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My Synthesis of Nitroethane via a AgNO2 Packed Column
JW: I'm not sure why the anethole method is so unpopular.
The pseudonitrosite reaction for nitra ... |
19-4-2020 at 14:39
by: clearly_not_atara |
Use For Menthol?
You can eliminate the alcohol with dilute H2SO4 to 3-menthene. There is probably a way to convert th ... |
19-4-2020 at 11:16
by: clearly_not_atara |
My Synthesis of Nitroethane via a AgNO2 Packed Column
[quote]The holy grail is finding the conditions or OTC solvent that can do this with sodium nitrite. ... |
19-4-2020 at 09:28
by: clearly_not_atara |
Cheap OTC DCM in the USA?
[quote]Hmm, I wonder if my local home depot would actually stock that. There's definitely no 'pool' ... |
19-4-2020 at 09:13
by: clearly_not_atara |
pyrex vs PYREX
Also, I'm pretty sure that the true borosilicate pyrex tends to be thinner than the cheaper soda-lim ... |
18-4-2020 at 15:16
by: clearly_not_atara |
Was shipped wrong item, got a bottle of glucose instead of choline chloride. Anything cool I can do with glucose?
You can make levulinic acid from sucrose!
But you should complain. You bought a high value produc ... |
18-4-2020 at 08:56
by: clearly_not_atara |
Was shipped wrong item, got a bottle of glucose instead of choline chloride. Anything cool I can do with glucose?
Reduction of glucose gives sorbitol.
Sorbitol can then be converted to sorbitan or isosorbide by ... |
17-4-2020 at 22:06
by: clearly_not_atara |
TiCL3 made at home?
TiCl3 is a unique reducing agent in organic chemistry; it tends to reduce nucleophilic substrates, w ... |
17-4-2020 at 21:22
by: clearly_not_atara |
Cheap OTC DCM in the USA?
20-30% ether I think you could work with... 10% sucks. Ether can dissolve in seventeen parts water, ... |
17-4-2020 at 08:40
by: clearly_not_atara |
Thiourea dioxide
In particular, thiourea dioxide is soluble in alcohols, as I recall.
That should make it much ea ... |
17-4-2020 at 08:17
by: clearly_not_atara |
Cheap OTC DCM in the USA?
Chloroform is easily synthesized if hypochlorites are available. However, its instability and toxici ... |
16-4-2020 at 10:27
by: clearly_not_atara |
Iodate to chlorate?
What does this have to do with iodate?
But anyway, this is pretty much impossible, and wouldn't b ... |
15-4-2020 at 13:14
by: clearly_not_atara |
Coronavirus pandemic model
S_S: You don't consider the discovery of penicillin, sulfanilamide, streptomycin, chloramphenicol, i ... |
15-4-2020 at 11:20
by: clearly_not_atara |
Nitromethane torch?
Nitromethane also seems like a particularly poor choice of fuel for a torch simply because of its po ... |
15-4-2020 at 08:25
by: clearly_not_atara |
Coronavirus pandemic model
[rquote=634018&tid=155170&author=sodium_stearate]In short, we likely will never know the tru ... |
14-4-2020 at 13:09
by: clearly_not_atara |
Benzyl alcohol + FeCl₃ in HCl → toluene (or benzene)???
Sounds like benzyl chloride, especially if the smell was sharp and acidic. Since you were using pero ... |
13-4-2020 at 11:59
by: clearly_not_atara |
Trimethyl Phosphate
S.C.Wack: it seems like they replace "Ba2" with "Ag2" on the next page. Therefore I would consider t ... |
13-4-2020 at 08:44
by: clearly_not_atara |
The Short Questions Thread (4)
Does the Sandmeyer reaction work for alkyl fluorides with alkali nitrite and hydrofluoric acid? All ... |
12-4-2020 at 10:18
by: clearly_not_atara |
Political message in signature?
MineMan: Dude's signature was really intense. I guess if he had just said "Free Hong Kong" we might ... |
12-4-2020 at 09:27
by: clearly_not_atara |
nitroethane synthesis question
Propanal can be made from propylene glycol and halogenated with CuCl2 or CuBr2. Further oxidation wi ... |
10-4-2020 at 19:50
by: clearly_not_atara |
nitroethane synthesis question
The problem is that the formation of nitrite esters actually results in the destruction of the forme ... |
10-4-2020 at 19:31
by: clearly_not_atara |
nitroethane synthesis question
No. The carboxylate group at alpha position is necessary to suppress the formation of the alkyl nitr ... |
10-4-2020 at 11:22
by: clearly_not_atara |
The structure of benzene has been determined
The 126 "dimensions" are not dimensions of space but [i]coordinates[/i] of particles which are model ... |
7-4-2020 at 15:19
by: clearly_not_atara |
Diazonium salts from NO2 instead of NaNO2+HCl ?
The fact that you are even considering this suggests that you do not have nearly enough respect for ... |
7-4-2020 at 14:10
by: clearly_not_atara |
About some details of the Birkeland-Eyde nitric acid synthesis
The preparation of ortho-nitrobenzaldehyde is given on Orgsyn:
http://www.orgsyn.org/demo.aspx?prep ... |
5-4-2020 at 13:02
by: clearly_not_atara |
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