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nitroglycerin
Using the ratios given by palpy may give an undesirably high concentration of glycerol dinitrate in ...
22-9-2003 at 02:50
by: Microtek
Peroxide of Acetylacetone (2,4-pentandione) ??
If trying an untested synthesis of an unstable energetic compound, you should always begin with mini ...
18-9-2003 at 22:53
by: Microtek
hexamethylenetetramine dinitrate
My HMTD doesn't make DDT on its own either unless fully confined ( at least not in the small am ...
26-8-2003 at 01:49
by: Microtek
N2 - nitrogen from air
It is well known that different countries regulate different chemicals. For instance, I cannot legal ...
30-5-2003 at 00:09
by: Microtek
oleum & SO3
Industrially, the SO3 is absorbed in circulating concentrated H2SO4 which is then diluted with water ...
26-5-2003 at 01:00
by: Microtek
help with drying out ammonium nitrate please
Dry it in the oven at 120 C. This drives out enough of the moisture for most purposes.
24-5-2003 at 01:50
by: Microtek
heat capacity of Sorguyl
I think you should use the tabulated value of a somewhat similar material. And a heat capacity of 25 ...
15-5-2003 at 07:18
by: Microtek
Searching for Beilstein-synthesis of picramic acid
NH4-picramate is easy just partially reduce picric acid with NH4HS ( or (NH4)2S ). Just as easy as p ...
4-5-2003 at 23:26
by: Microtek
Bismuth dethroned as heaviest stable element.
In fact, even protons ( and thus all matter ) decays with a half life of 10^32 years.
27-4-2003 at 09:10
by: Microtek
Sucralose Nitrate
Remember that the sticky product will retain a LOT of acid after neutralization, so you should disso ...
25-4-2003 at 10:21
by: Microtek
Sucralose Nitrate
You should just use NH4NO3 + H2SO4 then. The AN dissolves nicely in sulfuric acid, though it tends t ...
24-4-2003 at 10:01
by: Microtek
Post from Mr Anonymous and my reply to it!
I presume that the NaCl would be produced by reaction of HCl gas with NaNO2 ? If this is the case I ...
9-4-2003 at 04:35
by: Microtek
RDX synthesis
Another exception: DAPT can be nitrated to diacetyl-dinitro tetrazocine with HNO3 + H2SO4 in a promi ...
7-4-2003 at 22:22
by: Microtek
Acetaldehyde, the holy grail-method
Formic acid is easily made by reaction of anhydrous ( or nearly so; it is sufficient to heat 85% gly ...
6-4-2003 at 21:55
by: Microtek
Ni from coins
NiS does not precipitate below about Ph 0.4 but CuS does, so adjust the acidity to about this level ...
24-3-2003 at 23:23
by: Microtek
a question
Mixed acids work just fine, as does H2SO4 + alkali metal nitrate though the yield suffers. You don&# ...
23-3-2003 at 03:15
by: Microtek
Trinitrotoluene preparation
Oleum is unneccessary; you can use fuming nitric acid instead ( not as a substitute of course, but a ...
22-3-2003 at 06:04
by: Microtek
Aluminium Nitrate Synthesis
I tried the complex from mr A's referenced patent, mixing supposed Al(NO3)3 prepared as I have ...
14-3-2003 at 13:22
by: Microtek
Aluminium Nitrate Synthesis
If this even works it will be extremely messy and difficult to separate. I suggest this:

Al + 3 ...
13-3-2003 at 12:11
by: Microtek
perchloric acid
Silveracetylide-nitrate can be made by bubbling acetylene through a solution of silver in nitric aci ...
6-3-2003 at 11:00
by: Microtek
P2O5 solvent
From a lab supply. I function as a freelance researcher for a small business so I can get most chemi ...
26-2-2003 at 04:10
by: Microtek
Dinitroacetone peroxide
If I draw inositol hexanitrate ( inositol is a cyclohexane ring with OH-groups on all carbons ) and ...
24-2-2003 at 00:45
by: Microtek
picramic acid from picric
But it is not a partial reduction. You will likely get triaminophenol with Fe/HCl. Of course you cou ...
22-2-2003 at 05:56
by: Microtek
P2O5 solvent
In that patent Xoo posted, they used chloroform as their preferred embodiment. I'm pretty sure ...
21-2-2003 at 09:42
by: Microtek
P2O5 solvent
Just a quick question:
I'm looking for a nice inert solvent for P2O5 to eliminate some of the ...
20-2-2003 at 01:38
by: Microtek
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