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PbO2
The picture I <i>intended</i> to attach, instead of that horrible closeup:
21-9-2004 at 19:37
by: axehandle
FTP Server #2
You seem like a real masochist, but upload as much as you want, I'm not complaining... :)

As ...
21-9-2004 at 18:20
by: axehandle
My steaming vat of poison
Not steaming, actually, but it sounded more dramatic that way. Here's a picture of my 2nd run, ...
21-9-2004 at 17:49
by: axehandle
Darwin's Black Box
Seems I have to clarify what I meant. First, I didn't mean "religious crackpots" as i ...
21-9-2004 at 15:40
by: axehandle
Darwin's Black Box
Evolution isn't a "belief", it's a scientific fact. There isn't a debate be ...
21-9-2004 at 07:51
by: axehandle
abuse of member registration
Yes.

I've deleted it. Sometimes I do really stupid things.
20-9-2004 at 14:53
by: axehandle
FTP Server #2
Yes, please. I've PM:d you my addy.
20-9-2004 at 13:27
by: axehandle
ArrrrgggghhH!!!!
EDIT: Deleted


[Edited on 2004-9-20 by axehandle]
20-9-2004 at 11:16
by: axehandle
PbO2
Well, bleach works, but I stupidly used some kind of outdoor furniture cleaner containing soap, NaOH ...
19-9-2004 at 19:57
by: axehandle
PbO2
I shouldn't have evaporated the water on a hotplate -- damned PbO<SUB>2</SUB> decom ...
19-9-2004 at 14:18
by: axehandle
Scrapheap Challenge (industrial scavenging)
The PSU would be very good for electrochemical procedures. Some hotwiring of it is necessary, I can ...
18-9-2004 at 19:41
by: axehandle
Alternative route PbAc2 --&raquo; PbO2
I just conducted a small electrochemical experiment:

Approximately 10g of PbAc<SUB>2</SU ...
18-9-2004 at 19:37
by: axehandle
PbO2
PbO<SUB>2</SUB> isn't water soluble and besides I doubt a couple of grams would rai ...
18-9-2004 at 18:47
by: axehandle
PbO2
A centrifuge would have been lovely for this process. I think half of the PbO<SUB>2</SUB> ...
18-9-2004 at 14:44
by: axehandle
More on PbO2 electrodes
Hmm, that's a point I've given some thought actually --- I don't know if a welding tr ...
18-9-2004 at 11:08
by: axehandle
PbO2
*grumbles irritatedly* fascist regulations.... oh how I hate this country.... I should poison the ci ...
18-9-2004 at 08:43
by: axehandle
More on PbO2 electrodes
Oh, plexiglass I can find easily, but not until tomorrow :(... thanks for the idea though.

Gonna ...
17-9-2004 at 13:41
by: axehandle
VERY weird
Can anyone explain this:

(I've done the "let sink down to half the height then pour off ...
17-9-2004 at 11:17
by: axehandle
More on PbO2 electrodes
Yes, plexiglass is polymethyl methacrylate (PMMA) or polymethyl-2-methylpropanoate.
17-9-2004 at 10:54
by: axehandle
PbO2
Are you telling me that the chem supplier I contacted (Svenska Kemi) are so unwilling to make money ...
17-9-2004 at 10:51
by: axehandle
More on PbO2 electrodes
Good idea! It also gave me another: Acrylic, Plexiglass! Perhaps even polycarbonate (although that b ...
17-9-2004 at 07:23
by: axehandle
More on PbO2 electrodes
Can anyone think of a suitable, easily available piece of plastic to use as the substrate for the a ...
16-9-2004 at 21:04
by: axehandle
PbO2
I just implemented an improvement of the process that's not really obvious: I dumped in an aqua ...
16-9-2004 at 20:39
by: axehandle
NaClO4 production using a Pt clad Ti anode and a Ti cathode.
This was before I abandoned the Pt anode and decided to build a PbO<SUB>2</SUB> anode in ...
15-9-2004 at 09:55
by: axehandle
oleum & SO3
[quote]
Axehandle, what happened to this experiment? Did it work out?
[/quote]
Yes, I just forgot ...
12-9-2004 at 18:05
by: axehandle
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