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An attempt at making Phorone
Very cool! This can be used as a precursor for TEMPO which is a very useful oxidizing catalyst. Ther ... |
12-1-2021 at 16:10
by: mr_bovinejony |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
They sure are cheap but I cant find a supplier! The patents are mostly gibberish but from what I cou ... |
3-1-2021 at 10:25
by: mr_bovinejony |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
What's your plan for this methyl 2 azidoacetate? I forgot to tell you I had bought some ortho vanill ... |
3-1-2021 at 09:56
by: mr_bovinejony |
Gamma Amino Butanal from GABA
I have nothing to add but I'm interested in this reaction too for 4-chlorobutanal. Could the amine b ... |
2-1-2021 at 15:00
by: mr_bovinejony |
Halosaccharins
Yeah the iodine compound was just a fun exercise since I had never made elemental iodine before.
... |
22-12-2020 at 15:01
by: mr_bovinejony |
Acid Chlorides
Cyanuric chloride is kinda shitty to work with. I've had two volcanoes so far but I think the third ... |
22-12-2020 at 09:18
by: mr_bovinejony |
Halosaccharins
I got my saccharin today so I ran some trials. Heres the specifics
3 beakers each with 10.25 g of ... |
21-12-2020 at 16:42
by: mr_bovinejony |
Halosaccharins
I had planned on trying the finkelstein reaction to make some iodine compound, but I do have some si ... |
14-12-2020 at 11:38
by: mr_bovinejony |
Halosaccharins
Yeah you sent that paper, but after finding saccharin for very cheap I decided to look more into it. ... |
13-12-2020 at 15:54
by: mr_bovinejony |
Halosaccharins
I've never had that issue with NBS i think, or if I did it was simple enough to remove. But the idea ... |
13-12-2020 at 15:33
by: mr_bovinejony |
Halosaccharins
I have heard about these halo saccharin compounds a few weeks back but hadn't really looked into the ... |
13-12-2020 at 14:43
by: mr_bovinejony |
Acid Chlorides
For the synthesis of acid chlorides from cyanuric chloride, are acetone and triethylamine absolutely ... |
2-12-2020 at 10:13
by: mr_bovinejony |
Nitriles and aldehydes from amino acids and bromosuccinimide
Yeah I had started my search after reading the post about the dcca method. I had found two of these ... |
28-11-2020 at 06:41
by: mr_bovinejony |
Nitriles and aldehydes from amino acids and bromosuccinimide
Here are 3 papers explaining this route but I need some help understanding what products are being f ... |
27-11-2020 at 15:22
by: mr_bovinejony |
Otc oxalyl chloride success?
Well I know for next time I need to use way more hcl gas, and probably keep the heat on a bit so it ... |
21-11-2020 at 12:18
by: mr_bovinejony |
Otc oxalyl chloride success?
Oh I meant oxalic acid, I would think that because its barely soluble in the Acetonitrile it didn't ... |
21-11-2020 at 07:17
by: mr_bovinejony |
Otc oxalyl chloride success?
The problem is that the amount of oxalic acid that was not in solution was overwhelming, if there w ... |
21-11-2020 at 06:53
by: mr_bovinejony |
Otc oxalyl chloride success?
I've only had bad experiences with halogens and dmso, my wife could smell the shit 3 days after it ... |
20-11-2020 at 11:18
by: mr_bovinejony |
Otc oxalyl chloride success?
Oxalic acid is soluble in dmso? I'll try a few tests with it and Acetonitrile |
20-11-2020 at 10:58
by: mr_bovinejony |
Otc oxalyl chloride success?
Let me preface this by saying like most preparations in my lab, this one was done half assed and hal ... |
20-11-2020 at 10:14
by: mr_bovinejony |
Acid Chlorides
Ah for fucks sake! Well we at least know acetyl chloride is doable thanks to chemplayer. I'm going t ... |
16-11-2020 at 08:25
by: mr_bovinejony |
Acid Chlorides
https://onlinelibrary.wiley.com/doi/10.1002/9780470771273.ch2
Check this out. I'm not sure where ... |
15-11-2020 at 21:51
by: mr_bovinejony |
Acid Chlorides
Has anyone tried to use n chloro saccharin with oxalic acid? In this paper here
https://jpharmsci. ... |
15-11-2020 at 16:45
by: mr_bovinejony |
Decarboxylation of L-tryptophan in DMSO
That's strange that you have a red oil, have you tried doing some hexane or naphtha pulls on it for ... |
13-11-2020 at 07:44
by: mr_bovinejony |
Decarboxylation of L-tryptophan in DMSO
Well that's a new one, I've always seen it extracted with portions of acid, never seen the whole mix ... |
11-11-2020 at 09:52
by: mr_bovinejony |
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