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Acetonitrile synth
Why do people prefer complicated speculative syntheses rather than the published easy ones?
31-1-2019 at 16:18
by: clearly_not_atara
Mn(3+)SO4
Fortunately the ortho-methoxyamphetamine you would make from that isn't an active recreational drug. ...
31-1-2019 at 00:47
by: clearly_not_atara
Oxidation of Nitriles to Nitro groups
https://pubs.acs.org/doi/abs/10.1021/ja037325a
30-1-2019 at 22:27
by: clearly_not_atara
indole from solvent extraction of feces
this is unironically awesome if it works but

[i]where[/i]

did you get the idea that there was ...
30-1-2019 at 18:26
by: clearly_not_atara
Preparation of N-Bromosuccinimide
There are reports of making succinimide by heating succinic acid and urea; with catalytic metal oxid ...
30-1-2019 at 13:03
by: clearly_not_atara
The Short Questions Thread (4)
I noticed that the reaction:

N2 + 5/2 O2 + 2 KOH >> 2 KNO3 + H2O

has ΔH = [2 * -494] + ...
29-1-2019 at 01:07
by: clearly_not_atara
3,4,5-trimethoxyphenylacetonitrile hydrogenation problems
What kind of mineral acid are you using? The studies I see use sodium dihydrogen phosphate. I get th ...
27-1-2019 at 00:00
by: clearly_not_atara
Oxidation of Nitriles to Nitro groups
Two equivalents of acetonitrile oxide dimerize to 4,5-dimethylfuroxan.
25-1-2019 at 21:25
by: clearly_not_atara
Ethanolamine Synthesis
Oxirane: wrong! Toxic, lachrymatory, explosive and flammable.
Nitroethanol: wrong! The compound is ...
25-1-2019 at 11:28
by: clearly_not_atara
Oxidation of Nitriles to Nitro groups
It doesn't really work. The nitrile oxide is produced and it dimerizes to a furoxan.

You can mak ...
25-1-2019 at 11:16
by: clearly_not_atara
Boiling HNO3 plus even hotter cooking oil ?
[rquote=586313&tid=131379&author=Herr Haber]Working with multi Kg of silver at a time I just ...
22-1-2019 at 12:18
by: clearly_not_atara
How to determine the ratio of two chemicals mixed together?
What does potassium nitrate have to do with anything? The perchlorate isn't supposed to be an oxidiz ...
17-1-2019 at 19:15
by: clearly_not_atara
How to determine the ratio of two chemicals mixed together?
In this particular case, if sodium perchlorate is available, you can simply dissolve some of the sam ...
17-1-2019 at 15:10
by: clearly_not_atara
Where is the new location of the Vespiary website?
There has never existed any such website
17-1-2019 at 15:01
by: clearly_not_atara
How to determine the ratio of two chemicals mixed together?
You don't need to use toluene. It can be any liquid that doesn't dissolve salt. Even olive oil would ...
17-1-2019 at 13:29
by: clearly_not_atara
1,3-Diaminoacetone(1,3-diamino-2-propanone) problems
Yes, self-condensation is an issue. The formation of a 2,5-dihydropyrazine makes the condensed produ ...
16-1-2019 at 13:23
by: clearly_not_atara
The Short Questions Thread (4)
^Also, solutions of iron chloride are brown.

The HCl itself isn't colored, but with zinc it is? I ...
14-1-2019 at 20:11
by: clearly_not_atara
P2P-please don't discard, is just a scientific question with no intention about that chemical's synthesis
[rquote=581949&tid=127971&author=morganbw]I think that P2P actually became scheduled prior t ...
14-1-2019 at 09:48
by: clearly_not_atara
Easy synthesis of hydroiodic acid
HI can be produced from iodides using phosphoric acid, which is what he was referring to. It can als ...
12-1-2019 at 20:33
by: clearly_not_atara
Mom-and-pop lemonade-stand-style ways to make quick legal cash from chemistry
Guess again sweaty

All of the small carboxylic acids have their own characteristic flavor. This i ...
10-1-2019 at 18:20
by: clearly_not_atara
Mom-and-pop lemonade-stand-style ways to make quick legal cash from chemistry
[quote] - Look for niche markets: silver nitrate, silver or gold in powder or other form that your b ...
10-1-2019 at 13:25
by: clearly_not_atara
Easy synthesis of hydroiodic acid
There should not be any chromium present, so I do not understand the concern. All acids catalyze oxi ...
9-1-2019 at 15:32
by: clearly_not_atara
Easy synthesis of hydroiodic acid
[rquote=580026&tid=120001&author=Felab]
Are you sure that oxalic acid can displace iodides ...
9-1-2019 at 14:28
by: clearly_not_atara
Permanganates
[rquote=459691&tid=8480&author=Romain]Update: The crystals that formed from the evaporated a ...
9-1-2019 at 13:00
by: clearly_not_atara
isatoic anhydride condensation
It looks like the original question resulted from a mistakenly omitted "NH2" in a Kekule diagram. I ...
9-1-2019 at 12:47
by: clearly_not_atara
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