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Vilsmeier reagent/POCl3 formation The reaction with water should work as long as you add only one equivalent of water. Any POCl[sub]3[ ... |
16-5-2021 at 06:45 by: Texium |
Survey: Reagent Wish List [rquote=659810&tid=157426&author=njl]Glacial acetic acid too. I think it's one of the most v ... |
12-5-2021 at 15:17 by: Texium |
TLC results interpretation The benzyl alcohol may contain a small amount of benzaldehyde. That may be what the smaller, faster ... |
11-5-2021 at 09:11 by: Texium |
Perfluorpolyeter Exactly! |
8-5-2021 at 19:16 by: Texium |
Perfluorpolyeter I would expect that all the CF[sub]3[/sub]s listed at the end there are supposed to be attached to t ... |
8-5-2021 at 12:06 by: Texium |
Alcohol 99,9% It is likely that your ethanol contains some methanol, and vice versa. A simple distillation won’t ... |
8-5-2021 at 07:04 by: Texium |
24/40, 24/29, 29/32, what is the best? [rquote=659594&tid=157232&author=Blunotte]Hi Texium, I don't know if you can see from the im ... |
8-5-2021 at 05:35 by: Texium |
24/40, 24/29, 29/32, what is the best? Oooo bad bad bad... you’re heating a closed system! You need to include some way for pressure to e ... |
8-5-2021 at 05:21 by: Texium |
Using silver shot for a heat bath instead of sand? Copper or aluminum shot is already well known as an excellent heating medium. Presumably silver woul ... |
6-5-2021 at 09:06 by: Texium |
Question about Ethyl Bromide If you just want to experiment with alkyl halides in general, perhaps consider making a less volatil ... |
6-5-2021 at 07:43 by: Texium |
Path to 4-Anisaldehyde [rquote=659335&tid=157350&author=S.C. Wack]Acetic and sulfuric acids are often added. Good/b ... |
4-5-2021 at 07:18 by: Texium |
Hydroiodic acid from Vitamin C ! [rquote=659228&tid=157375&author=njl]Also the video says that the byproduct is "benzene hexo ... |
4-5-2021 at 07:14 by: Texium |
Path to 4-Anisaldehyde Yeah, it's best to grind up the aniseed into a fine powder before doing the steam distillation. That ... |
3-5-2021 at 13:15 by: Texium |
how to replicate this? Dry ice is pretty “vulgar” considering you can buy it at the grocery store. It’s the best answ ... |
2-5-2021 at 17:33 by: Texium |
Synthesis of Ethyl Methylphenylglycidate Seriously? Buy a ring stand or two and some utility clamps, and while you’re at it, we’re in the ... |
1-5-2021 at 18:58 by: Texium |
What chemistry are you working on. [rquote=659174&tid=157373&author=paulll]What is that you're working on, Texium? Interesting- ... |
30-4-2021 at 20:49 by: Texium |
Synthesis of Ethyl Methylphenylglycidate You're clearly going to need some experience with simpler stuff before you pursue this. If you want ... |
30-4-2021 at 20:02 by: Texium |
Synthesis of Ethyl Methylphenylglycidate Actually, njl is half-right. This compound can't be used to make phenylacetone. Its isomer can be. I ... |
30-4-2021 at 16:39 by: Texium |
Synthesis of Ethyl Methylphenylglycidate See things clearly? I hardly think you’re seeing clearly. You’ve seemed so pessimistic and paran ... |
30-4-2021 at 14:46 by: Texium |
What chemistry are you working on. Right now the only chemistry I'm working on is in the research lab, but here's a summary of the reac ... |
30-4-2021 at 11:26 by: Texium |
Path to 4-Anisaldehyde As I mentioned, it was a steam distillation, so... water. I'm afraid you won't want to bring out the ... |
29-4-2021 at 22:08 by: Texium |
Basic Chemicals and Glassware acquisition Well, I'm sorry that all of my suggestions for acquiring chemicals are not relevant to you then. I p ... |
29-4-2021 at 22:02 by: Texium |
Synthesis of Ethyl Methylphenylglycidate [rquote=659021&tid=157363&author=Russianwannabe76]I am interested in synthesizing ethyl meth ... |
29-4-2021 at 21:41 by: Texium |
Acetic anhydride preparation [rquote=659067&tid=9&author=njl]Atara is referring to a thread on the vespiary by user Scare ... |
29-4-2021 at 20:01 by: Texium |
preparation/acquisition of acetone (weird problem ik) [rquote=659066&tid=157362&author=njl]Methylacetylene is available from MAPP gas canisters, u ... |
29-4-2021 at 12:35 by: Texium |
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