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Did I accidently make Titanium tetrachloride?
I guess you are doing this in a reflux setup, you could put a drying tube on top and let it go for h ...
27-11-2019 at 23:34
by: Tsjerk
Did I accidently make Titanium tetrachloride?
TiI4 and water form HI which fumes and smells like HCl.

I would try again in dry xylene, excess t ...
27-11-2019 at 23:17
by: Tsjerk
Report on making Manganese Iodide MnI2
The end point equilibrium (water content in compound A vs. compound B) will be the same whether you ...
27-11-2019 at 08:54
by: Tsjerk
Report on making Manganese Iodide MnI2
[rquote=626858&tid=154483&author=Sulaiman][rquote=626792&tid=154483&author=Lion850]I ...
26-11-2019 at 10:55
by: Tsjerk
Report on making Manganese Iodide MnI2
[rquote=626813&tid=154483&author=Lion850]

Tsjerk it did not work in xylene; I do not know ...
26-11-2019 at 03:32
by: Tsjerk
Report on making Manganese Iodide MnI2
What about the solubility of MnI2 in for example ethanol or acetone? Maybe you get a more fine preci ...
25-11-2019 at 23:53
by: Tsjerk
Blacklight as a light source for chlorination?
What about uv-c LED?

A random site I found :

https://www.ledwv.com/uv/uvc-leds-c-31.html?gclid ...
21-11-2019 at 05:55
by: Tsjerk
Ammonium formate from Ammonium chloride
[rquote=626436&tid=154078&author=B.D.E]. I decided just pouring it to a crystalizing dish an ...
20-11-2019 at 23:02
by: Tsjerk
Do NH4OH and S React?
The ammonia sulfur styrene reaction is done in a pressure chamber to be able to heat it enough to ge ...
20-11-2019 at 07:58
by: Tsjerk
Python
The Udemy beginner courses I know all start with a section on what software to install and how to co ...
20-11-2019 at 00:13
by: Tsjerk
Ammonium formate from Ammonium chloride
Toluene will just give you a two phase system, nothing in your mixture is miscible with it.
19-11-2019 at 07:24
by: Tsjerk
Python
I like udemy.com, courses usually are 13 Euro, but you can get your money back within 30 days if you ...
18-11-2019 at 23:36
by: Tsjerk
Ammonium formate from Ammonium chloride
How do you generate ammonia from ammonium chloride? Mixing the chloride with excess NaOH and slowly ...
18-11-2019 at 23:18
by: Tsjerk
Troubleshooting Zn/HCl reduction of nitrostyrenes
I did this reaction on 2,5-DMNS in methanol and with concentrated HCl. I dissolved the styrene in me ...
14-11-2019 at 04:41
by: Tsjerk
How to synthesise Sulfosalicylic acid
Did you try to crystallize from cold saturated brine as Hexavalent did in 2013?

I do wonder how h ...
13-11-2019 at 11:06
by: Tsjerk
Glycated hemoglobin, HbA1c levels
[rquote=625693&tid=154249&author=wg48temp9]

On a vaguely related subject I had an appoint ...
8-11-2019 at 04:25
by: Tsjerk
What's the minimum concentration for h2so4 to be oxidising?
[rquote=625553&tid=154276&author=artemov]Sorry, just to tack on this thread ... what about t ...
6-11-2019 at 06:40
by: Tsjerk
Tungsten metal plus piranha solution?
How would hydrogen peroxide be reducing? I can only imagine it being oxidized by something like fluo ...
3-11-2019 at 04:01
by: Tsjerk
How to verify/identify sodium azide?
Both sodium azide and nitrite are colorless powders. For some reason colorless lead nitrate and sodi ...
1-11-2019 at 13:47
by: Tsjerk
DCM shrinks genuine coke bottle.
I usually get glass bottles with a ptfe liner. I don't know what the cap is made off.
28-10-2019 at 13:22
by: Tsjerk
How to kill or at least repel or block ants?
I just ordered some precursors to make difluorodiphenyltrichloroethane, the fluor analog of DDT. I w ...
28-10-2019 at 02:07
by: Tsjerk
Why does the site log me out frequently?
When I get logged out I usually log in. Get over it. The current software is shit, and the forum has ...
27-10-2019 at 13:41
by: Tsjerk
Preparation of ammonium azide
Can you prepare or get barium/calcium azide? With sulfuric acid that will give a solution of hydrazo ...
24-10-2019 at 10:17
by: Tsjerk
So what actually are not allowed in whimsy?
I like to answer Yttrium's most silly question way, way more than ignoring fusso's ignorance.

[Edi ...
13-10-2019 at 09:11
by: Tsjerk
Burnt hotplate cord
You could cut out the damaged part and reconnect the wires with something like [url=https://www.goo ...
8-10-2019 at 03:50
by: Tsjerk
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