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NaNO3 to KNO3 and purify it
The solubility of potassium chloride is not very high. I suggest using a more soluble potassium salt ... |
20-4-2019 at 20:58
by: clearly_not_atara |
Preparation of Oleum by Use of Phosphoric Acid
Silicon carbide is apparently used for some of these kinds of extremely corrosive solutions.
http ... |
19-4-2019 at 12:35
by: clearly_not_atara |
Preparation of Acetic Anhydride
The separation of Ac2O from AcOH is the harder question. I can't think of anything but fractional di ... |
18-4-2019 at 14:23
by: clearly_not_atara |
Possible OTC, 'safe' methylating agents
It’s the Pinner reaction. But apparently HCl is required. However, the basic idea still has merit. ... |
17-4-2019 at 22:09
by: clearly_not_atara |
Possible OTC, 'safe' methylating agents
So I had a sudden realization.
Orthoesters are produced by reacting a nitrile with an alcohol in ... |
17-4-2019 at 16:07
by: clearly_not_atara |
Is there any way to make 3 amino phenol from salicamide?
Do you mean 2-aminophenol? I'm guessing you could probably pull that off. 3-aminophenol, though... t ... |
16-4-2019 at 13:49
by: clearly_not_atara |
Most extreme compounds known to man
Silver (still) has the highest bulk conductivity at room temperature of any [i]material[/i].
Gra ... |
16-4-2019 at 12:53
by: clearly_not_atara |
silver pyroglutamate and succinimide
There continues to be no easily accessible alternative to nitric acid for the dissolution of silver. ... |
10-4-2019 at 11:37
by: clearly_not_atara |
T-butanol from Citric acid?
If you're looking for an OTC source of t-butanol, consider instead the dietary supplement hydroxymet ... |
10-4-2019 at 11:19
by: clearly_not_atara |
Improving yields of TMP methylation?
I'm gonna disagree with bipolar about the inert atmosphere -- aldehydes are oxidized by air, and the ... |
7-4-2019 at 22:14
by: clearly_not_atara |
Making the most dense solution possible - that doesn't react with Cu or Al
Pumukli: I get the impression he's trying to gravimetrically separate aluminium powder from denser c ... |
7-4-2019 at 15:59
by: clearly_not_atara |
Potassium ethoxide
I think that you could probably get a pretty decent solution of KOEt by the rxn of K2CO3 with Mg(OEt ... |
7-4-2019 at 14:38
by: clearly_not_atara |
Sodium Ethoxide and anhydrous EtOH
When I discovered this thread, I, like everyone else, thought it was a huge breakthrough in the prep ... |
3-4-2019 at 12:01
by: clearly_not_atara |
Carbon disulfide synthesis (alternative routes)
[rquote=607003&tid=147199&author=12thealchemist]I went through Reaxys a few months ago and c ... |
2-4-2019 at 14:09
by: clearly_not_atara |
Preparation of S2Cl2
[rquote=606492&tid=78027&author=Feriman]Is it possible to dissolve sulfur in Sulfur Chloride ... |
26-3-2019 at 10:37
by: clearly_not_atara |
Nitration of 2-EH
2-ethylhexylnitrite seems plausible. It might have a GC/MS a little bit like the formate (NO and CHO ... |
22-3-2019 at 21:36
by: clearly_not_atara |
Any interesting uses for dimethylglyoxime?
If you convert both oximes to the iminyl tosylates, reduction with zinc amalgam might produce a shor ... |
22-3-2019 at 16:53
by: clearly_not_atara |
Preparation of S2Cl2
Adding sulfur is more than sufficient for converting SCl2 to S2Cl2. I'm not sure what is causing the ... |
22-3-2019 at 10:41
by: clearly_not_atara |
Anhydrous Zinc Chloride Attempted Synthesis
[quote]Sorry for ressurrecting this thread, but I'm looking at a synthesis that requires a small amo ... |
22-3-2019 at 10:38
by: clearly_not_atara |
What are some OTC thiols for thioketal formation?
Dodecanethiol bp: 268 C
1,3-propanedithiol bp: 169 C
Wiki: [i]"This liquid, which is readily ava ... |
21-3-2019 at 19:27
by: clearly_not_atara |
What are some OTC thiols for thioketal formation?
I've considered using alpha-lipoic acid, possibly after decarboxylating it somehow. Decarboxylated A ... |
20-3-2019 at 15:00
by: clearly_not_atara |
Preparation of S2Cl2
The dark red is probably SCl2, which is red; S2Cl2 is yellow-orange.
The product has a strong ten ... |
19-3-2019 at 13:36
by: clearly_not_atara |
Reducing copper hydroxide
FYI Rochelle salt can be made in situ by heating equimolar amounts of sodium bicarbonate and potassi ... |
15-3-2019 at 13:21
by: clearly_not_atara |
Cinnamaldehyde azeotrope with ethanol?
It simply happens that the human nose is extremely sensitive to cinnamaldehyde. Some contaminants ar ... |
13-3-2019 at 18:03
by: clearly_not_atara |
Disodium 1,2-ethanediolate Production
Just make sure it's protected from air, because alkoxides get oxidized pretty quickly -- and the rxn ... |
11-3-2019 at 14:22
by: clearly_not_atara |
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