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synthesis of O-nitroaniline
Hi nitro-genes, I presume you haven't got any aniline as this would be easier, avoiding the chloro g ...
23-3-2018 at 10:11
by: Boffis
hemicellulose solvents, glycerine and alkali react?
I'm no expert on sugar/wood chemistry but I can see a few problems and misconceptions in your experi ...
20-3-2018 at 04:19
by: Boffis
Decarboxylation of Glycine to Methylamine?!
@ Diball; when you heat glycine with glycols you get cyclitisation to to piperazine-2,5-dione. Alani ...
15-3-2018 at 13:23
by: Boffis
paradiclorobenzene - possible degradation of
Hi Elemental Phosphorus; I prepared a large amount of the mononitro compound using standard 68% nitr ...
14-3-2018 at 05:39
by: Boffis
Antimony toxicity?
Why would anyone just randomly go and have a test for heavy metal poisoning. There is clearly more t ...
10-3-2018 at 12:11
by: Boffis
Experiments with Vanillin and Ethyl Vanillin Ideas
You can fuse it with KOH and prepare 3,4-dihydroxybenzoic acid (pyrocatechuic acid), reduce it with ...
8-3-2018 at 07:14
by: Boffis
nitration of xylene using HNO3/DCM mixture
@mackolol, I have been reading up on this subject. From what I can find in papers by Strazzolini et ...
8-3-2018 at 06:03
by: Boffis
DDNP & related compounds: The über thread!
Woow nitro-genes! This method certainly beats the pants of the sulphide methods, can't wait to give ...
4-3-2018 at 23:29
by: Boffis
Copper Ferrocyanide, Copper Hydrogen Ferrocyanide Tetrahydrate, and Sodium Copper Hydrogen Ferrocyanide
For hard copies try Amazon. A lot of really old c100 years or more are now available as facsimile re ...
4-3-2018 at 22:45
by: Boffis
Copper Ferrocyanide, Copper Hydrogen Ferrocyanide Tetrahydrate, and Sodium Copper Hydrogen Ferrocyanide
I have a large number of basic chemistry books. When I am drawn into a new field I simply read-up on ...
4-3-2018 at 11:42
by: Boffis
Sodium Hydroxide and Nickel
Nickel will not dissolve in sodium hydroxide solution. In fact we use nickel crucibles for NaOH fusi ...
4-3-2018 at 01:45
by: Boffis
Reaction between copper sulfate and ferric chloride
@Ajoker, your post is complete bollocks.

IF your solutions are dilute or neutral slow hydrolysis ...
4-3-2018 at 01:38
by: Boffis
Copper Ferrocyanide, Copper Hydrogen Ferrocyanide Tetrahydrate, and Sodium Copper Hydrogen Ferrocyanide
I think that all of you question will be answered by reading:

The chemistry of Cyanogen compounds ...
3-3-2018 at 11:01
by: Boffis
paradiclorobenzene - possible degradation of
Well, the first problem I see is the presence of acetone as a solvent in the presence of sodium hydr ...
2-3-2018 at 10:23
by: Boffis
Nitroethane from ethylsulfate, Desseigne variation.
@Crowfjord. Thankyou very much for the reference and your comments. I think they pretty much rule ou ...
2-3-2018 at 09:53
by: Boffis
Reaction between copper sulfate and ferric chloride
This question has been asked a hundred times before in some form or other. They are both highly disa ...
2-3-2018 at 07:54
by: Boffis
Reaction evolving H2 or CO gas, need help identifying
I think you are all out to lunch! Woelen I suspect is closest. It is very unlikely that you are goin ...
1-3-2018 at 22:57
by: Boffis
Low Temp Decomposition of Sodium Sulfate ?
The colour is due to impurities in your "super cheap" reagents, most likely iron. After filtering of ...
1-3-2018 at 22:16
by: Boffis
Nitroethane from ethylsulfate, Desseigne variation.
@clear_not_atara;? do you mean tert-nitrobutane? I don't know. If the reaction works once then I sup ...
1-3-2018 at 08:00
by: Boffis
Dinitroresorcinol preparation
@roXefeller, that sound pretty promising, it will be interesting to see what melting point you get f ...
1-3-2018 at 07:09
by: Boffis
Practical chemistry
@Akhil Jain, If you have the metals (Cr Fe etc) in sulphuric acid solution you can simply boil it an ...
28-2-2018 at 22:29
by: Boffis
Preparation of 1,4-Dibromobutane
@LearnedAmateur; that's basically my reason for asking the question. I notice that some aliphatic ha ...
28-2-2018 at 12:58
by: Boffis
Nitroethane from ethylsulfate, Desseigne variation.
I have a silly question!

Since nitromethane reacts with formaldehyde in a base catalyzed system t ...
28-2-2018 at 12:37
by: Boffis
Preparation of 1,4-Dibromobutane
Does anyone know if it is possible to produce butadiene gas by say dropping 1,4-dibromobutane into s ...
28-2-2018 at 12:09
by: Boffis
Pseudonitrosites
[rquote=50423&tid=2960&author=Axt]From the attachment three posts up.

"Franklin and Willt ...
28-2-2018 at 09:55
by: Boffis
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