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alpha-chloropropionic acid ethyl ester
The solution from above had been sitting around for a bit, and had discolored thoroughly to a bright ...
4-7-2005 at 12:52
by: Natures Natrium
condensation of NO2
Hmm, well, I'm not sure what the deal is then. I was using a 300mm west condenser with ice wat ...
1-7-2005 at 20:20
by: Natures Natrium
condensation of NO2
Just a quick request for anyone who has ever managed to succeed at condensing NO2 to post info about ...
1-7-2005 at 17:48
by: Natures Natrium
Oh yea.
Well, the SO2 tank is holding up nicely. I was able to reduce a solution of cupric chloride to cupr ...
27-6-2005 at 18:42
by: Natures Natrium
Well, I did it.
For better or worse, and hopefully death won't make me part, I did it. :D

I attempted to con ...
27-6-2005 at 01:04
by: Natures Natrium
Amine electrophiles
Vogels has a preparation which might interest you.

IV,38. p-NAPHTHYLAMINE
Pass a stream of sulph ...
26-6-2005 at 10:18
by: Natures Natrium
Good info
Ok, I think things are coming together. On further contemplation both the ideas of pop bottles and ...
22-6-2005 at 10:29
by: Natures Natrium
SO2 tank
I have some ideas for this and data to back it up, as well as some questions I could use answered. ...
21-6-2005 at 21:09
by: Natures Natrium
Rubber stopper and a weird story
[quote][i]Originally posted by Darkblade48[/i]

I've been trying this, but my problem runs ac ...
18-6-2005 at 07:33
by: Natures Natrium
Rubber stopper and a weird story
Hmm, direct prolonged contact with sulfuric acid renders stoppers hard as rocks. This might be more ...
17-6-2005 at 20:50
by: Natures Natrium
HELP
Ok, maybe I'm overstepping my bounds here, but I can't help but wonder why the hell this t ...
16-6-2005 at 07:21
by: Natures Natrium
alpha-chloropropionic acid ethyl ester
I tried the following. To the left over aqueous solution from above was added another half mol of l ...
15-6-2005 at 09:01
by: Natures Natrium
Hmm, no luck
Well, my method as posted above, except that the solution was left in the flask for 120 hours (w/ 6h ...
10-6-2005 at 08:30
by: Natures Natrium
alpha-chloropropionic acid ethyl ester
[quote][i]Originally posted by IPN[/i]
100ml of 80% lactic acid was refluxed for 2h in an oil bath ...
6-6-2005 at 12:15
by: Natures Natrium
"Ceramics uneffected by chlorine"
According to patent US 1,926,072, (quoted elsewhere on this board for the production of PCl3), an al ...
3-6-2005 at 11:59
by: Natures Natrium
alpha-chloropropionic acid ethyl ester
Ah, I see. Should I attempt this synthesis again, I shall use a modified procedure. If the concent ...
31-5-2005 at 07:50
by: Natures Natrium
alpha-chloropropionic acid ethyl ester
"Will the Zn/HCl work? No doubt, it *will* chlorinate the -OH group - "

I am curious as ...
30-5-2005 at 20:53
by: Natures Natrium
Hot toluene: a great solvent for sulfur
Wow, very interesting. Thank you garage chemist, for sharing! :D

Nature's Natrium
14-5-2005 at 20:43
by: Natures Natrium
2-Br Propionic Acid Physical Properties
Thanks Kinetic for the information. I didn't have a whole lot of hope for it, but I did have a ...
9-5-2005 at 05:30
by: Natures Natrium
2-Br Propionic Acid Physical Properties
Recently I attempted an expieriment which yielded what I believe to be 2-bromopropionic acid (aka al ...
6-5-2005 at 16:20
by: Natures Natrium
New Easy Way to Phosphorous!
[quote][i]Originally posted by hodges[/i]
Although phosphates are not too hard to find, there are o ...
1-4-2005 at 05:49
by: Natures Natrium
HELP! need thionyl chloride(SOCl2) synthesis
[quote][i]Originally posted by garage chemist[/i]
I'm sorry that this comes so late, but I fou ...
23-3-2005 at 05:58
by: Natures Natrium
dry HBr?
If you've got NaBr and high concentration H2SO4 (>70%), then (IMHO) the best way is to gener ...
22-3-2005 at 07:39
by: Natures Natrium
HELP! need thionyl chloride(SOCl2) synthesis
I believe that I was successful in converting the S2Cl2/SCl2 solution into mostly SCl2. It took a s ...
17-3-2005 at 16:08
by: Natures Natrium
HELP! need thionyl chloride(SOCl2) synthesis
[quote][i]Originally posted by S.C. Wack[/i]
Heating with NaOH, etc. will remove the S.

Was the ...
16-3-2005 at 16:52
by: Natures Natrium
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