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Low-Budget Homelab beginnings
China's glass is as good as anyone else's, and if you're willing to tolerate seconds you can get som ...
10-12-2017 at 12:47
by: JJay
Nitric Acid and Silver Nitrate
[rquote=499963&tid=27851&author=AJKOER]
First, mix up a concentrated solution of MgSO4 (Eps ...
10-12-2017 at 12:27
by: JJay
latest glassware purchase
I just noticed this, but one thing I do like about Gilbert Hardware's wash bottles is the size of th ...
9-12-2017 at 17:32
by: JJay
1,3 propanediol from D- panthenol
That's interesting. You might also consider the possibility that you have a sulfuric acid ester.
9-12-2017 at 08:54
by: JJay
latest glassware purchase
I ordered two of Gilbert Hardware's wash bottles in the 125 mL size, and they arrived today. I was s ...
9-12-2017 at 00:44
by: JJay
Fuming HNO3 distillation plan - suggestions?
I'm getting ready to make some nitric acid. I'm getting everything set up tonight, but I'll probably ...
7-12-2017 at 18:56
by: JJay
Acetaminophen purification issue
I've done this before and also noticed some weird colors, namely pink and a mottled grey color that ...
7-12-2017 at 08:03
by: JJay
What were your first experiments when you got in to this hobby?
I remember doing the red cabbage experiment as a child but didn't really get into it until I was in ...
6-12-2017 at 06:45
by: JJay
Quartz Tube Reactor
I'm getting these here pretty soon (they're quartz). They are just simple standard taper tubes, but ...
4-12-2017 at 15:40
by: JJay
Quartz Tube Reactor
[rquote=499413&tid=78702&author=aga]Do you have access to this design of quartzware, or the ...
4-12-2017 at 15:12
by: JJay
Quartz Tube Reactor
I've been working on a design for a quartz tube reactor. I'd like to be able to use it to make metal ...
4-12-2017 at 14:31
by: JJay
Fuming HNO3 distillation from drain cleaner + KNO3
Several Chem Player videos have music playing during reactions. This one for example: https://www.yo ...
3-12-2017 at 15:28
by: JJay
Fuming HNO3 distillation from drain cleaner + KNO3
I am planning on doing the same thing in the next few days, although I'll probably just aim for azeo ...
2-12-2017 at 17:09
by: JJay
latest glassware purchase
I got some 4L glass gallon jugs that formerly held fruit juice. I have several of these; I thoroughl ...
2-12-2017 at 16:55
by: JJay
Latest chemical order?
I got some sodium. It is crusty white with sodium oxides or sodium hydroxide, but it is also 100 gra ...
2-12-2017 at 16:39
by: JJay
Preparation of Thionyl Chloride
That is 10.2g more thionyl chloride than I have, and I think it's awesome. I really have no idea wha ...
30-11-2017 at 23:49
by: JJay
Reduce cinnamaldehyde to hydrocinnamaldehyde
I don't really suggest trying this, but you can make sodium amalgam by electrolysis of sodium chlori ...
30-11-2017 at 11:10
by: JJay
Reduce cinnamaldehyde to hydrocinnamaldehyde
I don't think NaBH4 can reduce that double bond by itself with the acetal in place. I'm actually not ...
30-11-2017 at 06:30
by: JJay
Reduce cinnamaldehyde to hydrocinnamaldehyde
Couldn't you protect the carbonyl by forming an acetal and then hydrolyze it after the reduction?
30-11-2017 at 06:15
by: JJay
Firefox
Yeah, hopefully Gary is ok... those hospital bills can get expensive.
29-11-2017 at 20:50
by: JJay
Firefox
Are these the same company?
29-11-2017 at 17:36
by: JJay
Firefox
Firefox is a U.S.-based pyro supplier that carries numerous pyro chemicals and a few uncommon items, ...
29-11-2017 at 13:21
by: JJay
Production of Cu (I) Cl with household chemicals. Problems.
[rquote=498949&tid=78599&author=Chemetix]Copper (II) sulphate + NaCl => Cu(II)Cl2

Cu( ...
29-11-2017 at 08:55
by: JJay
Firefox
I've been trying to reach Firefox to set up an account for the past couple of days, and they don't s ...
29-11-2017 at 02:01
by: JJay
Ethyl Iodide
Nicoderm's procedure using HCl looks quite easy if you have reagent grade hydrochloric acid on hand. ...
28-11-2017 at 13:56
by: JJay
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