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Realistic Microwave Modifications
I am actually looking for a quartz tube with a flange - to put through a hole in the top of the oven ... |
22-4-2013 at 02:32
by: aliced25 |
Realistic Microwave Modifications
I've been looking around at the various microwave modifications that have been suggested, and to be ... |
22-4-2013 at 00:17
by: aliced25 |
Synthesis of propanamide
Quick tip - ammonia is a base, propionic acid is an acid surprisingly enough. It can be used to neut ... |
21-4-2013 at 20:10
by: aliced25 |
Preparation of elemental phosphorus
Maybe activated charcoal and polyphosphoric acid? It should be easy enough to remove the door and ch ... |
21-4-2013 at 14:55
by: aliced25 |
Acetic anhydride preparation
[rquote=118968&tid=9&author=Sauron]Yes, S.C> I figured that was what you meant. As it hap ... |
21-4-2013 at 01:42
by: aliced25 |
Preparation of elemental phosphorus
What? To polyphosphoric acid from Ammonium Dihydrogen Phosphate? Too many times to count. My suggest ... |
21-4-2013 at 01:20
by: aliced25 |
Preparation of elemental phosphorus
Could I make an uneducated suggestion here? If the purpose is to liquify the charge with a high phos ... |
20-4-2013 at 01:40
by: aliced25 |
ethyl acetate - non-acetone nail polish remover
If you add a salt, say calcium chloride, shake the piss out of the mixture, add more CaCl2 until you ... |
24-4-2012 at 01:30
by: aliced25 |
Catalytic oxidation of sulfurous acid
weiming - there is a paper online about the freeze-thaw cycles with sulfurous and nitrous acids, to ... |
17-4-2012 at 08:30
by: aliced25 |
Peracetic Acid Preparation
[rquote=147971&tid=11862&author=Baphomet]Last night I tried to make peracetic acid by reacti ... |
5-4-2012 at 06:52
by: aliced25 |
First attempt at the rearrangement of 2-phenylpropanal
Oxidation of an aldehyde without touching a ketone, dunno... Perhaps [url=http://en.wikipedia.org/wi ... |
5-4-2012 at 04:12
by: aliced25 |
Making Lead(IV) acetate
The attached paper, from IUPAC, goes into quite a description of the difficulties surrounding prepar ... |
21-3-2012 at 16:41
by: aliced25 |
Glyoxylic Acid via Glycolic Acid Oxidation (Questions)
There is also the oxidative cleavage of tartaric acid (or esters thereof) by either lead tetraacetat ... |
21-3-2012 at 06:30
by: aliced25 |
Sulphuric Acid in Australia
[rquote=218633&tid=17244&author=Phthalic Acid]Thanks for the info plante1999! You seem to ha ... |
20-3-2012 at 20:29
by: aliced25 |
Cold extraction of piperine from black pepper
I do hate to ask, but why is the piperidine gaseous? From my recollection, it forms a dark, oil liqu ... |
20-3-2012 at 13:46
by: aliced25 |
UCLA prof and UC system face felony charges after lab accident
[rquote=231560&tid=18374&author=bbartlog]This is a matter for a civil suit at most. Criminal ... |
12-3-2012 at 03:42
by: aliced25 |
furfural
Here is some more - interestingly enough HCl or H3PO4 are the acids of choice for this procedure - w ... |
12-3-2012 at 01:38
by: aliced25 |
Sodium Ethoxide and anhydrous EtOH
Here's an idea from left-field
Add some aluminium -
I'm thinking that the NaOH will react wit ... |
6-3-2012 at 03:59
by: aliced25 |
Propiophenone rearrangement
[rquote=32503&tid=3006&author=Organikum]
Original reference is:
J. Pharm. Soc. Japan 73, ... |
20-2-2012 at 01:55
by: aliced25 |
Ethylamine Synthesis
Yep, nitroethane is the simplest of materials to access Ain't no issues with
the synthesis of that ... |
13-2-2012 at 00:52
by: aliced25 |
do-it-yourself nuclear magnetic resonance spectroscopy
According to FEMM if one were to utilize a certain design (using 25mm cubes as well as other compone ... |
2-12-2011 at 20:13
by: aliced25 |
desktop NMR?
Be a bloody sight smaller soon with luck
Anyone interested in a prototype modified halbach ... |
16-11-2011 at 02:02
by: aliced25 |
do-it-yourself nuclear magnetic resonance spectroscopy
Ok, looking very seriously at this now, as stated in several articles, we aren't going to be transmi ... |
10-11-2011 at 04:09
by: aliced25 |
DIY Atom Smasher
Ok, looking at the linear accelerators and the use of more and more stages in order to double the sp ... |
5-11-2011 at 15:39
by: aliced25 |
DIY Atom Smasher
Actually ran into the fusors a while back and thought that was plenty mad enough (accessing the deut ... |
3-11-2011 at 15:05
by: aliced25 |
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