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Easy synthesis of hydroiodic acid
In water, acid strength is not meaningful below pKa -1.6 or so. So while H2SO4, HCl, HBr, HClO4, and ...
7-1-2019 at 22:11
by: clearly_not_atara
An economical chain of experiments?
[rquote=578691&tid=125642&author=XeonTheMGPony][rquote=578621&tid=125642&author=itsa ...
7-1-2019 at 18:28
by: clearly_not_atara
Mom-and-pop lemonade-stand-style ways to make quick legal cash from chemistry
Perhaps you could sell lemonade? I've heard of people drinking "chemist's lemonade" which generally ...
7-1-2019 at 18:20
by: clearly_not_atara
Recent bromine synth
[rquote=578632&tid=125230&author=MrHomeScientist]This is a good lesson in safety. XeonTheMGP ...
7-1-2019 at 15:59
by: clearly_not_atara
Easy synthesis of hydroiodic acid
Don't you already have an iodide salt? It's not even clear why oxalate is involved in that process a ...
7-1-2019 at 13:34
by: clearly_not_atara
Easy synthesis of hydroiodic acid
HI reacts with ascorbic acid to make iodoalkanes. That's probably what you smelled.

I do not rec ...
7-1-2019 at 12:10
by: clearly_not_atara
Nicotinamide dehydration
There are some cases where amide -> nitrile happens with excess MeCN and a transition metal catal ...
6-1-2019 at 19:45
by: clearly_not_atara
How to scrub ethyl acetate vapors before releasing into the outside air? Hundreds of neighbors are complaining.
Actually one thing that should work pretty well is venting the exhaust through a big container of a ...
4-1-2019 at 16:50
by: clearly_not_atara
Tryptamine Isolation (HELP!!!)
Indole is unstable and will always partially decompose when refluxed under air. Those colors are dec ...
3-1-2019 at 13:48
by: clearly_not_atara
Easy synthesis of hydroiodic acid
[rquote=571933&tid=120001&author=Felab][Phosphoric acid is] what's normaly used but I don't ...
3-1-2019 at 13:35
by: clearly_not_atara
KOH
OP is interested in drying his KOH, not making it.

I think you might be able to dry it by heating ...
3-1-2019 at 12:45
by: clearly_not_atara
How to scrub ethyl acetate vapors before releasing into the outside air? Hundreds of neighbors are complaining.
Consider using different solvents? I'd be surprised if ethyl acetate were causing these problems but ...
3-1-2019 at 09:47
by: clearly_not_atara
Sensitive substance from fiction?
[quote] Or, if the glass can be shattered by resonance that could also detonate the nitroglycerine ? ...
26-12-2018 at 20:20
by: clearly_not_atara
What is the best way to go about making a nonacidic aluminum chloride solution (for an antiperspirant)?
Yeah I don't know why you'd intentionally put aluminium in your deodorant. Smelling is bad, sweating ...
23-12-2018 at 10:36
by: clearly_not_atara
Removing BrCl from Bromine
[b]unionised[/b] has a very good idea about using NaBr as the reducing agent. I think this is the wa ...
23-12-2018 at 00:17
by: clearly_not_atara
Question about h2s and phosphine
[quote]A weak oxidant reacting with excess of PH3 might be selective for reasons of mechanism, and p ...
22-12-2018 at 22:25
by: clearly_not_atara
Removing BrCl from Bromine
Sulfuryl chloride exists, but sulfuryl bromide does not, so maybe you can reduce the BrCl with SO2?
...
20-12-2018 at 21:22
by: clearly_not_atara
synthesis of 2-bromobenzoyl chloride
Haha, you're not trying to make benzos. You're interested in open-chain benzo analogs optimized for ...
19-12-2018 at 12:35
by: clearly_not_atara
Removing fishy smell from air - possible?
As long as we're producing acidic gases I'd guess releasing a small amount of SO2 would kill the fis ...
19-12-2018 at 11:59
by: clearly_not_atara
synthesis of 2-bromobenzoyl chloride
I think it would be better to use 2-bromobenzonitrile and p-chloroaniline together in a Sugasawa rea ...
19-12-2018 at 11:12
by: clearly_not_atara
Would it be possible to make 2-bromobenzoyl chloride from salicylic acid
The answer is probably not unless you can use Tf2O or chlorodiphenylimidazolium.
19-12-2018 at 10:44
by: clearly_not_atara
LiAlH4 vs NaAlH4
If it didn't produce any vapor there wouldn't be a flash point:

http://www.stanhope-seta.co.uk/fp ...
18-12-2018 at 23:56
by: clearly_not_atara
LiAlH4 vs NaAlH4
If I had to guess NaAlH4 is more reactive, which is probably annoying because LiAlH4 is already too ...
18-12-2018 at 20:50
by: clearly_not_atara
Demethylation of Vanillin and Eugenol
You could probably do it with all sorts of things. Particularly, the rxn is known to work with no DI ...
18-12-2018 at 11:26
by: clearly_not_atara
Demethylation of Vanillin and Eugenol
DIC in that article stands for what I expected, diisopropylcarbodiimide.

https://www.sciencedirec ...
17-12-2018 at 21:16
by: clearly_not_atara
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