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Pyrazine Synthesis?
I'm doubtful of the reaction of ammonia with chloroacetone. Aside from the noxious properties of the ... |
27-2-2024 at 09:29
by: clearly_not_atara |
Uses of Gallium
The key role of mercury in the chloralkali process is to dissolve sodium. But the interaction of sod ... |
26-2-2024 at 18:35
by: clearly_not_atara |
NO2 refusing to condense
I think NO2 tends to be produced at pretty low pressure, and in the vapor phase, I'm pretty sure a m ... |
24-2-2024 at 12:51
by: clearly_not_atara |
How do I recrystallize ferric chloride?
The easiest thing to do is to titrate the iron content of the solution by taking an aliquot of solut ... |
22-2-2024 at 19:37
by: clearly_not_atara |
Oxidation of styrene to phenylacetaldehyde
Unfortunately this never worked out. The product is pretty unstable, and the reaction conditions for ... |
22-2-2024 at 15:08
by: clearly_not_atara |
How do I recrystallize ferric chloride?
I think that [b]Bedlasky[/b]'s idea is a pretty good one.
[i]Ammonium chloroferrate was synthesi ... |
22-2-2024 at 10:27
by: clearly_not_atara |
Experiment with algebraic integers
It's an interesting finding, but it's important to remember two things:
- sums and products of al ... |
22-2-2024 at 06:25
by: clearly_not_atara |
How hazardous is fluorine chemistry?
[rquote=690961&tid=160167&author=unionised][rquote=690923&tid=160167&author=clearly_ ... |
17-2-2024 at 16:32
by: clearly_not_atara |
The Synthesis of Benzoyl Chloride via The Sulfur Catalyzed Chlorination of Benzaldehyde
For comparison:
http://orgsyn.org/demo.aspx?prep=cv1p0155
Note that the o-chloro makes the rea ... |
16-2-2024 at 12:40
by: clearly_not_atara |
How hazardous is fluorine chemistry?
It's a pretty broad question, isn't it? As Texium emphasized, HF is extremely dangerous. Many fluori ... |
14-2-2024 at 11:35
by: clearly_not_atara |
URGENT - To Vesp
https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7304568/
Describes the direct reaction of hydroxylam ... |
13-2-2024 at 06:26
by: clearly_not_atara |
Acetic anhydride preparation
I can't edit that post anymore, but I wanted to add that in the absence of phthalic acid, a high-boi ... |
11-2-2024 at 22:21
by: clearly_not_atara |
Looking for ideas for a new Synthesis Open Access Platform
I think I would avoid trying to be all things to all people. One thing I've thought would be useful ... |
10-2-2024 at 18:23
by: clearly_not_atara |
Acetic anhydride preparation
Loptr: It was discussed on the previous page. In order to better keep track of the enormous amount o ... |
10-2-2024 at 17:30
by: clearly_not_atara |
Acetic anhydride preparation
S2Cl2 is not so bad itself, but it's infamous for ruining any container you keep it in. So you proba ... |
9-2-2024 at 14:22
by: clearly_not_atara |
Acetic anhydride preparation
I just don't think it's considered interesting. Mostly we're interested in preparing acetic anhydrid ... |
9-2-2024 at 08:18
by: clearly_not_atara |
URGENT - To Vesp
Ha! And here I thought I had finally bored everyone to death |
9-2-2024 at 05:48
by: clearly_not_atara |
Questions in electroplating
I'm confused? Isn't the anode supposed to corrode? It's pitting because it's not noble enough to evo ... |
8-2-2024 at 18:58
by: clearly_not_atara |
Detonation Velocity of organic explosive cannot exceed 11 Km/s
It appears that this assertion may have been defeated in an unexpected manner. The novel superhard m ... |
8-2-2024 at 09:14
by: clearly_not_atara |
Can KBH4 substitute NaBH4 in ethanol/methanolic solutions for reduction of ketones to alcohol.
^I think you'd have a better time contributing to the Sciencemadness Wiki. Wikipedia usually wants " ... |
6-2-2024 at 21:06
by: clearly_not_atara |
Praparation of Nitromethane
I think a key reason is that it's the easiest saturated aliphatic nitro compound to make 
Unles ... |
6-2-2024 at 17:57
by: clearly_not_atara |
Eutectic salts for heating bath alternative
Since the methanesulfonates can substitute for nitrate in dissolving silver, I thought I would look ... |
2-2-2024 at 16:21
by: clearly_not_atara |
S2Cl2 by chlorination with CuCl2 in MeCN?
Because of the formation of the acetonitrile-Cu+ complex, copper (II) is more strongly oxidizing in ... |
2-2-2024 at 09:29
by: clearly_not_atara |
A failed attempt at p-hydroxybenzoic acid
Orgsyn says 230 C. Your procedure says 225 F. This discrepancy is alarming.
EDIT: Oh, I see. You ... |
30-1-2024 at 08:47
by: clearly_not_atara |
Synthesis of Chloroacetic acid
You shouldn't need any light with a sulfur catalyst, in this case the mechanism is fully ionic and n ... |
30-1-2024 at 08:45
by: clearly_not_atara |
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