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Ideas for iron powder The reduction of internal nitroalkenes to ketones with iron powder and hydrochloric acid is well-kno ...	24-8-2020 at 13:34 by: clearly_not_atara
Small scale production of H2SO4 in the amateur lab By far the simplest method I have heard of is to use the disproportionation of potassium bisulfate i ...	17-8-2020 at 06:57 by: clearly_not_atara
Alternative reducing agent to LAH Lithium aluminum hydride Red-Al solution sells for cheaper by weight than NaBH4 powder, but when you calculate the cost per m ...	13-8-2020 at 05:40 by: clearly_not_atara
reduction with HI without phosphorous Ascorbate could work in principle, but it will undergo SN2 OH->I substitution. Cyclohexadiene ...	8-8-2020 at 09:33 by: clearly_not_atara
How come amines only form salts with the H+ cation? Ammonium is not a "salt" or traditionally understood metal complex. It is a covalently bonded molecu ...	7-8-2020 at 07:45 by: clearly_not_atara
Chloroacetic acid from glycine or another bullshit patent? "unstable blue liquid" sounds an awful lot like N2O3 Extraction is just easier; it was 1919, vacu ...	4-8-2020 at 13:20 by: clearly_not_atara
Chloroacetic acid from glycine or another bullshit patent? The stoichiometric reaction is not the physical reaction. The physical reaction is more like: NO3 ...	3-8-2020 at 16:00 by: clearly_not_atara
Making Reducing agents and oxidizing agents Remember that the "reduction potential" does not by itself imply any reducing activity. KH is a stro ...	3-8-2020 at 13:54 by: clearly_not_atara
Preparation of elemental phosphorus [rquote=640773&tid=65&author=metalresearcher]I succeeded. I heated 7g (NaPO3)6 + 3g Al + ...	2-8-2020 at 20:26 by: clearly_not_atara
(safer) fluorination of benzaldehyde? If diphenylimidazol-2-ylidene carbenes are available, salicylaldehyde can be deoxyfluorinated direct ...	2-8-2020 at 09:17 by: clearly_not_atara
Hydroxychloroquine, could an amateur make this stuff ? [rquote=641883&tid=155899&author=unionised] And it says "These interim trial results show t ...	31-7-2020 at 08:26 by: clearly_not_atara
Hydroxychloroquine, could an amateur make this stuff ? I would like to highlight something regarding the "scientists" who are pushing this hydroxychloroqui ...	30-7-2020 at 21:08 by: clearly_not_atara
Pyrolysis of Metal Sulfates Problem with this idea is that it's generally not effective or safe to lead SO3 gas into water with ...	28-7-2020 at 10:44 by: clearly_not_atara
Getting Discouraged With Organic Chemistry As A Hobby. Failed Steglich Esterification [quote]After allowing to warm to room temp, the mixture was already opaque with white precipitate.[/ ...	17-7-2020 at 18:25 by: clearly_not_atara
Ways to precipitate sodium ions? [rquote=640552&tid=155783&author=Draeger]I just want to recover other elements that are more ...	13-7-2020 at 08:48 by: clearly_not_atara
Is it possible to perform O-methylations in acetonitrile [rquote=640485&tid=155779&author=NaK] Shouldn't 82C be more than enough considering the boi ...	12-7-2020 at 21:21 by: clearly_not_atara
Ways to precipitate sodium ions? This is very hard. Ammonium fluorosilicate comes to mind. If uranium (!) is available, Na+ can be pr ...	12-7-2020 at 07:04 by: clearly_not_atara
Is it possible to perform O-methylations in acetonitrile It should be fine, I think it's just unpopular because the bp of acetonitrile is kind of low. In ...	11-7-2020 at 09:19 by: clearly_not_atara
Societal collapse: What do you think would be most needed? Seems like you'd still need the Haber process... and if you couldn't build a Haber reactor the easie ...	10-7-2020 at 08:48 by: clearly_not_atara
a new sustainable polymer? It doesn't appear that there are any reports using dichromate on isosorbide and Bromolone probably h ...	8-7-2020 at 10:15 by: clearly_not_atara
Best general purpose "OTC"-explosive not requiring detonators? What you're looking for is basically a chemical that is more sensitive to heat than shock. You're mo ...	7-7-2020 at 11:24 by: clearly_not_atara
Anhydrous Aluminum Chloride prepration Another approach would be to dissolve CuCl in acetonitrile... obviously you get half the molar yield ...	7-7-2020 at 09:54 by: clearly_not_atara
Anhydrous Aluminum Chloride prepration So apparently CuCl2 produces too much heat when you use it? We switched to ZnCl2 for this reason? ...	7-7-2020 at 07:46 by: clearly_not_atara
Precursors to um… something. Suggestions invited. You may be able to make 2-methylbenzoxazole by the following sequence of reactions: ethoxyethyl a ...	4-7-2020 at 08:54 by: clearly_not_atara
Acetic anhydride preparation [b]Refinery:[/b] You are obviously more interested in defending your previously stated opinions than ...	3-7-2020 at 08:23 by: clearly_not_atara
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