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thf oxidation Don't forget that lactones are easily synthetised by deshydrogenating diols. Have anyone ever tri ...	14-4-2008 at 08:36 by: Methyl.Magic
Formylation of 4-MeO-phenol with Mg(MeO)2 : Synthesis of m-vanilline The magnesium salt has been stored in a dessicator over an inert athmosphere (nitrogen). The offi ...	5-4-2008 at 06:16 by: Methyl.Magic
Formylation of 4-MeO-phenol with Mg(MeO)2 : Synthesis of m-vanilline Hey ! Thanks for comment ! The toluÃ¨ne from the orange solution (filtrate) was boiled off w ...	5-4-2008 at 02:42 by: Methyl.Magic
Formylation of 4-MeO-phenol with Mg(MeO)2 : Synthesis of m-vanilline Today I decided to filtered the precipitate on a buchner under vacuum. The precipitate is a yellow-c ...	31-3-2008 at 11:49 by: Methyl.Magic
Formylation of 4-MeO-phenol with Mg(MeO)2 : Synthesis of m-vanilline 200ml of fluka-quality anhydrous MeOH is poued in a 750ml four-necked flask fitted with a reflux con ...	31-3-2008 at 11:35 by: Methyl.Magic
Formylation of 4-MeO-phenol with Mg(MeO)2 : Synthesis of m-vanilline Hey !!! Last Sunday I decided to test the Magnesium methoxide formylation. It has been reported ...	31-3-2008 at 10:53 by: Methyl.Magic
reductive amination with triacetoxyborohydride [quote][i]Message original : grind[/i] You can add 4 or more moles of AcOH to 1 mol of NaBH4, in t ...	30-3-2008 at 04:19 by: Methyl.Magic
Drying ethers over P2O5 [quote][i]Message original : Klute[/i] And do you dry your THF on 3A MS too? Is that sufficent to ...	19-3-2008 at 04:24 by: Methyl.Magic
Drying ethers over P2O5 Personally, I use THF for hydride reduction and diethylether for grignard... I always dry my Et2O ...	17-3-2008 at 10:40 by: Methyl.Magic
Isopropyl Mercaptan Synthesis good synthesis ! Don't forget that mercaptan can be synthethised by grignard reagent and sulfur w ...	16-3-2008 at 03:50 by: Methyl.Magic
Oxidising THF using calcium hypochlorite GBL is more used as substrate (i.e. for making 4-chlorobutyryl chloride) than as solvent... GBL ...	16-3-2008 at 03:38 by: Methyl.Magic
Methylation of phenolic aldehydes with MeI in DMF: 2-methoxybenzaldehyde Bien JouÃ© ! Ca c'est du bon boulot ! I'm happy to see that TMP alkylation gives good yield ! ...	16-3-2008 at 03:05 by: Methyl.Magic
Methylation of phenolic aldehydes with MeI in DMF: 2-methoxybenzaldehyde For the next Job perhaps I'll try a "all-in-one" o-formylation of phÃ©nol. 1) dissolve the phe ...	19-2-2008 at 10:55 by: Methyl.Magic
Amines from alcohols?? [quote][i]Message original : Nicodem[/i] You should provide more information for a reliable answer ...	19-2-2008 at 09:35 by: Methyl.Magic
Methylation of phenolic aldehydes with MeI in DMF: 2-methoxybenzaldehyde [quote][i]Message original : Klute[/i] How good were the yields? >70%? How long did you let ...	12-2-2008 at 11:54 by: Methyl.Magic
Green Methylating agent....comments personally I use trimethylphosphate : it's relatively nontoxic , cheap and more effective than DMC.	12-2-2008 at 11:16 by: Methyl.Magic
Methylation of phenolic aldehydes with MeI in DMF: 2-methoxybenzaldehyde hey this is a good job ! Your cristals are beautiful, I'll eat some for my breakfeast !!! and 73% ...	9-2-2008 at 03:26 by: Methyl.Magic
Solvant-free Decarboxylation of Amino-acid I 've just done the first trial. I used a hotplate equipped with a Pt-100. Decarboxylation starts ...	8-2-2008 at 09:46 by: Methyl.Magic
Solvant-free Decarboxylation of Amino-acid The standard decarboxylation method are not very good for L-tryptophan. Refluxing in a high bp so ...	7-2-2008 at 12:52 by: Methyl.Magic
Ether halogenation? intersesting question. Normally when you brominate a molecule the substrate is more reactive than ...	7-2-2008 at 12:11 by: Methyl.Magic
GBL Distillation - Vacuum or no? At frist distil sour DCM at standard pressure. Then, if you have a vacuum pump why not use it ??? Yo ...	29-11-2007 at 11:36 by: Methyl.Magic
GBL Distillation - Vacuum or no? You don't need vacuum !!! GBL is very stable to heat and easily distilled at atmospheric pressure ...	21-11-2007 at 09:48 by: Methyl.Magic
L-tryptophan decarboxylation [quote][i]Message original : Grimble_Gromble[/i] [quote][i]Originally posted by Methyl.Magic[/i] ...	10-10-2007 at 10:31 by: Methyl.Magic
oxidation alcohol to aldehyde with MnO2 Aldehydes can easily synthetised from alcool via Dehydrogenation with Copper chromite as catalyst !! ...	24-8-2007 at 10:19 by: Methyl.Magic
L-Proline Esterification the ether has been distilled to give 1.01g of ethyl prolinate as yellow oil. i didnt distill this oi ...	24-8-2007 at 10:02 by: Methyl.Magic
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