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Pyrazine Synthesis? I'm doubtful of the reaction of ammonia with chloroacetone. Aside from the noxious properties of the ... |
27-2-2024 at 09:29 by: clearly_not_atara |
Uses of Gallium The key role of mercury in the chloralkali process is to dissolve sodium. But the interaction of sod ... |
26-2-2024 at 18:35 by: clearly_not_atara |
NO2 refusing to condense I think NO2 tends to be produced at pretty low pressure, and in the vapor phase, I'm pretty sure a m ... |
24-2-2024 at 12:51 by: clearly_not_atara |
How do I recrystallize ferric chloride? The easiest thing to do is to titrate the iron content of the solution by taking an aliquot of solut ... |
22-2-2024 at 19:37 by: clearly_not_atara |
Oxidation of styrene to phenylacetaldehyde Unfortunately this never worked out. The product is pretty unstable, and the reaction conditions for ... |
22-2-2024 at 15:08 by: clearly_not_atara |
How do I recrystallize ferric chloride? I think that [b]Bedlasky[/b]'s idea is a pretty good one.
[i]Ammonium chloroferrate was synthesi ... |
22-2-2024 at 10:27 by: clearly_not_atara |
Experiment with algebraic integers It's an interesting finding, but it's important to remember two things:
- sums and products of al ... |
22-2-2024 at 06:25 by: clearly_not_atara |
How hazardous is fluorine chemistry? [rquote=690961&tid=160167&author=unionised][rquote=690923&tid=160167&author=clearly_ ... |
17-2-2024 at 16:32 by: clearly_not_atara |
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde For comparison:
http://orgsyn.org/demo.aspx?prep=cv1p0155
Note that the o-chloro makes the rea ... |
16-2-2024 at 12:40 by: clearly_not_atara |
How hazardous is fluorine chemistry? It's a pretty broad question, isn't it? As Texium emphasized, HF is extremely dangerous. Many fluori ... |
14-2-2024 at 11:35 by: clearly_not_atara |
URGENT - To Vesp https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7304568/
Describes the direct reaction of hydroxylam ... |
13-2-2024 at 06:26 by: clearly_not_atara |
Acetic anhydride preparation I can't edit that post anymore, but I wanted to add that in the absence of phthalic acid, a high-boi ... |
11-2-2024 at 22:21 by: clearly_not_atara |
Looking for ideas for a new Synthesis Open Access Platform I think I would avoid trying to be all things to all people. One thing I've thought would be useful ... |
10-2-2024 at 18:23 by: clearly_not_atara |
Acetic anhydride preparation Loptr: It was discussed on the previous page. In order to better keep track of the enormous amount o ... |
10-2-2024 at 17:30 by: clearly_not_atara |
Acetic anhydride preparation S2Cl2 is not so bad itself, but it's infamous for ruining any container you keep it in. So you proba ... |
9-2-2024 at 14:22 by: clearly_not_atara |
Acetic anhydride preparation I just don't think it's considered interesting. Mostly we're interested in preparing acetic anhydrid ... |
9-2-2024 at 08:18 by: clearly_not_atara |
URGENT - To Vesp Ha! And here I thought I had finally bored everyone to death |
9-2-2024 at 05:48 by: clearly_not_atara |
Questions in electroplating I'm confused? Isn't the anode supposed to corrode? It's pitting because it's not noble enough to evo ... |
8-2-2024 at 18:58 by: clearly_not_atara |
Detonation Velocity of organic explosive cannot exceed 11 Km/s It appears that this assertion may have been defeated in an unexpected manner. The novel superhard m ... |
8-2-2024 at 09:14 by: clearly_not_atara |
Can KBH4 substitute NaBH4 in ethanol/methanolic solutions for reduction of ketones to alcohol. ^I think you'd have a better time contributing to the Sciencemadness Wiki. Wikipedia usually wants " ... |
6-2-2024 at 21:06 by: clearly_not_atara |
Praparation of Nitromethane I think a key reason is that it's the easiest saturated aliphatic nitro compound to make ![:P](./images/smilies/tongue.gif)
Unles ... |
6-2-2024 at 17:57 by: clearly_not_atara |
Eutectic salts for heating bath alternative Since the methanesulfonates can substitute for nitrate in dissolving silver, I thought I would look ... |
2-2-2024 at 16:21 by: clearly_not_atara |
S2Cl2 by chlorination with CuCl2 in MeCN? Because of the formation of the acetonitrile-Cu+ complex, copper (II) is more strongly oxidizing in ... |
2-2-2024 at 09:29 by: clearly_not_atara |
A failed attempt at p-hydroxybenzoic acid Orgsyn says 230 C. Your procedure says 225 F. This discrepancy is alarming.
EDIT: Oh, I see. You ... |
30-1-2024 at 08:47 by: clearly_not_atara |
Synthesis of Chloroacetic acid You shouldn't need any light with a sulfur catalyst, in this case the mechanism is fully ionic and n ... |
30-1-2024 at 08:45 by: clearly_not_atara |
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