.
http://ifile.it/xp31ywt

The yields here are higher than clai ...
20-6-2009 at 14:21
by: S.C. Wack
Old Spectrophotometer Manuals - 21D
The manual is for the Spectronic 21 and covers the family.

Would a .pdf be cool?

I have a 21D ...
1-6-2009 at 14:28
by: S.C. Wack
The short questions thread (2)
http://dx.doi.org/10.1021/ja01343a024
31-5-2009 at 15:07
by: S.C. Wack
Propionic Acid through MEK haloform?
A couple hundred grams is not a daunting chore, many small reactions typical of chloroform preparati ...
31-5-2009 at 12:24
by: S.C. Wack
Ferricyanide precipitation?
I'm aware of an investigation
http://dx.doi.org/10.1002/zaac.19130840116
With several different ou ...
30-5-2009 at 07:54
by: S.C. Wack
CS2 a Different Way
[rquote=153743&tid=12267&author=Sauron]There's a procedure for dehydrating sodium sulfate no ...
27-5-2009 at 20:24
by: S.C. Wack
CS2 a Different Way
[rquote=153739&tid=12267&author=garage chemist]Aqueous K2S will always be an equilibrium mix ...
27-5-2009 at 18:14
by: S.C. Wack
CS2 a Different Way
[rquote=153656&tid=12267&author=Sauron]If anyone wants to know why you can't just bubble H2S ...
27-5-2009 at 17:26
by: S.C. Wack
Controlled Bacterial Nitrification (salpeter production, using nitrosomonas etc)
I see that the <1 MB pdf attachment on my last post has disappeared somehow. That's not a good si ...
24-5-2009 at 13:41
by: S.C. Wack
How much mercury is in a sphygmomanometer?
Average of several old discarded Baumanometers, after extensive cleanup: 107.5 g.

EDIT:
Since th ...
23-5-2009 at 13:13
by: S.C. Wack
CS2 a Different Way
http://dx.doi.org/10.1039/JR9280002068
21-5-2009 at 18:03
by: S.C. Wack
toluene --> benzaldehyde
Regarding t-butyl hypochlorite:

http://www.sciencemadness.org/talk/viewthread.php?tid=1896&pa ...
21-5-2009 at 03:08
by: S.C. Wack
The short questions thread (2)
A way to avoid an iodine clock reaction is hot aq. oxalic acid. It works.

[Edited on 16-5-2009 by S ...
16-5-2009 at 12:29
by: S.C. Wack
Disposal of (old) THF Still
I've used 70-100% IPA to decompose excess sodium many times, the reaction is very mild at STP for me ...
13-5-2009 at 10:54
by: S.C. Wack
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