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Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]For the washing of the extracted benz. is it DH2O only? thanks[/quote]
I have used both plai ... |
13-2-2007 at 09:27
by: Hilski |
A dumb question regarding ratios in general
Thanks for the replies. It's good to know that I wasn't missing something obvious that would have t ... |
11-2-2007 at 19:19
by: Hilski |
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]And then evap the MnSO4 solution to obtain the powder correct? because I did and got a faitly ... |
10-2-2007 at 21:29
by: Hilski |
A dumb question regarding ratios in general
I have noticed that in a lot of the older patents I have read through that many of them use the term ... |
10-2-2007 at 21:16
by: Hilski |
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
Unless huge quantities are needed, oxidation of toluene by manganese compounds would be the simplest ... |
9-2-2007 at 19:41
by: Hilski |
Morgellons sindrome
[quote]Over the last few years there have been quite a few TV news stories from all over the country ... |
6-2-2007 at 10:10
by: Hilski |
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]Those red plastic press on cover " coffee cans " that
13 ounces of coffee is sold , are HDPE ... |
1-2-2007 at 11:14
by: Hilski |
Morgellons sindrome
[quote]Where is the video of this stuff ??? [/quote]
Over the last few years there have been quite ... |
1-2-2007 at 07:26
by: Hilski |
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
Those are all good ideas, and the type of thing I would need to address if scaling up. But one thin ... |
1-2-2007 at 05:58
by: Hilski |
Some experiments
As I mentioned in another thread, I would like to set up a functional electrolytic cell that would ... |
31-1-2007 at 17:41
by: Hilski |
toluene --> benzaldehyde
I distilled the aldehyde from the reaction with the brownish Mn alum, and the yields were actually a ... |
31-1-2007 at 17:28
by: Hilski |
Tyvek may be the ticket
[quote]Those unglazed clay , terra cotta wine coolers don't have a drain hole IIRC , and you could p ... |
29-1-2007 at 11:20
by: Hilski |
toluene --> benzaldehyde
I think I have all the stuff I need to try this on a smaller scale. If I am successful, I will take ... |
27-1-2007 at 06:54
by: Hilski |
toluene --> benzaldehyde
I wonder if the need for a diaphragm to efficiently produce the persulfate can be done away with if ... |
26-1-2007 at 22:06
by: Hilski |
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
[quote]to see if anyone allowed the regeneration
to keep running longer than required to produce th ... |
26-1-2007 at 15:10
by: Hilski |
PC PSU to laboratory PSU
[quote]We invent new stuff here often enough , that when I google stuff to learn more , often what I ... |
26-1-2007 at 13:22
by: Hilski |
Acid in Large jug, how do I use a small amount?
Most all grocery and department stores have them in the kitchen gadget section, with the measuring c ... |
26-1-2007 at 13:19
by: Hilski |
Acid in Large jug, how do I use a small amount?
Big syringes like the ones used for injecting marinades into meats come in handy for these sorts of ... |
26-1-2007 at 13:13
by: Hilski |
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
I guess all in all, passing current through a non-divided cell for 24 hours isn't really all that ba ... |
26-1-2007 at 12:54
by: Hilski |
Amines in Acid/base extraction
Methylamine freebase is a gas. |
26-1-2007 at 09:50
by: Hilski |
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde
Thanks for that post, Roscoe.
I had been thinking about ways one could go about regenerating the ... |
25-1-2007 at 20:22
by: Hilski |
bitter almond benzaldehyde
[quote]And they can forget the overhyped biosynthesis with benzaldehyde and acetaldehyde, that was n ... |
24-1-2007 at 07:18
by: Hilski |
Possibly another (easy) oxidizer for toluene to benzaldehyde?
Here is an interesting patent that utilizes a manganic oxidizer made from oxidizing a mixture of man ... |
23-1-2007 at 15:21
by: Hilski |
Hydroiodic acid made in situ
[quote]My question: can the HI be made with I2, P and S in water? I have a non crank related applica ... |
22-1-2007 at 19:33
by: Hilski |
Effectiveness of hexane as a solvent for benzaldehyde.
[quote]It will work fine but has maybe half the dissolving power
as benzene or toluene so use more. ... |
22-1-2007 at 02:36
by: Hilski |
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