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toluene --> benzaldehyde 1 kg cinnamon oil feedstock
[img]http://www.sciencemadness.org/scipics/P4160045.JPG[/img]
Either ... |
17-4-2013 at 06:41 by: CycloKnight |
toluene --> benzaldehyde Volumetric flask making itself useful
[img]http://www.sciencemadness.org/scipics/P4170061.JPG[/img] ... |
17-4-2013 at 06:33 by: CycloKnight |
toluene --> benzaldehyde General setup:
[img]http://www.sciencemadness.org/scipics/P4160049.JPG[/img]
Between the free oi ... |
17-4-2013 at 06:23 by: CycloKnight |
toluene --> benzaldehyde No problem, any and all input appreciated.
I plan to first run through the 1 kg of oil using th ... |
16-4-2013 at 08:52 by: CycloKnight |
toluene --> benzaldehyde Not sure what about a "peach style", but I can do a CycloKnight style retro-aldol follow up to my ea ... |
15-4-2013 at 09:58 by: CycloKnight |
toluene --> benzaldehyde Sometime this week I'll be revisiting the cinnamon oil to benzaldehyde method utilizing insitu steam ... |
15-4-2013 at 06:29 by: CycloKnight |
toluene --> benzaldehyde [rquote=232141&tid=2223&author=questions]I love benzaldehyde, not just for it's broad uses, ... |
17-2-2012 at 06:15 by: CycloKnight |
Manganous-Ammonium alum and derivatives for use of toluene oxidation to benzaldehyde Nice work Hilski, lots of potential with this manganous-alum route. Great pics BTW !
This thread su ... |
13-2-2007 at 15:31 by: CycloKnight |
toluene --> benzaldehyde [quote] CycloKnight, I don´t understand why you use a not even insulated Vigreux in your steamdisti ... |
11-8-2006 at 02:46 by: CycloKnight |
Amino alcohol via Akabori, trial run Sorry maybe I should have explained that better.
I was only referring to aerosol carry over. Using ... |
10-8-2006 at 13:13 by: CycloKnight |
Amino alcohol via Akabori, trial run [quote][i]Originally posted by daFlo[/i]
why using a column, when boiling off the water? the PPA is ... |
11-7-2006 at 21:24 by: CycloKnight |
Amino alcohol via Akabori, trial run [quote][i]Originally posted by Maja[/i]
From one forum, one guy told that benzaldehyde can be repla ... |
8-7-2006 at 16:20 by: CycloKnight |
Update The yield of PPA given in the previous reaction was no more than about 50% of the final crystallised ... |
21-6-2006 at 23:25 by: CycloKnight |
Product composition. The freebase hasn't yet been isolated on its own in sufficient purity for a mp test. Any suggestion( ... |
10-6-2006 at 19:42 by: CycloKnight |
Blaster, nice pictures ! I recently made up a small batch of this powder, and I'm quite impressed with the results .
The m ... |
10-6-2006 at 14:56 by: CycloKnight |
Akabori runs ........only the reports of failure that were posted a couple of years ago by somebody named 'DRIVEN ... |
10-6-2006 at 13:56 by: CycloKnight |
NI3 iirc Seymour Lecker mentions this explosive in his book "improvised explosives" as one of the 10 exp ... |
9-6-2006 at 18:07 by: CycloKnight |
Amino alcohol via Akabori, trial run Recently I’ve been experimenting with the Akabori reaction, just curious to see if the process for ... |
8-6-2006 at 11:40 by: CycloKnight |
Acetaldehyde There is another route to acetaldehyde that I didn't see mentioned in the posts above.
This is the ... |
7-6-2006 at 12:28 by: CycloKnight |
Cinnamon oil to benzaldehyde update. Hi peeps, been off the forum a good while but its good to be back .
I’ve significantly impro ... |
6-6-2006 at 11:47 by: CycloKnight |
toluene --> benzaldehyde [quote][i]Originally posted by groaner[/i]
You are certainly right there bio2. Murphy is always lur ... |
2-5-2006 at 00:40 by: CycloKnight |
Recent outage I was beginning to fear the worst!
So, so relieved it was just temporary.
BTW, is it just me or ... |
2-3-2005 at 01:29 by: CycloKnight |
Another leap forward... Very good work psychokitty!
I don't know how you found that, but that looks pretty darned goo ... |
13-2-2005 at 02:06 by: CycloKnight |
Not too shabby! Well, there you have it folks - the end of chapter 1. Now go forth and be fruitful!
I would be ve ... |
11-2-2005 at 15:18 by: CycloKnight |
toluene --> benzaldehyde Okay, this is what the mix looks like after the steam distillation.
http://www.sciencemadness.org/s ... |
11-2-2005 at 14:12 by: CycloKnight |
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