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Dimethyl Sulfate, cheapest preparation, OTC !
Hi guys !

Chemistry is the science when always is a way to synthesis wanted chemical in cheaper w ...
20-12-2010 at 06:08
by: mario840
Thiosemicarbazide Synthesis
look at this, easy synth, no refluxing for such a long time, use cheaper KCNS and yield also fantast ...
18-12-2010 at 03:43
by: mario840
Preparation of cyanides
cyanureeves what can i say :D I HEARD this synthesis fucking rox , need low energy (boiling water ba ...
4-12-2010 at 01:26
by: mario840
Preparation of cyanides
[rquote=193852&tid=23&author=watson.fawkes][rquote=193832&tid=23&author=mario840]

...
2-12-2010 at 10:18
by: mario840
Preparation of cyanides
no hydrolysis but DEHYDRATION of formamide with P2O5 or AlCl3 , men can you read ??? hydrolysis was ...
2-12-2010 at 07:49
by: mario840
Preparation of cyanides
entropy51 good lord , holy mother of god , tell me and correct the recipe from Ledgard , tell me one ...
2-12-2010 at 01:33
by: mario840
Preparation of cyanides
People always amaze me how can they make life so difficult, 16 pages and almost eveything is trash , ...
1-12-2010 at 09:52
by: mario840
Reduction of oximes to corresponding amines
thx for reply , i think water and alcohol without acid will be fine , in my original recepture i tho ...
1-10-2010 at 12:26
by: mario840
Reduction of oximes to corresponding amines
[quote]
A problem in your procedure is a missing H+ donor.
You have to add some formic- or acetic ...
29-9-2010 at 22:56
by: mario840
Reduction of oximes to corresponding amines
so the step when i add NaOH to liberate amine MUST BE DONE ? or can i right after when reaction is o ...
28-9-2010 at 09:27
by: mario840
Reduction of oximes to corresponding amines
Hello

At first i wanna say that i tried reductive amination to prepare primary amines with of cou ...
28-9-2010 at 06:18
by: mario840
Diphenhydramine hydrochloride
thanks men !! :)
25-9-2010 at 04:48
by: mario840
Diphenhydramine hydrochloride
is there any patent for making dimethylethanolamine from 2-chloroethanol and dimethylamine ? or you ...
25-9-2010 at 01:22
by: mario840
Diphenhydramine hydrochloride
but did you succesfull synthesised it ??
24-9-2010 at 10:58
by: mario840
Isopropylamine and Diisopropylamine from Acetone
i have also thinking why not isolate glyphosate too , if Roundup is aqueous solution so we need to a ...
18-9-2010 at 03:57
by: mario840
Isopropylamine and Diisopropylamine from Acetone
so better add alone NaCl to solution or previous saturated aq. solution NaCl and then add to the rea ...
17-9-2010 at 09:06
by: mario840
Isopropylamine and Diisopropylamine from Acetone
yes but i wonder if this "method" works , amine will form a layer on top (very low density) or what ...
16-9-2010 at 13:24
by: mario840
Isopropylamine and Diisopropylamine from Acetone
what about roundup ? there is 360SL 360 g salt per 1 liter for 5- 6 euro and I am really interesting ...
16-9-2010 at 13:06
by: mario840
Isopropylamine and Diisopropylamine from Acetone
so how to extract isopropylamine from roundup ? diethyl ether ? please tell me more about it
15-9-2010 at 10:20
by: mario840
Isopropylamine and Diisopropylamine from Acetone
so what Hydroxylamine and acetone form oxime ? we must heat it under reflux ? how long ? give some m ...
15-9-2010 at 01:19
by: mario840
drying ether
it should be: is NOT OTC :) for plutonium
6-8-2010 at 23:08
by: mario840
drying ether
sorry for me is OTC ..is cheap like a beer and on this site is illustrated how to make sodium metal ...
6-8-2010 at 23:07
by: mario840
drying ether
this is simple .... you take 1 l ether and add 120 CaCl2 and shake , leave for couple days , shake e ...
6-8-2010 at 00:16
by: mario840
Preparation of PBr3?
Say that my friend have PBr3 and PBr5 can he make PCl3 or POCl3 ??
31-7-2010 at 23:31
by: mario840
Diphenhydramine hydrochloride
I research synthesis I found I'll post link above then I studies and experiment how to increase yiel ...
28-7-2010 at 01:23
by: mario840
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