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Gas-phase apparatus construction
Good price. Those are usually about 3,000 USD for the ones that get to 1200C. I use two such pieces ...
17-1-2007 at 19:38
by: Fleaker
Mad Science at the max, where do you draw the line?
For me, any nerve agent or drug I will never, ever make. Also, no extreme radioactive materials of a ...
17-1-2007 at 19:01
by: Fleaker
Subjects Of A Questionable Nature
@Sauron: The first few pages of your Alfa Aesar or Sigma Aldrich catalog will tell you what schedule ...
13-1-2007 at 21:56
by: Fleaker
Distillation of ethanol
Ah Sauron, I see now. I thought you meant taking it from 95% to 100% anhydrous with sodium. That see ...
11-1-2007 at 17:14
by: Fleaker
Distillation of ethanol
If your feedstock is free it can be made to work. I have a friend who gets free sugar beets and make ...
11-1-2007 at 14:07
by: Fleaker
Distillation of ethanol
I still do not see the harm in using sieve. Some people love to use sodium wire to dry ethanol, but ...
11-1-2007 at 13:57
by: Fleaker
What Complete BS is this?
Isn't it akin to grotesque fascination? After all, isn't that why so many watch NASCAR, not to see i ...
10-1-2007 at 12:48
by: Fleaker
Any of these chems OTC?
No Mg fire starters? That's a shame as they're relatively pure. I suppose you could look for magnesi ...
4-1-2007 at 16:38
by: Fleaker
Quick question
Benzene, toluene, and xylenes are all used in high test ''race gases''.
3-1-2007 at 18:44
by: Fleaker
What do to with KMnO4?
On the small scale, this picture represents perhaps 3g of permanganate added to an excess sulfuric a ...
2-1-2007 at 00:19
by: Fleaker
Storing sodium
Here is a picture of that sodium metal from the can mentioned up above for reference. This was rathe ...
1-1-2007 at 23:42
by: Fleaker
Laboratory Pictures
Just a smattering of pics from the old laboratory my friend and I experimented in. Might as well pos ...
1-1-2007 at 22:33
by: Fleaker
Making own Nitric Acid
Sorry to resurrect an old thread, but my lab partner (NERV) and I are distilling more nitric acid to ...
1-1-2007 at 20:35
by: Fleaker
chemicals and elements available
What salts do you have? U2U me, I'm interested.
30-12-2006 at 22:55
by: Fleaker
Separation of Iodine from Xylene
Good idea Eclectic. As I recall, what you get depends on what the temperature/concentration of the N ...
30-12-2006 at 13:39
by: Fleaker
Spammers
I do not think we need more moderators...from what I've seen, simply reporting offensive/spammatory ...
30-12-2006 at 10:59
by: Fleaker
ridiculous ebay stuff
All too expensive, not enough feed back. Mercury is twice is much as it should be with shipping!

...
29-12-2006 at 12:05
by: Fleaker
Separation of Iodine from Xylene
"I was originally thinking AlI3 plus 3 moles water to iodine and Al(OH)3, but I'm unsure as to wheth ...
29-12-2006 at 11:56
by: Fleaker
Best and worst smelling chemicals?
[quote][i]Originally posted by JohnWW[/i]
Has anyone here actually smelled either H2Se, H2Te, H2Po, ...
29-12-2006 at 09:08
by: Fleaker
dry ethanol, ether, THF...
"Use a freshly opened bottle of absolute alcohol, distill it over sodium directly into rxn flask. "
...
25-12-2006 at 20:01
by: Fleaker
Victim of political correctness
Maybe he gave himself some sort of heavy metal poisoning which made him go mad. He has been extremel ...
12-12-2006 at 17:07
by: Fleaker
Storing methylene chloride
Or perhaps you can use a glass bottle with a phenolic cap? On my bottle of reagent grade dichloromet ...
6-12-2006 at 17:24
by: Fleaker
Recruits!!
[quote][i]Originally posted by woelen[/i]
I also am quite open about my experimenting and many peop ...
5-12-2006 at 16:45
by: Fleaker
Chemicals/labware to avoid?
Most importantly, I would use common sense. Oddly as this sounds, I advise you to read up on what is ...
5-12-2006 at 16:31
by: Fleaker
Recovery of silver nitrate from Anetek
First off, could you explain what Anetek is, and you have 11 troy pounds of what?
3-12-2006 at 16:47
by: Fleaker
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