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Want to make dimethylglyoxime, works with hydroxylamine?
Read and thou shall be enlightened
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9-4-2019 at 01:13
by: Boffis |
Stabilizing ether with BHT
I often recycle ether and therefore have to distil it and then store the unstabilized material for a ... |
8-4-2019 at 07:27
by: Boffis |
Lead(II) and Manganese(II) formate syntheses
OK I have dried and weighed the product from the manganese II preparation and I obtained 20.69g and ... |
8-4-2019 at 07:20
by: Boffis |
Lead(II) and Manganese(II) formate syntheses
I had reason to prepare a small quantity of manganese II formate and the results I got today were ra ... |
7-4-2019 at 13:31
by: Boffis |
OC experiments that can be done without lab
@ipwn: Have you seen this book? It describes a lot of chemistry that can be done at home and how to ... |
4-4-2019 at 12:09
by: Boffis |
Gallic acid extraction
I posted a comparison of different types of "tannin" and "tannic acid" see this thread about halfway ... |
31-3-2019 at 10:28
by: Boffis |
What are some OTC thiols for thioketal formation?
I have prepared 1,4-butane-dithiol from 1,4-dibromobutane and either thiosemicarbazide or thiourea, ... |
26-3-2019 at 09:00
by: Boffis |
Want to make dimethylglyoxime, works with hydroxylamine?
This procedure is in Vogel's Textbook of organic chemistry 3rd ed for certain and possibly in the 5t ... |
24-3-2019 at 04:06
by: Boffis |
Any interesting uses for dimethylglyoxime?
@metacelsus, dimethylglyoxime can be cyclotized to dimethylfurazan and then oxidized to the correspo ... |
24-3-2019 at 03:53
by: Boffis |
Selective reduction of nitrotoluenes with Na2S
This is called the Zinin reaction and a review of this reactions has been posted at least twice befo ... |
9-2-2019 at 03:23
by: Boffis |
1,3-Diaminoacetone(1,3-diamino-2-propanone) problems
@divinyl, the preparation of diaminoacetone dihydrochloride is described in Shirley's "Preparation o ... |
19-1-2019 at 09:37
by: Boffis |
Easy synthesis of hydroiodic acid
@Felab, if the oxalate method works why not just make cadmium oxate and treat it likewise and you wi ... |
8-1-2019 at 10:55
by: Boffis |
Easy synthesis of hydroiodic acid
@Ajoker, I have used hydrogen sulphide as a reducing agent many time because it is so easily handled ... |
7-1-2019 at 11:47
by: Boffis |
Easy synthesis of hydroiodic acid
What is wrong with the traditional method of using Hydrogen sulphide and iodine. The hydrogen sulphi ... |
6-1-2019 at 08:17
by: Boffis |
diAmmine, diNitro Platinum
On the SM library there are several books on platinum metal chemistry and that is probably the best ... |
21-12-2018 at 10:44
by: Boffis |
how could I synthesize this molecule
1,3-diaminoacetone is prepared from acetonedicarboxylic acid via 1,3-diisonitrosoacetone. It is desc ... |
20-12-2018 at 08:47
by: Boffis |
UK supplier, which thread was it mentioned in?
Many thanks DavidJR and Sulaiman. Actually, the problem isn't the search engine as much as I couldn' ... |
13-12-2018 at 12:33
by: Boffis |
UK supplier, which thread was it mentioned in?
Hi, within about the last 3 months or so there was a thread in which an SM member (I can't remember ... |
8-12-2018 at 09:49
by: Boffis |
Resazurin synthesis (planning first steps)
I wonder if you could do this as a one-pot synthesis by dissolving 2 mol-equiv of resorcinol on ice ... |
29-11-2018 at 10:14
by: Boffis |
Resazurin synthesis (planning first steps)
Resazurin is a trivial name which tells us nothing about its constitution. In order to answer your q ... |
26-11-2018 at 23:44
by: Boffis |
Cyanide synthesis by thermal decomposition of Thiocyanate
As the thread seems to be wondering off coarse here is a excerpt from a book on the subject of the d ... |
16-11-2018 at 00:18
by: Boffis |
Extraction of gallic acid
Acetic acid will not hydrolyse complex tannins, you need a mineral acid, dilute hydrochloric or sulp ... |
14-11-2018 at 22:25
by: Boffis |
Looking for [2,2'-bithiophen]-5-yltrimethyl-stannane
The structure image doesn't correspond the the named compound. Its the 4-nitrophenyl rather than the ... |
13-11-2018 at 03:07
by: Boffis |
Cyanide synthesis by thermal decomposition of Thiocyanate
In the characterization of organic and inorganic compounds fused KSCN (I suspect NaSCN works too but ... |
11-11-2018 at 22:54
by: Boffis |
Cyanide synthesis by thermal decomposition of Thiocyanate
On a preparative scale you will need to add something to take up the sulphur otherwise they simply r ... |
10-11-2018 at 22:33
by: Boffis |
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