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Quick question: Oximes
I'll keep that in mind for next time. You're right, the one-pot does usually end up a mess. What sol ... |
8-12-2012 at 17:45
by: Rich_Insane |
Quick question: Oximes
Well here's what I'm doing with the last of my reagents (sadly I started before your reply):
Inst ... |
8-12-2012 at 17:33
by: Rich_Insane |
Quick question: Oximes
According to that reference, the nitrile is a part of a catalytic cycle in which the copper (II) cat ... |
8-12-2012 at 15:37
by: Rich_Insane |
Quick question: Oximes
I do not have access to TLC, unfortunately. All starting materials excepting the substrate (aldehyde ... |
8-12-2012 at 15:02
by: Rich_Insane |
Quick question: Oximes
I've been trying to manipulate oximes to synthesize amides lately, with little success. I was wonder ... |
6-12-2012 at 20:52
by: Rich_Insane |
Sodium Hypochlorite
I have not seen anything around. There are farm supply stores around here, but I'd rather purchase i ... |
19-11-2012 at 10:21
by: Rich_Insane |
Sodium Hypochlorite
I do have NaOH (approximately 400 grams) and HCl on the way, but I fear this is not enough to pursue ... |
15-11-2012 at 22:12
by: Rich_Insane |
Orygun local
I'm located in the land of the Ore-gone. I don't have very much however. U2U me. |
5-11-2012 at 10:27
by: Rich_Insane |
Sodium Hypochlorite
I tried ordering from one of those eBay sources (different vendor), but they cancelled my order stat ... |
4-11-2012 at 13:57
by: Rich_Insane |
Sodium Hypochlorite
[quote]
Whats so wrong with 5 gallons pails? When I needed to buy some 10-12.5% sodium hypochlori ... |
2-11-2012 at 11:17
by: Rich_Insane |
Sodium Hypochlorite
[quote]
Why not just evaporate the water from bleach until you get the concentration you want?[/q ... |
1-11-2012 at 10:16
by: Rich_Insane |
Sodium Hypochlorite
I can't really afford to buy too many other reagents for the sole purpose of producing NaOCl. I inte ... |
31-10-2012 at 20:34
by: Rich_Insane |
Sodium Hypochlorite
So I've recently found out that one of the companies I ordered sodium hypochlorite from has decided ... |
31-10-2012 at 13:24
by: Rich_Insane |
Cooking stoves!
So, I was planning on purchasing a hotplate, but I realized that I've gone over budget and am unlike ... |
16-10-2012 at 09:22
by: Rich_Insane |
Extraction of 5-HTP and decarboxylation to serotonin?
PureBulk sells large amounts of 5HTP powder for reasonable prices, iirc. See if your results are dif ... |
16-10-2012 at 09:16
by: Rich_Insane |
N-Methyl-d,l Alanine
Wouldn't it be best just to use racemic alanine? |
1-10-2012 at 08:25
by: Rich_Insane |
N-Methyl-d,l Alanine
[quote]
I have one idea: 1) Oxidation of lactic acid to the corresponding carbonyl compound 2) Re ... |
28-9-2012 at 11:42
by: Rich_Insane |
In Need of Some Equipment
Hey everyone!
It's that time of year when I go around looking for equipment I may need for future ... |
28-9-2012 at 11:38
by: Rich_Insane |
Hydroxylamine/copper
I've been interested in a particular method for formation of amides from aldehydes for a while -- th ... |
20-9-2012 at 10:40
by: Rich_Insane |
demethylation of methyl aryl ethers
Wasn't there a patent not long ago that described cleavage of aryl methyl ethers with thiourea and A ... |
17-9-2012 at 07:30
by: Rich_Insane |
aldehyde to amide musings and needed help
What about reaction of the aldehyde with hydroxylamine followed be rearrangement to amide via the Cu ... |
8-9-2012 at 17:23
by: Rich_Insane |
Modified Phenylethylamine as antidepressant?
I wonder if N-acetylation might allow for the creation of a prodrug. Or perhaps substitution on the ... |
6-9-2012 at 08:12
by: Rich_Insane |
Basic Solvent Choice
The polycyclic structure (largely aliphatic as well) and lack of significantly electronegative atoms ... |
26-7-2012 at 14:19
by: Rich_Insane |
Making solar panels from Chlorophyll without any pollution HELP
I've been doing a lot of work lately with various biologically produced pigments that react to light ... |
13-6-2012 at 13:19
by: Rich_Insane |
Extraction of caffeine with diethyl ether
I'd use dichloromethane just 'cause that's what is generally used for solvent-based caffeine extract ... |
30-5-2012 at 19:28
by: Rich_Insane |
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