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Oxidation of aldehydes to carboxylic acids?
Oxidizing an aldehyde to a carboxylic acid is one of the easiest functional group transformations. G ...
6-7-2020 at 18:20
by: JJay
Anhydrous Aluminum Chloride prepration
I have made small amounts of aluminum chloride from hydrogen chloride and aluminum in a quartz tube. ...
30-6-2020 at 08:30
by: JJay
Retort & Stand Questions
Cody of Cody's Lab stuck a retort in a sand bath: https://youtu.be/aUzMms62hKw?t=69

Retorts are i ...
27-6-2020 at 15:59
by: JJay
Oxalyl Chloride Challenge
I had an idea.

[file]81793[/file]

Trichloromethylbenzene is capable of chlorinating carboxyli ...
24-6-2020 at 20:24
by: JJay
Oxalyl Chloride Challenge
I'd think that oxidation of ethylene glycol with PCC or chromium VI oxide peroxide etherate would wo ...
24-6-2020 at 08:33
by: JJay
Oxalyl Chloride Challenge
[rquote=639064&tid=82462&author=clearly_not_atara][rquote=639048&tid=82462&author=ma ...
24-6-2020 at 02:26
by: JJay
Oxalyl Chloride Challenge
Glyoxal can be prepared by the action of nitric acid on ethanol and purified by the bisulfite adduct ...
23-6-2020 at 14:59
by: JJay
Oxalyl Chloride Challenge
This challenge is still on.
23-6-2020 at 07:50
by: JJay
Almost getting caught
[rquote=638990&tid=155603&author=NonEthicalPyrotechnics]I feel like I should say i'm not an ...
23-6-2020 at 05:57
by: JJay
Nitrates in decent yield from the oxidation of melamine by calcium hypochlorite
This is excellent work.
21-6-2020 at 11:36
by: JJay
Preparing a chromatography column
I have certainly read of burettes being used as columns. (See, for example, https://pubs.acs.org/doi ...
18-6-2020 at 17:20
by: JJay
Almost getting caught
[rquote=638555&tid=155603&author=NonEthicalPyrotechnics]I'm sorta new to energetic chemistry ...
18-6-2020 at 17:12
by: JJay
Phenylacetaldehyde from Phenylalanine
As it turns out, monochlorination of phenylalanine leads to a degradation that produces phenylacetal ...
9-5-2020 at 14:17
by: JJay
Melgar has died
I am extremely sorry to learn of Melgar's passing. I know a lot of people think I didn't like Melgar ...
6-5-2020 at 14:56
by: JJay
Oxalyl Chloride Challenge
[rquote=516600&tid=82462&author=JJay]
[sub]5. I reserve the right to close the competition ...
15-12-2018 at 18:43
by: JJay
Oxalyl Chloride Challenge
[rquote=563166&tid=82462&author=Texium (zts16)][rquote=563003&tid=82462&author=JJay] ...
15-12-2018 at 13:47
by: JJay
Oxalyl Chloride Challenge
I will be actively working to synthesize oxalyl chloride next week. I'll check back, and if someone ...
15-12-2018 at 01:14
by: JJay
Post #2000 and an apology for accidentally deleting a thread
No, not a chance, absolutely not. As a U.S. citizen, I will not be a part of a forum where Melgar is ...
15-12-2018 at 00:25
by: JJay
Post #2000 and an apology for accidentally deleting a thread
My approach to this discussion was not counterproductive. Melgar's approach to this discussion was d ...
15-12-2018 at 00:16
by: JJay
Post #2000 and an apology for accidentally deleting a thread
So, I reiterate, and please, unless you are a mod, hold your peace:

If I write a superior spam-fi ...
14-12-2018 at 22:48
by: JJay
Post #2000 and an apology for accidentally deleting a thread
So let's say I come up with a working system, and it's better than Melgar's. Will it replace his? Se ...
14-12-2018 at 17:52
by: JJay
Post #2000 and an apology for accidentally deleting a thread
woelen: In response to my questions, Melgar gave a false and self-promoting excuse that wouldn't eve ...
14-12-2018 at 16:54
by: JJay
Post #2000 and an apology for accidentally deleting a thread
[rquote=562461&tid=112108&author=Tsjerk]You are great Melgar! [/rquote]

I have very sound ...
14-12-2018 at 00:23
by: JJay
Post #2000 and an apology for accidentally deleting a thread
[rquote=562400&tid=112108&author=Melgar]That's better than my GMail's spam filter, for both ...
13-12-2018 at 22:26
by: JJay
Post #2000 and an apology for accidentally deleting a thread
[rquote=562360&tid=112108&author=clearly_not_atara]Machine learning is a pain in the ass[/rq ...
13-12-2018 at 18:25
by: JJay
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