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Preparing elemental fluorine in your home lab ?
[rquote=267098&tid=22476&author=plante1999]I admire your wisdom Woelen and I agree I have on ...
27-11-2012 at 04:25
by: Mailinmypocket
Silicon Tetrafluoride - "Sand Gas"
[rquote=267052&tid=22494&author=garage chemist]Ouch. Are you using rubber stoppers or do you ...
26-11-2012 at 15:08
by: Mailinmypocket
Silicon Tetrafluoride - "Sand Gas"
[rquote=267037&tid=22494&author=garage chemist]Good job on replicating and documenting an ex ...
26-11-2012 at 14:47
by: Mailinmypocket
Silicon Tetrafluoride - "Sand Gas"
I found an old article relating to fluorides (see here http://www.sciencemadness.org/talk/viewthread ...
26-11-2012 at 12:37
by: Mailinmypocket
Bad days in the lab or with glassware?
[rquote=266993&tid=13214&author=kuro96inlaila]
Would superglue do the magic?:(

[Edited o ...
26-11-2012 at 11:38
by: Mailinmypocket
Hydrofluoric acid
Interesting article from the old days...


[file]21303[/file] [file]21305[/file] [file]21307[/fi ...
26-11-2012 at 07:22
by: Mailinmypocket
Latest chemical order?
[rquote=266968&tid=9890&author=borrowedlawyer][rquote=266930&tid=9890&author=Mailinm ...
26-11-2012 at 05:36
by: Mailinmypocket
Make Potassium (from versuchschemie.de)
The amount of t-butanol you are using seems to be a tad high compared to other successful results us ...
25-11-2012 at 17:02
by: Mailinmypocket
Latest chemical order?
1L of 50% HF in what seems to be an inappropriate bottle... Now I am debating disposing of it or reb ...
25-11-2012 at 15:00
by: Mailinmypocket
Pretty Pictures (1)
Ozone generator... Made with a test tube stuffed with Al foil and a wire coiled around the outside. ...
24-11-2012 at 13:50
by: Mailinmypocket
hexahydrate to monohydrate - what could I use ?
[rquote=266807&tid=22468&author=chemguy5000]My dear science friends,
I have a question abou ...
24-11-2012 at 10:43
by: Mailinmypocket
Make Potassium (from versuchschemie.de)
Well, I ordered some Shellsol :(

Not because I believe its the only solvent that will work, but I ...
22-11-2012 at 15:04
by: Mailinmypocket
question about exothermic reaction and Nonflammable Ration Heater (NRH)
I haven't read up on it but i remember a friend of mine in the forces told me that the material used ...
22-11-2012 at 10:29
by: Mailinmypocket
chemistry set appreciation
Some neat pictures from a time long forgotten: [url=http://forums.homesciencelab.com/viewtopic.php?f ...
21-11-2012 at 20:34
by: Mailinmypocket
Failed Methylethyl ketazine synthesis
[rquote=232824&tid=18487&author=aaparatuss]http://books.google.com/books?id=VqosZeMjNjEC& ...
21-11-2012 at 08:25
by: Mailinmypocket
Buying chinese glassware
[rquote=266459&tid=22409&author=l0k1]it doesn't make any difference whatsoever how tidy you ...
20-11-2012 at 07:00
by: Mailinmypocket
Make Potassium (from versuchschemie.de)
[rquote=264532&tid=14970&author=blogfast25]If so I would suggest to try: 1.55 g Mg, 3.06 KOH ...
19-11-2012 at 21:50
by: Mailinmypocket
Make Potassium (from versuchschemie.de)
[rquote=266430&tid=14970&author=Pok]I can imagine two reasons:

1. Maybe your lamp oil isn ...
19-11-2012 at 19:54
by: Mailinmypocket
Make Potassium (from versuchschemie.de)
The reason I didn't post the exact masses and timelines is because I followed the procedure done by ...
19-11-2012 at 17:28
by: Mailinmypocket
Pok's method
So, I tried again. Miserable failure, again.

I decided to follow the original process by Pok, I f ...
19-11-2012 at 16:07
by: Mailinmypocket
Buying chinese glassware
Just to be on the safe side, follow proper safety and storage procedures. Label everything meticulou ...
19-11-2012 at 15:21
by: Mailinmypocket
Buying chinese glassware
Well- don't worry about it, it seems like in the states pyro chemicals aren't that big a deal. Place ...
19-11-2012 at 15:03
by: Mailinmypocket
Stuck glass joints?
I downloaded a PDF from Sigma-Aldrich called "Safe Handling and Care of Glassware" It's by Corning a ...
19-11-2012 at 08:39
by: Mailinmypocket
Latest chemical order?
[rquote=266127&tid=9890&author=Hexavalent]All from eBay, total was £26.36:)

-500g copper ...
17-11-2012 at 14:05
by: Mailinmypocket
Phosphorus Pentachloride
He does. It is Len1 I believe
17-11-2012 at 12:34
by: Mailinmypocket
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