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Preparation of dinitroacetone
Since the direct nitration of acetone is too risky, I have begun considering alternate routes of pre ...
21-5-2002 at 16:14
by: madscientist
Ammonium permanganate preparation
A problem with preparing ammonium permanganate in aqueous solution has just occured to me. The NH4Mn ...
21-5-2002 at 16:03
by: madscientist
Preparation of nitrostarch
I still managed to get about ten grams of nitrostarch from my attempted nitration of twenty grams of ...
21-5-2002 at 12:01
by: madscientist
Preparation of nitrostarch
What the hell is going on? This is very strange. I had my sludgey mixture of nitrostarch and starch ...
21-5-2002 at 12:00
by: madscientist
Preparation of nitrostarch
Important information... As one should know, virtually all industrially produced acetone contains be ...
21-5-2002 at 11:58
by: madscientist
Preparation of nitrostarch
Hrm, I sure have heard otherwise from reputable sources, such as chemistry books and encyclopedias. ...
21-5-2002 at 11:57
by: madscientist
Preparation of nitrostarch
I am curious about nitration times. How long will it take to fully nitrate starch at about 0-5 degre ...
21-5-2002 at 11:56
by: madscientist
Nitromethane extraction
I would think that would be dangerously risky.
21-5-2002 at 11:53
by: madscientist
Organic peroxides
Hexamethylenetetramine (also called "hexamine" or "methanamine") is also sold as "Urotropine", a uri ...
21-5-2002 at 11:47
by: madscientist
Organic peroxides
Excerpt from one of my chemistry texts:

[i]There are many organic peroxides and hydroperoxides.
...
21-5-2002 at 11:46
by: madscientist
Organic peroxides
I don't see why the oxidation of isopropanol would form hydrogen peroxide. Isopropanol would probabl ...
21-5-2002 at 11:43
by: madscientist
Organic peroxides
I would forget trying to set off pure ammonium nitrate. I would make ANFO with it (about 96% prilled ...
21-5-2002 at 11:40
by: madscientist
Organic peroxides
Organic peroxides are a type of chemical. Many are explosive in nature. They are organic compounds ( ...
21-5-2002 at 11:34
by: madscientist
Preparation of cyanides
Yes, that is true. I realized that ammonium oxalate would probably decompose into ammonia and oxalic ...
21-5-2002 at 09:08
by: madscientist
Preparation of cyanides
Alternative method of production, by madscientist PREPARATION OF HYDROGEN CYANIDE FROM POTASSIUM PER ...
21-5-2002 at 09:04
by: madscientist
Extraction of HCl from solvent
I have heard that it is very difficult to find sulfuric acid in some countries other than the United ...
21-5-2002 at 08:56
by: madscientist
Toxic-gas liberating explosives
Nitrotrichloroacetamide (CCl3CONHNO2) would be a very effective chemical weapon. It is an explosive ...
20-5-2002 at 20:15
by: madscientist
Toxic-gas liberating explosives
Here are a few ideas for energetic compounds that would liberate toxic gasses when detonated:

(CH ...
20-5-2002 at 20:14
by: madscientist
Methyl Ethyl Ketone Peroxide
Another name for methyl ethyl ketone could be isobutanone.I recently prepared some methyl ethyl keto ...
20-5-2002 at 20:11
by: madscientist
Methyl Ethyl Ketone Peroxide
It depends what kind of ether you are using... there is isopropol ether,ethyl ether, propyl ether, m ...
20-5-2002 at 20:10
by: madscientist
Methyl Ethyl Ketone Peroxide
It seems that dimeric 2-peroxybutane (MEKP) is more stable than previously thought. It does not expl ...
20-5-2002 at 20:08
by: madscientist
Methyl Ethyl Ketone Peroxide
That post was written in a text file on my computer... I simply copied and pasted it back in here.
20-5-2002 at 20:07
by: madscientist
Methyl Ethyl Ketone Peroxide
I recently prepared some methyl ethyl ketone peroxide. This time it was a higher isomer, it is a mix ...
20-5-2002 at 20:06
by: madscientist
Methyl Ethyl Ketone Peroxide
PREPARATION AND PROPERTIES OF METHYL ETHYL KETONE PEROXIDE

The three most common forms of methyl ...
20-5-2002 at 20:06
by: madscientist
Carboxyl amines
So, a peroxycarboxylic acid can be prepared by reacting a carboxylic acid with hydrogen peroxide in ...
20-5-2002 at 19:44
by: madscientist
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