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Isocyanate synthesis via halide displacement
[rquote=649418&tid=156558&author=ArbuzToWoda]
Maybe, but why do we need to come up with alt ...
19-11-2020 at 12:19
by: clearly_not_atara
Ammonia by the haber process--tabletop chemistry
[rquote=649335&tid=13838&author=Fluorite]
https://m.youtube.com/watch?v=8LriocEzpC0 They tr ...
18-11-2020 at 10:21
by: clearly_not_atara
perchlorate without electricity
PbO2 <> Pb2+ SEP = +1.5 V, ClO4- <> ClO3- SEP = +1.2 V, so this reaction is at least not ...
16-11-2020 at 07:48
by: clearly_not_atara
Acid Chlorides
The best way I know to make alpha-halo ethers is to use the reaction of acetals with ZnCl2 and acety ...
16-11-2020 at 07:40
by: clearly_not_atara
Free radical bromination on only the terminal ends of hexane
[rquote=649166&tid=156532&author=Triflic Acid]@clearly_not_atara Is there any way to create ...
15-11-2020 at 19:30
by: clearly_not_atara
Acid Chlorides
You're confusing electrophilic chlorination with nucleophilic chlorination. C3N3Cl3 transfers Cl-. C ...
15-11-2020 at 19:12
by: clearly_not_atara
Free radical bromination on only the terminal ends of hexane
TA: if you brominate at random the chance of getting 1,6 is one in 15, a 6.7% yield before you even ...
15-11-2020 at 08:55
by: clearly_not_atara
Free radical bromination on only the terminal ends of hexane
Hm... Wurtz coupling of allyl bromide and anti-Markovnikov dihydrobromination of the 1,5-hexadiene w ...
14-11-2020 at 18:38
by: clearly_not_atara
Iodine did not precipitate from Potassium Iodide? (HCL+ H2O2)
Use H2SO4/H3PO4, since these do not form complexes with I+ or I3+ ions. It may be possible to recove ...
14-11-2020 at 13:35
by: clearly_not_atara
diethyl carbonate (NO PHOSGENE)
So I'm not sure if you're aware, but ethylene glycol and urea makes ethylene carbonate, not diethyl ...
11-11-2020 at 18:24
by: clearly_not_atara
Sodium benzoate -> Ferric benzoate (and similar rxns)
I thought it was the ferrous salts?

Anyway you could start from ferrous sulfate and calcium benzo ...
10-11-2020 at 15:14
by: clearly_not_atara
Straight-chain acyl chlorides from TCCA and aldehyde
It's highly unlikely. The same reaction is well-known for benzoyl and alpha-quaternary chlorides (th ...
9-11-2020 at 12:04
by: clearly_not_atara
Acetic anhydride preparation
[rquote=648344&tid=156476&author=Triflic Acid]So how do I convert benzyl-acetic anhydride to ...
6-11-2020 at 05:24
by: clearly_not_atara
Acetic anhydride preparation
You actually need to do the double dehydrohalogenation in two steps because otherwise you'll probabl ...
5-11-2020 at 14:35
by: clearly_not_atara
Acetic anhydride preparation
It would have to be 1-phenylpropyne in order for cleavage to generate an acetyl anhydride. Phenylace ...
5-11-2020 at 10:08
by: clearly_not_atara
Can I have an account at the SM wiki?
oh yeah me too if that's a thing

it's low effort day
1-11-2020 at 17:18
by: clearly_not_atara
GRE Chemistry 3rd edition for sale.
Be careful with those manuals. I used one to study for the GRE physics and only realized on the day ...
1-11-2020 at 13:33
by: clearly_not_atara
Acid Chlorides
The best anyone can do with that is "maybe" since we don't have a very good idea of how (or when) th ...
30-10-2020 at 16:14
by: clearly_not_atara
How to cut 1oz silver bar into pieces that will fit in a test tube
[rquote=647786&tid=156433&author=itsallgoodjames]
The NO2 isn't really all that much of a c ...
30-10-2020 at 12:16
by: clearly_not_atara
How to cut 1oz silver bar into pieces that will fit in a test tube
Agree with unionised, or at least [i]try[/i] hammering it, it allows you to cut more accurately and ...
30-10-2020 at 08:43
by: clearly_not_atara
Amateur route from R-OH to R-Cl
If the resulting alkyl chloride is soluble in water, you might be able to use an iodide (or bromide) ...
27-10-2020 at 15:00
by: clearly_not_atara
DIY acid washed sand changed color unexpectedly
Your sand looks greenish, that suggests iron or nickel chlorides. If there is some kind of alkali in ...
26-10-2020 at 17:13
by: clearly_not_atara
Acyl chlorides stability
I see no reasonable formation pathway for phosgene from acetyl chloride.

A [i]tiny[/i] amount of ...
26-10-2020 at 15:57
by: clearly_not_atara
Is the mad science report newsletter ready to be added to prepublication
We want typesetting!

I'll try to mock something up this weekend if nobody gets to it before me.
26-10-2020 at 07:01
by: clearly_not_atara
Acetic anhydride preparation
[rquote=647176&tid=9&author=teodor]
I will not force anybody to use this substance, just wa ...
23-10-2020 at 06:22
by: clearly_not_atara
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