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reduction with HI without phosphorous I remember reading something about using aluminum a while back on another forum... as I recall, it w ...	8-8-2020 at 19:22 by: JJay
(safer) fluorination of benzaldehyde? Why not start with toluidines? You could diazotize and react with fluoroboric acid, then add a carbo ...	6-8-2020 at 18:07 by: JJay
Latest chemical order? I have been meaning to get some lithium.... It's not cheap, but a little goes a long way.	6-8-2020 at 17:43 by: JJay
jacketless condenser An air condenser? https://www.ebay.com/itm/600mm-24-2-9-Air-Condenser-Heat-Exchange-Tube-Lab-Glasswa ...	6-8-2020 at 17:40 by: JJay
What Happened in Beirut A small tactical nuclear device would have a blast radius about 2-3x larger. But the explosion is ki ...	5-8-2020 at 06:59 by: JJay
Latest chemical order? Yeah, it's pretty easy to find, or at least it was... I don't see why anyone would refuse to sell it ...	4-8-2020 at 18:37 by: JJay
Chromate/Dichromate thermite [rquote=642190&tid=155917&author=Nitrosio]https://www.researchgate.net/publication/236556739 ...	4-8-2020 at 05:34 by: JJay
Chromate/Dichromate thermite Offhand, I see Schlessinger's Inorganic Laboratory Preparations in the Sciencemadness library contai ...	3-8-2020 at 14:44 by: JJay
Chromate/Dichromate thermite Potassium dichromate is better for thermite because it is not hygroscopic. As I recall, it's typica ...	3-8-2020 at 03:41 by: JJay
Making Reducing agents and oxidizing agents Pyrophoric nickel (from pyrolysis of nickel oxylate): https://www.youtube.com/watch?v=4gO92eqQcB4 A ...	2-8-2020 at 16:54 by: JJay
Latest chemical order? Tribasic calcium phosphate. I am going to try to reduce it with aluminum.	2-8-2020 at 10:24 by: JJay
Oxidation of styrene to phenylacetaldehyde Cool. This is actually second on my list of syntheses to try when I get a new lab space. I believe y ...	26-7-2020 at 19:05 by: JJay
Oxidation of styrene to phenylacetaldehyde How do you know that you have successfully synthesized the epoxide? For that matter, how do you know ...	25-7-2020 at 09:35 by: JJay
Why doesn't anyone use glove boxes for things like fluorine? I'm told that glove boxes are used for phosgene in graduate research labs. It's slightly more toxic ...	22-7-2020 at 16:54 by: JJay
Makeshift way of routing sulfur dioxide/gasses? I would think you could draw air and sulfur dioxide through an apparatus with an aspirator. I hav ...	22-7-2020 at 16:51 by: JJay
Using a 24/40 flask with my other 24/29 glassware I personally prefer 24/29 flasks and 24/40 everything else. I have a combination of both sizes of bo ...	18-7-2020 at 12:36 by: JJay
Avoiding Explosions with Fumehood's Inline Fan -Spark Hazard Most ventilation fans that are intended for removing fumes are designed to keep the motor outside of ...	18-7-2020 at 02:20 by: JJay
Can you make methanol from formic acid? It's possible with lithium aluminum hydride. It can probably be done with nickel boride. I don't ...	11-7-2020 at 12:38 by: JJay
Lab and insects [rquote=640277&tid=155757&author=B(a)P][rquote=640226&tid=155757&author=JJay]I usual ...	10-7-2020 at 08:05 by: JJay
Lab and insects I usually have more luck with traps than poisons unless I can actually spray the pests directly. Fly ...	9-7-2020 at 16:50 by: JJay
Oxidation of aldehydes to carboxylic acids? [rquote=640103&tid=155740&author=DraconicAcid]I don't know- I've been using hydrogen peroxid ...	7-7-2020 at 18:57 by: JJay
Oxidation of aldehydes to carboxylic acids? [rquote=640100&tid=155740&author=DraconicAcid][rquote=640090&tid=155740&author=JJay] ...	7-7-2020 at 12:31 by: JJay
Oxidation of aldehydes to carboxylic acids? Are there any selective aldehyde oxidation reactions that work generally and don't oxidize primary a ...	7-7-2020 at 11:24 by: JJay
Anhydrous Aluminum Chloride prepration It's probably possible to get Al-CuCl2 to work to produce useful amounts of AlCl3, but as far as I a ...	7-7-2020 at 09:28 by: JJay
Oxidation of aldehydes to carboxylic acids? Pinnick oxidation?	7-7-2020 at 04:56 by: JJay
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