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Anhydrous AlCl3 attempt
Ohh yeah, Cl2 is the worst, you can't tell you're breathing it after a while, at least HCl alerts yo ... |
28-8-2010 at 03:30
by: spong |
Anhydrous AlCl3 attempt
I had another try with a glass reactor tube and a CO2 generator to push the AlCl3 vapour through the ... |
28-8-2010 at 02:47
by: spong |
Anhydrous AlCl3 attempt
Ohh yeah sorry about that, if someone could merge this thread with chainhit's that'd be great 
Ye ... |
26-8-2010 at 01:45
by: spong |
Anhydrous AlCl3 attempt
I was a bit worried about the chlorine but I didn't expect that, I was a more afraid of the hydrogen ... |
25-8-2010 at 05:27
by: spong |
Anhydrous AlCl3 attempt
After seeing chainhit's [url=http://www.sciencemadness.org/talk/viewthread.php?tid=14224]thread [/ur ... |
24-8-2010 at 23:42
by: spong |
Australians: spare toluene and methanol
Yeah that is a good point, I remember a few years ago I saw plenty of tins of toluene in bunnings. N ... |
23-8-2010 at 23:29
by: spong |
Australians: spare toluene and methanol
Hi, I've got 20L of both toluene and methanol and I really don't need that much, I'm also a bit worr ... |
23-8-2010 at 01:10
by: spong |
Laboratory Tips and Tricks
If you're distilling something that would usually attack the rubber seals on ordinary thermometer ad ... |
19-8-2010 at 00:55
by: spong |
p-hydroxybenzaldehyde?
I'd still get an odd look from the chem supplier, they always assume I'm making either drugs of expl ... |
18-8-2010 at 03:51
by: spong |
p-hydroxybenzaldehyde?
I don't have access to phenol in Australia unfortunately so the Riemer-Tiemann route is out, as well ... |
18-8-2010 at 00:54
by: spong |
p-hydroxybenzaldehyde?
Wouldn't p-cresol be pretty sensitive to oxidation? |
17-8-2010 at 03:59
by: spong |
Preparation of elemental phosphorus
[rquote=181383&tid=65&author=Random]I am interested in getting red phosphorus from matchboxe ... |
16-8-2010 at 19:44
by: spong |
p-hydroxybenzaldehyde?
I was after the hydroxy benzaldehyde but demethylating the methoxy shouldn't be too bad, thanks :coo ... |
16-8-2010 at 19:31
by: spong |
p-hydroxybenzaldehyde?
Hi
I'm wanting to one day make some raspberry ketone but first I'll need some p-hydroxybenzalde ... |
16-8-2010 at 18:21
by: spong |
Anhydrous Aluminum Chloride prepration
Ohh I see, well that would probably be better than using such a large amount of AlCl3 on the Gatterm ... |
13-8-2010 at 16:29
by: spong |
Anhydrous Aluminum Chloride prepration
In Organic Reactions v5 (from the library section) it says "An industrial grade of aluminum chloride ... |
13-8-2010 at 04:50
by: spong |
Weird bromine contaminant
Ohh yes that would explain it, I used salt, ice and water pumped from the foam box the bromine flask ... |
11-8-2010 at 05:56
by: spong |
Weird bromine contaminant
I went out to then and it was gone, there's nothing but bromine fumes in there. I couldn't see the c ... |
11-8-2010 at 05:17
by: spong |
Weird bromine contaminant
I thought it could have been water or ice but when I first distilled it I had a problem with suckbac ... |
11-8-2010 at 03:21
by: spong |
Weird bromine contaminant
Hi I made some bromine yesterday by bubbling chlorine through KBr solution, I
distilled it today ... |
11-8-2010 at 01:50
by: spong |
Uranium
If you want to make it from ore, have a look here, it's only the first step as they haven't complete ... |
28-7-2010 at 03:37
by: spong |
Anhydrous Aluminum Chloride prepration
Wow that's a really good setup, even if the yields aren't the best who cares, it costs a few dollars ... |
28-7-2010 at 03:08
by: spong |
Yellow impurity in nitrobenzene?
Gosh I'd probably have loads of dinitrobenzene if you got that much. I'll try distilling it under th ... |
14-7-2010 at 17:14
by: spong |
Yellow impurity in nitrobenzene?
Well the second time I distilled the benzene I was drying it but it still remained cloudy, I used Ca ... |
13-7-2010 at 17:48
by: spong |
Yellow impurity in nitrobenzene?
Ahh yes dinitrobenzene would make sense as I accidentally let the temperature get to about 80*C when ... |
13-7-2010 at 16:58
by: spong |
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