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Diethylamine Hydrochloride Synthesis
I'm giving this a try with 5 mL DEET and 4.4 mL azeotropic HCl.
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13-8-2017 at 20:17
by: JJay |
benzyl alcohol oxidation
Oh, no, it's ok... I certainly don't know everything, but I'm not as ignorant as I appear 
If I ... |
13-8-2017 at 19:23
by: JJay |
benzyl alcohol oxidation
I've oxidized Cr+3 to Cr+6 at high pH, so I'm not really sure what you're getting at. I don't think ... |
13-8-2017 at 11:18
by: JJay |
benzyl alcohol oxidation
Isn't there more to oxidizer strength than electrode potential, though? Dichromate has lower electro ... |
13-8-2017 at 10:14
by: JJay |
benzyl alcohol oxidation
Hmm... I had thought hypochlorite was a stronger oxidizer than almost anything except hydrogen perox ... |
13-8-2017 at 09:23
by: JJay |
benzyl alcohol oxidation
That's kind of interesting. I have never tried making benzaldehyde, but I suspect the process is rat ... |
13-8-2017 at 06:06
by: JJay |
When Chemistry Goes Wrong
Oh, and I was distilling some benzyl alcohol earlier and managed to melt a screw cap by heating the ... |
13-8-2017 at 03:34
by: JJay |
When Chemistry Goes Wrong
If I'd accidentally made benzene a couple of years ago I would have been overjoyed, but the same thi ... |
13-8-2017 at 03:12
by: JJay |
Tour My Lab
I see. I have a bag of a dozen boss heads that I've been meaning to use to put together a frame, but ... |
12-8-2017 at 23:09
by: JJay |
stainless steel still and calcium acetate
Calcium acetate probably not, but the calcium carbonate that will be formed can attack glass at high ... |
12-8-2017 at 20:14
by: JJay |
New to Forum/Questions about the synthesis of Butyramide
There are lots of ways to make it; most involve reacting a derivative of butyric acid with ammonia. ... |
12-8-2017 at 04:03
by: JJay |
The Short Questions Thread (4)
[rquote=490238&tid=25055&author=Ramium]Thank for the respones.
Oh yeah your right, forgo ... |
12-8-2017 at 03:41
by: JJay |
new toys
Nice. Those diaphragm pumps definitely have their uses. |
11-8-2017 at 19:45
by: JJay |
Geosmin synthesis
[rquote=490217&tid=76101&author=zts16]
As for diethylamine HCl, the best method in an amate ... |
11-8-2017 at 07:38
by: JJay |
Ammonium acetate
Oh, and I should probably mention that I finally found a paper that detected decomposition at just a ... |
11-8-2017 at 05:42
by: JJay |
The Short Questions Thread (4)
Hydration of styrene would typically result in 1-phenylethanol. You'd have to demethylate it somehow ... |
11-8-2017 at 03:27
by: JJay |
Mercury thermometer broke, and fell into methyl iodide boiling flask. How concerned should I be?
What is the best way to neutralize something like that? Concentrated sodium thiosulfate? |
10-8-2017 at 17:19
by: JJay |
Sodium Ethyl Sulfate
I've read that it takes days for ethylsulfuric acid to hydrolyze in water at room temperature. I'm n ... |
10-8-2017 at 10:55
by: JJay |
Sodium Ethyl Sulfate
There is an equilibrium between ethanol + sulfuric acid and ethyl sulfuric acid + water. The reactio ... |
10-8-2017 at 09:32
by: JJay |
Sodium Ethyl Sulfate
The higher the yield, the less impurities you have to eliminate. The starting materials are cheap. |
10-8-2017 at 07:45
by: JJay |
Testing for presence of chromium
There was quite a bit of discussion on that on this thread: http://www.sciencemadness.org/talk/viewt ... |
10-8-2017 at 06:54
by: JJay |
Sodium Ethyl Sulfate
I did some more research on it, and it looks like the highest yields are possible by just heating eq ... |
10-8-2017 at 06:27
by: JJay |
Leaking stopcocks
Not yet, but I'll let you know when I do. |
10-8-2017 at 04:47
by: JJay |
Leaking stopcocks
Oh, that reminds me... I cleaned the grease off of my addition funnel and tried the bedding in proce ... |
10-8-2017 at 04:20
by: JJay |
When Chemistry Goes Wrong
[rquote=490072&tid=63645&author=nitro-genes]Also had an incident with an ammonia generator u ... |
9-8-2017 at 22:32
by: JJay |
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