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Vilsmeier reagent/POCl3 formation
The reaction with water should work as long as you add only one equivalent of water. Any POCl[sub]3[ ...
16-5-2021 at 06:45
by: Texium
Survey: Reagent Wish List
[rquote=659810&tid=157426&author=njl]Glacial acetic acid too. I think it's one of the most v ...
12-5-2021 at 15:17
by: Texium
TLC results interpretation
The benzyl alcohol may contain a small amount of benzaldehyde. That may be what the smaller, faster ...
11-5-2021 at 09:11
by: Texium
Perfluorpolyeter
Exactly!
8-5-2021 at 19:16
by: Texium
Perfluorpolyeter
I would expect that all the CF[sub]3[/sub]s listed at the end there are supposed to be attached to t ...
8-5-2021 at 12:06
by: Texium
Alcohol 99,9%
It is likely that your ethanol contains some methanol, and vice versa. A simple distillation won’t ...
8-5-2021 at 07:04
by: Texium
24/40, 24/29, 29/32, what is the best?
[rquote=659594&tid=157232&author=Blunotte]Hi Texium, I don't know if you can see from the im ...
8-5-2021 at 05:35
by: Texium
24/40, 24/29, 29/32, what is the best?
Oooo bad bad bad... you’re heating a closed system! You need to include some way for pressure to e ...
8-5-2021 at 05:21
by: Texium
Using silver shot for a heat bath instead of sand?
Copper or aluminum shot is already well known as an excellent heating medium. Presumably silver woul ...
6-5-2021 at 09:06
by: Texium
Question about Ethyl Bromide
If you just want to experiment with alkyl halides in general, perhaps consider making a less volatil ...
6-5-2021 at 07:43
by: Texium
Path to 4-Anisaldehyde
[rquote=659335&tid=157350&author=S.C. Wack]Acetic and sulfuric acids are often added. Good/b ...
4-5-2021 at 07:18
by: Texium
Hydroiodic acid from Vitamin C !
[rquote=659228&tid=157375&author=njl]Also the video says that the byproduct is "benzene hexo ...
4-5-2021 at 07:14
by: Texium
Path to 4-Anisaldehyde
Yeah, it's best to grind up the aniseed into a fine powder before doing the steam distillation. That ...
3-5-2021 at 13:15
by: Texium
how to replicate this?
Dry ice is pretty “vulgar” considering you can buy it at the grocery store. It’s the best answ ...
2-5-2021 at 17:33
by: Texium
Synthesis of Ethyl Methylphenylglycidate
Seriously? Buy a ring stand or two and some utility clamps, and while you’re at it, we’re in the ...
1-5-2021 at 18:58
by: Texium
What chemistry are you working on.
[rquote=659174&tid=157373&author=paulll]What is that you're working on, Texium? Interesting- ...
30-4-2021 at 20:49
by: Texium
Synthesis of Ethyl Methylphenylglycidate
You're clearly going to need some experience with simpler stuff before you pursue this. If you want ...
30-4-2021 at 20:02
by: Texium
Synthesis of Ethyl Methylphenylglycidate
Actually, njl is half-right. This compound can't be used to make phenylacetone. Its isomer can be. I ...
30-4-2021 at 16:39
by: Texium
Synthesis of Ethyl Methylphenylglycidate
See things clearly? I hardly think you’re seeing clearly. You’ve seemed so pessimistic and paran ...
30-4-2021 at 14:46
by: Texium
What chemistry are you working on.
Right now the only chemistry I'm working on is in the research lab, but here's a summary of the reac ...
30-4-2021 at 11:26
by: Texium
Path to 4-Anisaldehyde
As I mentioned, it was a steam distillation, so... water. I'm afraid you won't want to bring out the ...
29-4-2021 at 22:08
by: Texium
Basic Chemicals and Glassware acquisition
Well, I'm sorry that all of my suggestions for acquiring chemicals are not relevant to you then. I p ...
29-4-2021 at 22:02
by: Texium
Synthesis of Ethyl Methylphenylglycidate
[rquote=659021&tid=157363&author=Russianwannabe76]I am interested in synthesizing ethyl meth ...
29-4-2021 at 21:41
by: Texium
Acetic anhydride preparation
[rquote=659067&tid=9&author=njl]Atara is referring to a thread on the vespiary by user Scare ...
29-4-2021 at 20:01
by: Texium
preparation/acquisition of acetone (weird problem ik)
[rquote=659066&tid=157362&author=njl]Methylacetylene is available from MAPP gas canisters, u ...
29-4-2021 at 12:35
by: Texium
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