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Lead powder Hi,
I will try the PbO test, to be sure of its composition.
I think the lead may have contained an ... |
11-2-2005 at 04:52 by: CycloKnight |
Cinnamon experiment #2 results Steam distillation has now been completed.
This is the mixture before I resumed the steam distill ... |
10-2-2005 at 13:58 by: CycloKnight |
Cinnamon experiment #2, update I refluxed the mixture for 12 hours straight.
I started the reflux yesterday at 20:00,
and I swit ... |
9-2-2005 at 14:01 by: CycloKnight |
PbO I know an easy way to make quite a fair amount of lead oxide, provided you have decent ventillation. ... |
9-2-2005 at 10:15 by: CycloKnight |
Update This is just an update on the reaction I started this evening.
Chemical used:
~430g Cinnamon ... |
8-2-2005 at 12:48 by: CycloKnight |
Mass Production For mass production of benzaldehyde from toluene, the air oxidation of toluene isn't so bad.
... |
8-2-2005 at 09:23 by: CycloKnight |
Benzaldehyde If all goes well, I should have the last batch of cinnamaldehyde (to benza.)started this evening.
... |
8-2-2005 at 06:44 by: CycloKnight |
Increasing yield.. It would be good if it were possible to extract the benzaldehyde out as it forms, it would certainly ... |
7-2-2005 at 14:49 by: CycloKnight |
Benzaldehyde Thanks for the compliments, I really enjoyed taking the pictures, I'll try to take more of futu ... |
7-2-2005 at 06:20 by: CycloKnight |
Extraction of psychoactive material from cannabis I've carried out the soxhlet extraction of the psychoactive ingredients of cannabis at least a ... |
7-2-2005 at 05:08 by: CycloKnight |
Cinnamon experiment complete Fractional distillation of the crude product has now been completed.
The fractional distillation wa ... |
6-2-2005 at 14:26 by: CycloKnight |
Manganese-Ammonium cell images "You tell me man, I only work here." - Hudson, Aliens
[img]http://www.sciencemadness.org ... |
5-2-2005 at 19:16 by: CycloKnight |
Cinnamon oil experiment update. The cinnamon oil to benzaldehyde conversion experiment is not yet complete.
So far I have extracted ... |
5-2-2005 at 12:46 by: CycloKnight |
Benzaldehyde from Cinnamon Oil. Okay, this is my latest experiment, and let me say - it truly works wonders.
If you are looking fo ... |
3-2-2005 at 14:38 by: CycloKnight |
Benzaldehyde Toluene oxidation...
Take 3.
Okay, regeneration is nearly complete.
[img]http://www.sciencemadn ... |
3-2-2005 at 13:37 by: CycloKnight |
toluene --> benzaldehyde For the manganese-ammonium sulphate mixture, the ingredients I have used are based on the patent rat ... |
1-2-2005 at 12:30 by: CycloKnight |
toluene --> benzaldehyde Okay, I did another run last night and it was a success. However, it was only a partial run.
I esti ... |
1-2-2005 at 01:29 by: CycloKnight |
Yield Okay, I would just like to say that the yield was a little on the low side, however please take the ... |
29-1-2005 at 15:30 by: CycloKnight |
Manganese ammonium alum cell Okay, as promised here is my photo essay of the mananese-ammonium alum cell, which can be used for t ... |
29-1-2005 at 14:58 by: CycloKnight |
Sassafras Albidum Sold by Sandeman Seeds.
http://www.sandemanseeds.com/acatalog/Trees_S.html |
28-1-2005 at 13:23 by: CycloKnight |
toluene --> benzaldehyde {img}http://www.sciencemadness.org/scipics/anode.jpg{/img}
[Edited on 29-1-2005 by CycloKnight] |
27-1-2005 at 13:48 by: CycloKnight |
Electric benzaldehyde Yes, i agree that there is a vast excess of oxidant. Though, it is perfectly regenerable and not too ... |
26-1-2005 at 06:39 by: CycloKnight |
Benzaldehyde via Cl2/toluene Hi folks,
what follows is some discouragement for the Cl2/toluene method and then a procedure for m ... |
26-1-2005 at 04:56 by: CycloKnight |
Nitrite That is very informative, thanks Polverone. That is indeed the information I'm looking for. In ... |
26-1-2005 at 03:20 by: CycloKnight |
Sodium or potasium nitrite Is there a reliable process for converting the nitrate into the nitrite using heat?
I recall using ... |
25-1-2005 at 07:54 by: CycloKnight |
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