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The short questions thread (2)
I'm trying to find procedures for acetylation of aniline with dilute acetic acid. Two references I h ...
12-7-2009 at 10:21
by: manimal
Good way to Methylamine HCl?
I'd like to contribute an improvement to Organikum's ethanol procedure. The reactants are combined i ...
9-7-2009 at 14:48
by: manimal
The short questions thread (2)
Ethylbenzene can be present in quite large amounts. According to it's MSDS, Startex brand xylene con ...
6-7-2009 at 01:31
by: manimal
The short questions thread (2)
Does anyone know the percentages of xylene isomers contained in commercial xylene solvent?

And: w ...
5-7-2009 at 19:35
by: manimal
The short questions thread (2)
Since concentrated ammonia solution is so useful but rather scarce, I was thinking that a promising ...
2-7-2009 at 14:39
by: manimal
The short questions thread (2)
Do amino acids form ammonium salts in the presense of ammonia, e.g. ammonium glycinate?
7-6-2009 at 17:08
by: manimal
Dreams
Plain alcohol influences my dreams to some extent. After retiring from a drinking spell, I usually n ...
5-6-2009 at 16:47
by: manimal
Thiourea Dioxide --> better than borohydride?
[rquote=147238&tid=11785&author=Nicodem]There were a couple of references where N-oxides of ...
5-6-2009 at 14:17
by: manimal
The short questions thread (2)
I have noted an inability to "salt out" 91% isopropanol. Added salt does not induce formation of lay ...
31-5-2009 at 14:50
by: manimal
Dreams
[rquote=149011&tid=11930&author=Nicodem]In principle even nicotine can be oneirogenic if apl ...
31-5-2009 at 01:03
by: manimal
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
No. Use overhead stirring (nickel or HDPE stirrer).
28-5-2009 at 12:12
by: manimal
Amino alcohol via Akabori, trial run
no1uwant2no, you may want to have a look at US patent 5346828. The Erlenmeyer phenylserine synthesis ...
23-5-2009 at 09:47
by: manimal
The short questions thread (2)
Some solubility values for substances list two different values: one for 'anhydrous' substance, and ...
18-5-2009 at 18:30
by: manimal
The short questions thread (2)
Can I use sodium carbonate or bicarbonate and ammonium sulfate to create concentrated ammonia soluti ...
18-4-2009 at 13:46
by: manimal
Willgerodt rxn: Styrene monomer -> phenylacetamide
I just realized that the experimental part of the Chinese patent came straight out of Organic Reacti ...
14-3-2009 at 13:50
by: manimal
Zinc catalysed reduction on 1-Phenyl-2-nitropropene
The former compound was a saturated nitropropane, correct? Zn/HCl will reduce a nitro group but not ...
8-3-2009 at 14:00
by: manimal
Willgerodt rxn: Styrene monomer -> phenylacetamide
One thing I don't understand about this procedure is how the addition of ethanol can improve the rea ...
4-3-2009 at 17:59
by: manimal
The short questions thread (1)
Methylamination of camphor gives d,l N methylbornylamine. The isomeric bornylamines melt at 163C and ...
26-2-2009 at 17:10
by: manimal
Thiourea Dioxide --> better than borohydride?
Here's a cleaned-up machine translation using a combination of google and altavista, and cross check ...
25-2-2009 at 07:19
by: manimal
The short questions thread (1)
What is a kewl?
22-2-2009 at 04:22
by: manimal
The short questions thread (1)
[quote][i]Originally posted by Formula409[/i]
Actually, I was planning on exploring whether thioure ...
21-2-2009 at 03:58
by: manimal
Thiourea Dioxide --> better than borohydride?
Am I right in ascertaining from the pictures that it can reduce benzylic ketones all the way to the ...
20-2-2009 at 20:16
by: manimal
Thiourea Dioxide --> better than borohydride?
[quote][i]Originally posted by Baphomet[/i]
If anyone has the full text for "Reduction of organic c ...
18-2-2009 at 23:29
by: manimal
mercury
[quote][i]Originally posted by Lambda-Eyde[/i]
[url=http://secure.sciencecompany.com/Mercury-Metal- ...
18-2-2009 at 20:22
by: manimal
Thiourea Dioxide --> better than borohydride?
[quote][i]Originally posted by UnintentionalChaos[/i]

I wonder if this reaction can be modified t ...
16-2-2009 at 13:10
by: manimal
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