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Preparation of cyanides
Yes don't even think about it, all sorts of crap would be in the destillate. This method is complete ... |
27-9-2009 at 07:09
by: Taoiseach |
Preparation of cyanides
This is from "the industry of cyan compounds":
Ammonium cyanide, NH4CN, is a highly volatile fl ... |
27-9-2009 at 00:41
by: Taoiseach |
Diving Into the World of Fulminates
@Hennig Brand
in one of those excerpts Rosco posted above, it says that moist SF when dried in d ... |
16-9-2009 at 22:34
by: Taoiseach |
Exotic Primaries - Complex Salts
I never heard that filter paper soaked in 10% HClO3 ignites and I highly doubt it would. The concent ... |
10-9-2009 at 22:26
by: Taoiseach |
Exotic Primaries - Complex Salts
Wikipedia once again proved guilty of spread of bullshit and disinformation  Yes
Pb(ClO3)2 is h ... |
8-9-2009 at 22:44
by: Taoiseach |
Exotic Primaries - Complex Salts
Fascinating stuff. The patent is quite vague tough. Here's the relevant info I scraped together: "Us ... |
5-9-2009 at 11:48
by: Taoiseach |
Permanganates
Very interesting stuff monoceros!
[quote]there was more whitish matter that was probably BaCO3 fr ... |
5-9-2009 at 02:43
by: Taoiseach |
Preparation of ionic nitrites
I'm also confused. Obviously I did something wrong - but what?
I did everything as described in lit ... |
29-8-2009 at 14:55
by: Taoiseach |
Preparation of ionic nitrites
Altough difficult to see in the image, quite a lot of lead remained unreacted. I extracted the fused ... |
29-8-2009 at 08:08
by: Taoiseach |
Preparation of ionic nitrites
This is the end product. The mixture became thicker and thicker and in the end it was impossible to ... |
29-8-2009 at 07:41
by: Taoiseach |
Preparation of ionic nitrites
I had a go at the lead+NaNO3 method also. A coal fire in an old saucepan was used as heat source.
... |
29-8-2009 at 07:39
by: Taoiseach |
Exotic Primaries - Complex Salts
Thx for the paper. I wish I had it before my experiments 
I didnt find a prep so I just tried i ... |
17-8-2009 at 23:12
by: Taoiseach |
Diazidodiamminocopper(II)
was prepared according to
CuSO4*5H2O + 2NH3 + 2NaN3 ---> [(NH3)2(N3)2Cu] + Na2SO4 + 5H2O
NH ... |
17-8-2009 at 05:33
by: Taoiseach |
K2MnO4 conversion to KMnO4
In his exact words he has multiplicated 1 kilogram of K2MnO4 into 270 kilograms. Altough this sounds ... |
15-8-2009 at 02:19
by: Taoiseach |
Antimony chloride?
Destillation of SbCl3 is troublesome. You need to catch it at the right time, otherwise all you get ... |
11-8-2009 at 22:50
by: Taoiseach |
Hydrazine
Sounds good. Isocyanuric acid is a beproduct of chlorine production via TCCS+HCl. Question is: How c ... |
11-8-2009 at 07:48
by: Taoiseach |
Thermochemical sodium?
I just read the paper on thermal decomposition of hexacyanoferrate. To recap
-K can be obtained i ... |
11-8-2009 at 05:01
by: Taoiseach |
Mr Anonymous method & ideas 4 improvement
I have performed the hydrazine synthesis according to Mr. anonymous method numerous times now and it ... |
11-8-2009 at 04:02
by: Taoiseach |
Thermochemical sodium?
Someone wrote about it on another forum. He found KN3 was very difficult to decompose. A strong heat ... |
10-8-2009 at 04:50
by: Taoiseach |
Thermochemical sodium?
"Alkali metal compounds, such as the hexacyanoferrates (II), cyanides, and azides can be decomposed ... |
9-8-2009 at 23:45
by: Taoiseach |
Which oxidizers are explosives?
CoII and CoIII also gave very energetic and sensitive ammino complexes in my experiments, however bo ... |
8-8-2009 at 06:55
by: Taoiseach |
Which oxidizers are explosives?
A lot of oxidizers are explosive by semself, simply because they are not very stable and release a l ... |
6-8-2009 at 05:59
by: Taoiseach |
Azides
sorry 4 broken link here's the complete one:
http://www.dtic.mil/cgi-bin/GetTRDoc?AD=AD404719& ... |
2-7-2009 at 14:43
by: Taoiseach |
Azides
Semi-safe (only 2 explosions occured during experimentation  ) method for
generating gaseous HN3:
... |
2-7-2009 at 14:36
by: Taoiseach |
Azides
*Update*
The AgN3 -> NaN3 route has been worked out before:
http://www.sciencemadness.org/t ... |
23-6-2009 at 05:13
by: Taoiseach |
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