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First o-toluidine synthesis - running into some issues with the reaction mixture
You need to add an excess of hydroxide to redissolve the tin hydroxide. It initially turns very thic ...
14-3-2021 at 11:26
by: RustyShackleford
Waste disposal men, and no, not the trash-can kind
I hand all my chemical waste to the dump/recycling centre. i have no idea what they do with it but t ...
12-3-2021 at 17:46
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
Vacuum is better, i just dont have a pump good enough for that.
I would like to see all of those d ...
12-3-2021 at 16:04
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
@Bezaleel
Wow that lithium salt looks amazing!
I have also noticed that its not really possible to ...
12-3-2021 at 14:54
by: RustyShackleford
Various chlorotoluenes produced during Toluene+TCCA+uv synthesis
My experience w that reaction was that it almost only formed benzyl chloride, did you add something ...
8-3-2021 at 14:11
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
Remade the aniline violurate with distilled clean amine, its a very dark red.
Anthranilic acid vio ...
7-3-2021 at 09:58
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
[rquote=655623&tid=156755&author=Amos]I don't believe I've seen anyone post an aniline salt ...
28-2-2021 at 11:46
by: RustyShackleford
KClO3 or KClO4 after electrolysis ?
MMO does not produce perchlorate, the reason for your voltage difference is dissolved KCl, it should ...
28-2-2021 at 06:45
by: RustyShackleford
No KClO3 formation in chlorate cell?
Everything metalresearcher said is correct. I also ran a cell with 1.2L volume and i had 10A of curr ...
27-2-2021 at 10:05
by: RustyShackleford
Making KMnO4 ?
Chlorine gas works
23-2-2021 at 13:29
by: RustyShackleford
Polyphosphoric acid
[rquote=655386&tid=156165&author=draculic acid69]Rustyshackleford is that a Friedel craft rx ...
23-2-2021 at 04:11
by: RustyShackleford
Polyphosphoric acid
[rquote=655373&tid=156165&author=karlosĀ³]I liked the P2O5/85% H3PO4 reaction to make polyph ...
22-2-2021 at 13:29
by: RustyShackleford
Polyphosphoric acid
aprox 125ml of 85% orthophosphoric acid was heated on the maximum setting with a heating mantle.
T ...
22-2-2021 at 12:15
by: RustyShackleford
Attempt to make molten lead from oxalate
Some metals decompose into oxide by
MC2O4 -> MO + CO + CO2
22-2-2021 at 03:38
by: RustyShackleford
Improving chloroform yield with acid.
[rquote=654913&tid=156572&author=Amos]Since the topic of using calcium hypochlorite is fresh ...
21-2-2021 at 12:51
by: RustyShackleford
Yellowing MEK/Butanone
an acid inhibitor makes sense, as bases in contact ketones tend to form a complicated mixture of bro ...
21-2-2021 at 12:47
by: RustyShackleford
1000%+ of expected yield of cobalt from lithium ion batteries. Why?
You should read my post here about the extraction and purification of cobalt from Li batteries
htt ...
15-2-2021 at 16:54
by: RustyShackleford
NiCl2 Weirdness
jesus, just put the nickel in HCl and stir it / bubble air through it for a few days or a week
14-2-2021 at 06:44
by: RustyShackleford
New Video: Holding Breath with Pure O2
If you want to redo it, a plastic bag of some sort should definitely be used to make the breathing e ...
13-2-2021 at 04:19
by: RustyShackleford
Something strange happened to my CuSO4 solution
Commercial/garden grade copper sulfate has carbonate and sometimes a waxy residue (of yellow apperan ...
13-2-2021 at 04:18
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
[rquote=654689&tid=156755&author=Housane]Ok thanks, where did you find your nitrite? As it i ...
9-2-2021 at 03:53
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
[rquote=654639&tid=156755&author=vano]I gladly tried the following metals. Scandium, cadmium ...
8-2-2021 at 14:57
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
[rquote=654600&tid=156755&author=Housane]What amazing colours, I want to try and make sum bu ...
8-2-2021 at 13:32
by: RustyShackleford
what do you use to store iodine/bromine
[rquote=207821&tid=15452&author=thethule]Hi guys, i have a nice element collection going, bu ...
2-2-2021 at 13:25
by: RustyShackleford
Mark Robers Secret Devil's Toothpaste Recipe Revealed
Well i mean so dangerous that it will explode by itself, 50% still has a ton of water to "stabilize" ...
1-2-2021 at 01:13
by: RustyShackleford
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