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Cubane instead of benzene with the phenylethylamine backbone
Ah, yes, I thought potassium tert-butoxide was used, tert-butoxide peroxide is going to be a bit har ...
30-12-2019 at 07:24
by: Tsjerk
Cubane instead of benzene with the phenylethylamine backbone
I think I have a new project on hands...
29-12-2019 at 08:16
by: Tsjerk
Cubane instead of benzene with the phenylethylamine backbone
[rquote=628670&tid=153370&author=Tellurium]Well synthesis of the cubane itself seems doable, ...
28-12-2019 at 08:31
by: Tsjerk
Airport Chemical Screening
These machines are small mass spectrometers, they catch anything that is a volatile organic. I can i ...
24-12-2019 at 05:28
by: Tsjerk
Report on making Iron Iodide
Is there a legal amount of P to own in Australia? I can send you some for shipping costs but I also ...
23-12-2019 at 15:31
by: Tsjerk
Chemistry techniques to improve cooking skills
Looking at what is actually happening in the pan/oven and understanding what is going on definitely ...
23-12-2019 at 15:23
by: Tsjerk
Trying to prepare sort of Aqua regia, but wonder if I will be fast enough before it decomposes
Language is a beautiful thing... Communication an ever more beautiful thing.
20-12-2019 at 01:48
by: Tsjerk
Help with carbon reduction of cyanate
[rquote=628150&tid=154586&author=PirateDocBrown]
Separate from unreacted KOH via recrystall ...
18-12-2019 at 09:21
by: Tsjerk
FC alkylation?
[rquote=628134&tid=154587&author=chemist1243][rquote=628099&tid=154587&author=Dracon ...
18-12-2019 at 08:01
by: Tsjerk
Help with carbon reduction of cyanate
[rquote=628132&tid=154586&author=XeonTheMGPony][rquote=628087&tid=154586&author=Terr ...
18-12-2019 at 06:49
by: Tsjerk
Iodine resublimation
Very nice sample Dan! Although no one would have expected differently from you of course.
18-12-2019 at 01:52
by: Tsjerk
(success) Preparation of isopropyl salicylate fragrant ester
Is there a reason you don't let the reaction run longer? Or with less salicylic acid, or with more a ...
17-12-2019 at 23:52
by: Tsjerk
Report on making Indium Iodide
[rquote=628001&tid=154570&author=Lion850]Tsjerk - the reaction was happening in the beaker. ...
15-12-2019 at 03:34
by: Tsjerk
Crap from "attempt to make isopropyl salicylate, something interesting happened"
[rquote=627996&tid=154569&author=Cou]Just finished reflux. 25 mL of isopropyl alcohol, 7.3 g ...
15-12-2019 at 03:18
by: Tsjerk
Report on making Indium Iodide
You should get yourself a drying tube you could place on one of those roundbottoms... DCM could be e ...
14-12-2019 at 04:35
by: Tsjerk
Magpie has died
Too bad.. Condolences to everyone.
12-12-2019 at 14:50
by: Tsjerk
Amounts of sulfuric acid and excess reactant in fischer esterificatoin procedures
Did you take the work-up of the product in account? I would hate a precursor in my mixture I can't s ...
10-12-2019 at 01:29
by: Tsjerk
What's the minimum concentration for h2so4 to be oxidising?
I know I shouldn't comment on AJKOER's comments, but AJKOER... Have you tried to perform the reactio ...
4-12-2019 at 10:09
by: Tsjerk
Chemistry gone wrong: peroxide, pH, peculiarities
pka H2O2 = 11,7
2-12-2019 at 21:38
by: Tsjerk
Grow Calcite Crystals and Birefringence
Try to grow a triglycine disulfate crystal. I got a three centimeter crystal easily, I just left the ...
2-12-2019 at 14:36
by: Tsjerk
Report on making Aluminium Iodide
Apperantly Al(I)I does exist, although not stable by itself, it can be stabilized as adduct with tri ...
2-12-2019 at 06:57
by: Tsjerk
Jute nitration failure
Rule of thumb: if plant derived material is strong (jute eg.) there is a lot of lignin, if it is fle ...
1-12-2019 at 23:18
by: Tsjerk
An odd smell from some acetone
Pure caffeine does smell a bit, it smells a bit bitter, but only slightly, you really have to stick ...
28-11-2019 at 23:15
by: Tsjerk
Did I accidently make Titanium tetrachloride?
[rquote=626983&tid=154496&author=unionised][rquote=626980&tid=154496&author=Tsjerk]A ...
28-11-2019 at 09:38
by: Tsjerk
Did I accidently make Titanium tetrachloride?
And what about putting a stopper in the round bottom and putting it in a cupboard for a couple of we ...
28-11-2019 at 01:46
by: Tsjerk
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