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Alkali nitrite salt (home production, purification via esterification)
If you don't have nitric acid but have a nitrate salt, you can use HCl and H2O2 instead:

2HCl(aq) ...
3-3-2018 at 23:18
by: ninhydric1
Would you invest in a stirrer hot plate as a noob, or just start with a regular hot plate?
I have a 0.01 g balance and that is good for most purposes. If your doing microchemistry, a 0.001 g ...
26-2-2018 at 13:22
by: ninhydric1
The Short Questions Thread (4)
https://www.ebay.com/itm/10-30g-Natural-Powdered-Cinnabar-Pigment-Powder-Evil-Talisman-Taoists-New/1 ...
25-2-2018 at 21:44
by: ninhydric1
Distilling vinegar - removing water before AA passes over?
I ought to try it then. Getting GAA without distilling acetic acid itself would be relatively simple ...
25-2-2018 at 16:50
by: ninhydric1
Can i generate lead carbonate using lead electrodes on a sodium bicarbonate cell?
I feel like either dissolving lead in acetic acid/H2O2 then using a carbonate salt to precipitate it ...
24-2-2018 at 17:28
by: ninhydric1
Distilling vinegar - removing water before AA passes over?
Sedit I assume any nonpolar solvent would work for the procedure you mentioned?
I don't have a lot ...
24-2-2018 at 17:25
by: ninhydric1
Magnetic Carbon?
The flask reminds me of a 600 mL beaker that I broke while washing. The whole bottom just fell out, ...
22-2-2018 at 17:55
by: ninhydric1
Short question / quick answer - Thread
The hydrogen on the hydroxyl group of phenol is slightly acidic due to the electron delocalization o ...
22-2-2018 at 17:54
by: ninhydric1
Dissolving titanium metal/dioxide
While doing research on titanium dioxide nanoparticles I was looking for a way to make TiCl4 from Ti ...
22-2-2018 at 17:50
by: ninhydric1
Remotely monitored distillations using a Pi
It would be handy if we could set this up so that when the distillation reaches a certain temperatur ...
16-2-2018 at 16:50
by: ninhydric1
Processing BaSO4 to either carbonate or sulfide
Nope, your sodium carbonate and carbon reaction was never thermodynamically favorable.

G=H-TS (wi ...
16-2-2018 at 10:25
by: ninhydric1
Processing BaSO4 to either carbonate or sulfide
BaSO4 (s) <--> Ba2+(aq) + (SO4)2-(aq)

Ba2+(aq) + (CO3)2- (aq) --> BaCO3 (s)

If BaSO4 ...
16-2-2018 at 08:01
by: ninhydric1
Processing BaSO4 to either carbonate or sulfide
RawWork, I don't think you understand what OP is trying to do. OP wants to convert BaSO4 to other sa ...
15-2-2018 at 21:12
by: ninhydric1
The Short Questions Thread (4)
Thanks, JJay. I should use a fake email for this, good idea.
15-2-2018 at 16:47
by: ninhydric1
Processing BaSO4 to either carbonate or sulfide
I would go with the carbon reduction method, simply because you wouldn't introduce cationic contamin ...
15-2-2018 at 07:52
by: ninhydric1
Questions regarding NaHSO3 synthesis
There is a brand of stump remover that isn't KNO3 but sodium metabisulfite, and I feel like sodium m ...
14-2-2018 at 15:33
by: ninhydric1
Do you think it is immoral to steal chemicals and equipment?
[rquote=507308&tid=80462&author=Melgar]In high school once, there was potassium nitrate solu ...
13-2-2018 at 18:51
by: ninhydric1
triphosgene
1 L of DMC for $30 on Amazon:
https://www.amazon.com/MG-Chemicals-Dimethyl-Carbonate-Metal/dp/B06XS ...
8-2-2018 at 18:40
by: ninhydric1
Carbamazepine Synthesis
There is a phosgene-less synthesis I found that uses MeOH and CO2 with KOMe as a catalyst in the pre ...
7-2-2018 at 22:09
by: ninhydric1
Found some Fisher Chems locally - how are these prices?
I feel like these are overkill for a home lab. Unless you have a GC/MS (some people do), these are w ...
7-2-2018 at 17:39
by: ninhydric1
Are you procedural or model driven?
[rquote=506440&tid=80295&author=aga]Which one is alcohol and which one is money ?[/rquote]
...
7-2-2018 at 17:36
by: ninhydric1
Please replace your passwords-
[rquote=506488&tid=80372&author=j_sum1]qwertyuiop[ is your new friend if you want a truly ra ...
7-2-2018 at 17:34
by: ninhydric1
Carbamazepine Synthesis
This is supposed to be in Beginnings.

https://commons.wikimedia.org/wiki/File:Carbamazepine_syn.p ...
7-2-2018 at 17:28
by: ninhydric1
Are you procedural or model driven?
The feel like I am both; I use a procedure as the foundation of my experimentation, then build my ow ...
7-2-2018 at 11:34
by: ninhydric1
Dealing with NO2 fume residues in vessels.
Cody's Lab has tried that in one of his silver metal refining videos, but the problem is silver cata ...
7-2-2018 at 08:46
by: ninhydric1
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